INSTRUMENT CONTROL PARAMETERS: ECD_R --------------------------------------- D:\MassHunter\GCMS\1\methods\PCB.M Mon Feb 26 21:33:57 2018 Control Information ------- ----------- Sample Inlet : GC Injection Source : GC ALS Injection Location: Front No Sample Prep method has been assigned to this method. GC Oven Temperature Setpoint On (Initial) 150 °C Hold Time 0.5 min Post Run 0 °C Program #1 Rate 35 °C/min #1 Value 220 °C #1 Hold Time 0 min #2 Rate 20 °C/min #2 Value 330 °C #2 Hold Time 4 min Equilibration Time 0.5 min Max Temperature 330 °C Maximum Temperature Override Enabled Slow Fan Disabled Cryo Off ALS Front Injector Syringe Size 10 μL Injection Volume 2 μL Solvent A Washes (PreInj) 1 Solvent A Washes (PostInj) 3 Solvent A Volume 8 μL Solvent B Washes (PreInj) 1 Solvent B Washes (PostInj) 3 Solvent B Volume 8 μL Sample Washes 1 Sample Wash Volume 8 μL Sample Pumps 2 Dwell Time (PreInj) 0 min Dwell Time (PostInj) 0 min Solvent Wash Draw Speed 300 μL/min Solvent Wash Dispense Speed 3000 μL/min Sample Wash Draw Speed 300 μL/min Sample Wash Dispense Speed 3000 μL/min Injection Dispense Speed 6000 μL/min Viscosity Delay 0 sec Sample Depth Disabled Injection Type Standard L1 Airgap 0.2 μL Solvent Wash Mode A-A6,B-B4 Sample Overlap Mode Sample overlap is not enabled ALS Errors Pause for user interaction Front SS Inlet He Mode Split Heater On 250 °C Pressure On 7.8861 psi Total Flow On 9 mL/min Septum Purge Flow On 3 mL/min Gas Saver On 20 After 2 min mL/min Split Ratio 5 :1 Split Flow 6.5878 mL/min Column Column #1 Flow Setpoint Off (Initial) 1.3176 mL/min Post Run 2 mL/min 0 °C—325 °C (325 °C): 30 m x 320 μm x 0.5 μm Column lock Unlocked In Front SS Inlet He Out Front Detector μECD (Initial) 150 °C Pressure 9.8663 psi Flow 1.3176 mL/min Average Velocity 28.593 cm/sec Holdup Time 1.7487 min Column #2 Flow Setpoint Off (Initial) 1 mL/min Post Run 1 mL/min 0 °C—325 °C (325 °C): 30 m x 320 μm x 0.5 μm Column lock Unlocked In Front SS Inlet He Out Back Detector μECD (Initial) 150 °C Pressure 7.8861 psi Flow 1 mL/min Average Velocity 22.992 cm/sec Holdup Time 2.1746 min Column Outlet Pressure 0 psi Front Detector μECD Heater On 320 °C Makeup Flow On 60 mL/min Electrometer On Back Detector μECD Heater On 320 °C Makeup Flow On 60 mL/min Electrometer On Signals Signal #1: Front Signal Description Front Signal Details Front Signal (μECD) Save On Data Rate 50 Hz Dual Injection Assignment Front Sample Signal #1 Events #1 Time 0 min #1 Event Freeze Signal #2 Time 3 min #2 Event Resume Signal Signal #2: Back Signal Description Back Signal Details Back Signal (μECD) Save On Data Rate 50 Hz Dual Injection Assignment Back Sample Signal #2 Events #1 Time 0 min #1 Event Freeze Signal #2 Time 3 min #2 Event Resume Signal Signal #3: Test Plot Description Test Plot Details Save Off Data Rate 50 Hz Dual Injection Assignment Back Sample Signal #4: Test Plot Description Test Plot Details Save Off Data Rate 50 Hz Dual Injection Assignment Back Sample END OF INSTRUMENT CONTROL PARAMETERS ------------------------------------