INSTRUMENT CONTROL PARAMETERS: ECD-P --------------------------------------- C:\MassHunter\GCMS\1\methods\BAKE.M Fri Aug 19 20:12:51 2022 Control Information ------- ----------- Sample Inlet : GC Injection Source : GC ALS Injection Location: Front No Sample Prep method has been assigned to this method. ============================================================================= 6890 GC METHOD ============================================================================= OVEN Equilibration time: 0.50 min Maximum temp: 330 C Initial temp: 250 C (On) Initial time: 0.50 min Ramps: # Rate Final temp Final time 1 35.00 300 10.00 2 0 (Off) Post temp: 0 C Post time: 0.00 min Run time: 11.93 min FRONT INLET (SPLIT/SPLITLESS) Mode: Split Initial temp: 220 C (On) Pressure: 17.8 psi (On) Split ratio: 1.76:1 Split flow: 7.1 mL/min Total flow: 12.8 mL/min Gas saver: On Saver flow: 20.0 mL/min Saver time: 2.00 min Gas type: Helium BACK INLET (UNKNOWN) COLUMN 1 Capillary Column Serial Number: MR1 Max temperature: 340 C Nominal length: 30.0 m Nominal diameter: 320.00 um Nominal film thickness: 0.50 um Calibrated length: 30.0 m Calibrated diameter: 320.00 um Mode: constant pressure Pressure: 17.8 psi Nominal initial flow: 2.0 mL/min Average velocity: 44 cm/sec Inlet: Front Inlet Outlet: Front Detector Outlet pressure: ambient COLUMN 2 Capillary Column Serial Number: MR2 Max temperature: 340 C Nominal length: 30.0 m Nominal diameter: 320.00 um Nominal film thickness: 0.25 um Calibrated length: 30.0 m Calibrated diameter: 320.00 um Mode: (see column 1) Pressure: 17.8 psi Nominal initial flow: 2.0 mL/min Average velocity: 44 cm/sec Inlet: Front Inlet Outlet: Back Detector Outlet pressure: ambient FRONT DETECTOR (uECD) Temperature: 320 C (On) Mode: Constant makeup flow Makeup flow: 60.0 mL/min (On) Makeup Gas Type: Argon methane 5% Electrometer: On BACK DETECTOR (uECD) Temperature: 320 C (On) Mode: Constant makeup flow Makeup flow: 60.0 mL/min (On) Makeup Gas Type: Argon methane 5% Electrometer: On SIGNAL 1 Data rate: 20 Hz Type: front detector Save Data: On Start Save Time: 1.50 min Stop Save Time: 11.92 min SIGNAL 2 Data rate: 20 Hz Type: back detector Save Data: On Start Save Time: 1.50 min Stop Save Time: 11.92 min POST RUN Post Time: 0.00 min INJECTOR 1 Sample pre-washes: 2 Sample pumps: 2 Sample Volume (uL): 1.000 Syringe size (uL): 10.0 Pre washes from bottle A: 2 Pre washes from bottle B: 1 Post washes from bottle A: 1 Post washes from bottle B: 1 Viscosity delay (seconds): 0 Pre injection dwell (min): 0.00 Post injection dwell (min): 0.00 Sample skim depth (mm): 0.0 (Off) Plunger Speed: Fast Solvent saver: Off Solvent Wash Mode: A, B Waste Bottle Use: A Only ALS ERRORS: On missing vial: pause TIME TABLE Time(min) Parameter & Setpoint Column 1 Inventory Number : Column 2 Inventory Number : END OF INSTRUMENT CONTROL PARAMETERS ------------------------------------