Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_P\Data\PP022718\ Data File : PP024025.D Signal(s) : Signal #1: ECD1A.CH Signal #2: ECD2B.CH Acq On : 28 Feb 2018 7:07 Operator : UA/AJ Sample : J1161-02 Misc : HERB Soil LOQ; 400 PPB ECD_P ALS Vial : 44 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Feb 28 13:14:22 2018 Quant Method : P:\HPCHEM1\ECD_P\methods\PP020618.M Quant Title : 8080.M QLast Update : Tue Feb 06 02:07:55 2018 Response via : Initial Calibration Integrator: ChemStation 6890 Scale Mode: Large solvent peaks clipped Volume Inj. : 2 µl Signal #1 Phase : Rtx-CLPesticides Signal #2 Phase: Rtx-CLPesticides2 Signal #1 Info : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x 0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 4) S 2,4-DCAA 11.573 11.361 424.7E6 467.1E6 828.735 770.226m Target Compounds 1) T Dalapon 3.019 2.554 167.4E6 394.1E6 209.715 476.115m# 2) T 3,5-DICHL... 9.983 9.482 235.1E6 249.9E6 295.194 299.651 3) T 4-Nitroph... 11.156 10.523 75173882 82934336 174.835 178.699m 5) T DICAMBA 11.891 11.660 662.7E6 712.5E6 308.200 313.739 6) T MCPP 12.221 11.860 51410727 42695729 35.064m 26.535 7) T MCPA 12.473 12.249 59153590 57646548 26.856m 24.756m 8) T DICHLORPROP 13.074 12.771 174.0E6 189.1E6 327.536 322.040 9) T 2,4-D 13.434 13.257 204.8E6 242.4E6 305.875 315.789 10) T Pentachlo... 13.823 13.817 2698.5E6 2918.9E6 331.952 339.038 11) T 2,4,5-TP ... 14.686 14.413 1018.6E6 1100.1E6 307.496 307.489 12) T 2,4,5-T 15.085 15.044 921.3E6 889.4E6 294.875 288.700m 13) T 2,4-DB 15.826 15.638 117.2E6 149.7E6 298.057m 346.247m 14) T DINOSEB 17.293 16.039 604.3E6 638.1E6 263.276 259.406 15) T Picloram 17.106 17.384 1221.7E6 1264.0E6 250.937 253.755 16) T DCPA 17.660 17.261 825.5E6 1007.5E6 210.518 231.549 --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. PP020618.M Fri May 04 15:15:15 2018