Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_R\Data\PR022618\ Data File : PR025651.D Signal(s) : Signal #1: ECD1A.ch Signal #2: ECD2B.ch Acq On : 26 Feb 2018 12:48 Operator : UA/SM Sample : AR1254 LOQ Misc : 100PPB WATER ECD_R ALS Vial : 18 Sample Multiplier: 1 Integration File signal 1: events.e Integration File signal 2: events2.e Quant Time: Feb 27 02:27:19 2018 Quant Method : P:\HPCHEM1\ECD_R\Method\PR021018.M Quant Title : GC EXTRACTABLES QLast Update : Thu Feb 08 01:43:39 2018 Response via : Initial Calibration Integrator: ChemStation Volume Inj. : 2 µl Signal #1 Phase : ZB-MR1 Signal #2 Phase: ZB-MR2 Signal #1 Info : 30Mx0.32mmx 0.50µ Signal #2 Info : 30M x 0.32mm x 0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 1) SA Tetrachlo... 4.396 3.771 400.7E6 687.3E6 23.799 23.944 2) SA Decachlor... 10.019 8.756 308.3E6 544.5E6 27.231 25.741m Target Compounds 26) L6 AR-1254-1 5.813 5.081 48635325 87824401 119.603 129.461 27) L6 AR-1254-2 6.604 5.786 129.5E6 129.0E6 122.818 87.158m# 28) L6 AR-1254-3 6.966 6.188 152.5E6 273.6E6 135.364 111.774m 29) L6 AR-1254-4 7.248 6.412 118.9E6 133.8E6 145.397 88.382m# 30) L6 AR-1254-5 7.664 6.829 99887690 211.3E6 120.875 105.972m --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.