INSTRUMENT CONTROL PARAMETERS:    Instrument #2
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   C:\MSDCHEM\2\METHODS\BNA_F.M

Control Information
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Sample Inlet      :  GC
Injection Source  :  GC ALS
Mass Spectrometer :  Enabled

=============================================================================
                                6890 GC METHOD
=============================================================================


OVEN
   Initial temp:  40 'C (On)               Maximum temp:  340 'C
   Initial time:  3.40 min                 Equilibration time:  0.50 min
   Ramps:
      #  Rate  Final temp  Final time
      1 25.00      320        7.00
      2   0.0(Off)
   Post temp:  0 'C
   Post time:  0.00 min
   Run time:  21.60 min


FRONT INLET (SPLIT/SPLITLESS)           BACK INLET (UNKNOWN)
   Mode:  Pulsed Splitless
   Initial temp:  275 'C (On)
   Pressure:  23.00 psi (On)
   Pulse pressure:  44.0 psi
   Pulse time:  0.70 min
   Purge flow:  16.1 mL/min
   Purge time:  0.00 min
   Total flow:  19.8 mL/min
   Gas saver:  Off
   Gas type:  Helium


COLUMN 1                                COLUMN 2
   Capillary Column                        (not installed)
   Model Number:  Agilent 121-9723
   20M X 0.18mm X 0.36um
   Max temperature:  350 'C
   Nominal length:  20.0 m
   Nominal diameter:  180.00 um
   Nominal film thickness:  0.36 um
   Mode:  constant flow
   Initial flow:  1.2 mL/min
   Nominal init pressure:  23.01 psi
   Average velocity:  49 cm/sec
   Inlet:  Front Inlet
   Outlet:  MSD
   Outlet pressure:  vacuum


FRONT DETECTOR (NO DET)                 BACK DETECTOR (NO DET)


SIGNAL 1                                SIGNAL 2
   Data rate:  20 Hz                       Data rate:  20 Hz
   Type:  test plot                        Type:  test plot
   Save Data:  Off                         Save Data:  Off
   Zero:  0.0 (Off)                        Zero:  0.0 (Off)
   Range:  0                               Range:  0
   Fast Peaks:  Off                        Fast Peaks:  Off
   Attenuation:  0                         Attenuation:  0


COLUMN COMP 1                           COLUMN COMP 2
   (No Detectors Installed)                (No Detectors Installed)


THERMAL AUX 2
   Use:  MSD Transfer Line Heater
   Description:
   Initial temp:  320 'C (On)
   Initial time:  0.00 min
      #  Rate  Final temp  Final time
      1   0.0(Off)


                                        POST RUN
                                           Post Time: 0.00 min


TIME TABLE
   Time       Specifier                     Parameter & Setpoint




                               GC Injector


     Front Injector:
        Sample Washes                 1
        Sample Pumps                  2
        Injection Volume           1.00 microliters
        Syringe Size               10.0 microliters
        PreInj Solvent A Washes       3
        PreInj Solvent B Washes       3
        PostInj Solvent A Washes      3
        PostInj Solvent B Washes      3
        Viscosity Delay               0 seconds
        Plunger Speed              Fast
        PreInjection Dwell         0.00 minutes
        PostInjection Dwell        0.00 minutes


     Back Injector:
No parameters specified

 Column 1 Inventory Number : AGILENT DB
 Column 2 Inventory Number :  

                                MS ACQUISITION PARAMETERS


General Information
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Tune File                : 092415.U
Acquistion Mode          : Scan


MS Information
-- -----------

Solvent Delay            : 2.05 min

EM Absolute              : False
EM Offset                : 12
Resulting EM Voltage     : 1552.9

[Scan Parameters]

Low Mass                 : 35.0
High Mass                : 550.0
Threshold                : 300
Sample #                 : 3       A/D Samples    8

[MSZones]

MS Quad                  : 200 C   maximum 200 C
MS Source                : 300 C   maximum 300 C


                             END OF MS ACQUISITION PARAMETERS


                              TUNE PARAMETERS for SN:  
                        -----------------------------

 EMISSION    :      34.610
 ENERGY      :      69.922
 REPELLER    :      22.584
 IONFOCUS    :      75.922
 ENTRANCE_LE :       0.000
 EMVOLTS     :    1541.176
 AMUGAIN     :    1124.000
 AMUOFFSET   :     132.688
 FILAMENT    :       1.000
 DCPOLARITY  :       0.000
 ENTLENSOFFS :     16.314@  3    16.314@ 50    12.800@ 69    13.051@131    14.557@219    15.812@414    18.573@502    18.573@1049 
 MASSGAIN    :    -939.000   
 MASSOFFSET  :     -39.000   


                           END OF TUNE PARAMETERS
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                               END OF INSTRUMENT CONTROL PARAMETERS
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