Evaluate Continuing Calibration Report Data Path : Z:\HPCHEM1\BNA_F\Data\BF021214\ Data File : BF068753.D Acq On : 13 Feb 2014 00:25 Operator : JDU Sample : SSTDCCC040 Misc : ALS Vial : 2 Sample Multiplier: 1 Quant Time: Feb 13 02:59:11 2014 Quant Method : Z:\HPCHEM1\BNA_F\METHOD\8270-BF020714.M Quant Title : ASP BNA STANDARDS FOR 5 POINT CALIBRATION QLast Update : Sat Feb 08 05:51:57 2014 Response via : Initial Calibration Min. RRF : 0.000 Min. Rel. Area : 50% Max. R.T. Dev 0.50min Max. RRF Dev : 25% Max. Rel. Area : 150% Compound Amount Calc. %Dev Area% Dev(min) ------------------------------------------------------------------------- 1 I 1,4-Dichlorobenzene-d4 20.000 20.000 0.0 111 -0.06 2 1,4-Dioxane 40.000 38.902 2.7 113 -0.07 3 Pyridine 40.000 42.060 -5.2 105 -0.09 4 n-Nitrosodimethylamine 40.000 39.262 1.8 103 -0.08 5 S 2-Fluorophenol 80.000 79.969 0.0 108 -0.07 6 Aniline 40.000 40.079 -0.2 110 -0.06 7 S Phenol-d6 80.000 85.660 -7.1 116 -0.05 8 2-Chlorophenol 40.000 42.681 -6.7 113 -0.06 9 Benzaldehyde 40.000 39.603 1.0 108 -0.06 10 C Phenol 40.000 41.564 -3.9 120 -0.05 11 bis(2-Chloroethyl)ether 40.000 40.471 -1.2 107 -0.06 12 1,3-Dichlorobenzene 40.000 41.844 -4.6 114 -0.06 13 C 1,4-Dichlorobenzene 40.000 39.114 2.2 107 -0.06 14 1,2-Dichlorobenzene 40.000 40.168 -0.4 110 -0.06 15 Benzyl Alcohol 40.000 40.381 -1.0 110 -0.06 16 2,2'-oxybis(1-Chloropropane 40.000 36.593 8.5 99 -0.06 17 2-Methylphenol 40.000 41.613 -4.0 113 -0.06 18 Hexachloroethane 40.000 40.961 -2.4 111 -0.06 19 P n-Nitroso-di-n-propylamine 40.000 40.630 -1.6 108 -0.06 20 3+4-Methylphenols 40.000 40.833 -2.1 109 -0.05 21 I Naphthalene-d8 20.000 20.000 0.0 111 -0.06 22 Acetophenone 40.000 41.939 -4.8 118 -0.06 23 S Nitrobenzene-d5 80.000 81.686 -2.1 114 -0.06 24 Nitrobenzene 40.000 40.056 -0.1 108 -0.06 25 Isophorone 40.000 41.049 -2.6 107 -0.06 26 C 2-Nitrophenol 40.000 44.892 -12.2 125 -0.06 27 2,4-Dimethylphenol 40.000 43.458 -8.6 116 -0.06 28 bis(2-Chloroethoxy)methane 40.000 39.292 1.8 106 -0.05 29 C 2,4-Dichlorophenol 40.000 42.495 -6.2 109 -0.06 30 1,2,4-Trichlorobenzene 40.000 41.250 -3.1 114 -0.06 31 Naphthalene 40.000 40.682 -1.7 112 -0.06 32 Benzoic acid 40.000 43.123 -7.8 123 -0.03 33 4-Chloroaniline 40.000 43.339 -8.3 119 -0.05 34 C Hexachlorobutadiene 40.000 42.499 -6.2 113 -0.06 35 Caprolactam 40.000 46.510 -16.3 125 -0.05 36 C 4-Chloro-3-methylphenol 40.000 42.482 -6.2 108 -0.06 37 2-Methylnaphthalene 40.000 41.720 -4.3 114 -0.06 38 I Acenaphthene-d10 20.000 20.000 0.0 115 -0.06 39 1,2,4,5-Tetrachlorobenzene 40.000 41.253 -3.1 115 -0.06 40 P Hexachlorocyclopentadiene 40.000 39.778 0.6 115 -0.06 41 S 2,4,6-Tribromophenol 80.000 89.393 -11.7 132 -0.06 42 C 2,4,6-Trichlorophenol 40.000 40.002 -0.0 118 -0.06 43 2,4,5-Trichlorophenol 40.000 41.224 -3.1 113 -0.06 44 S 2-Fluorobiphenyl 80.000 77.813 2.7 113 -0.07 45 1,1'-Biphenyl 40.000 39.115 2.2 110 -0.06 46 2-Chloronaphthalene 40.000 40.099 -0.2 111 -0.06 47 2-Nitroaniline 40.000 43.166 -7.9 117 -0.06 48 Acenaphthylene 40.000 41.946 -4.9 116 -0.06 49 Dimethylphthalate 40.000 41.268 -3.2 114 -0.06 50 2,6-Dinitrotoluene 40.000 38.280 4.3 112 -0.06 51 C Acenaphthene 40.000 39.232 1.9 109 -0.06 52 3-Nitroaniline 40.000 39.992 0.0 121 -0.06 53 P 2,4-Dinitrophenol 40.000 50.647 -26.6# 177 -0.06 54 Dibenzofuran 40.000 39.502 1.2 113 -0.07 55 P 4-Nitrophenol 40.000 41.862 -4.7 115 -0.05 56 2,4-Dinitrotoluene 40.000 44.550 -11.4 126 -0.06 57 Fluorene 40.000 41.259 -3.1 118 -0.06 58 2,3,4,6-Tetrachlorophenol 40.000 43.511 -8.8 114 -0.06 59 Diethylphthalate 40.000 41.846 -4.6 118 -0.06 60 4-Chlorophenyl-phenylether 40.000 40.142 -0.4 117 -0.06 61 4-Nitroaniline 40.000 38.555 3.6 122 -0.06 62 Azobenzene 40.000 39.763 0.6 112 -0.07 63 I Phenanthrene-d10 20.000 20.000 0.0 114 -0.07 64 4,6-Dinitro-2-methylphenol 40.000 46.319 -15.8 144 -0.05 65 c n-Nitrosodiphenylamine 40.000 39.104 2.2 112 -0.07 66 4-Bromophenyl-phenylether 40.000 43.407 -8.5 126 -0.06 67 Hexachlorobenzene 40.000 43.763 -9.4 127 -0.06 68 Atrazine 40.000 43.443 -8.6 121 -0.07 69 C Pentachlorophenol 40.000 40.610 -1.5 123 -0.07 70 Phenanthrene 40.000 41.629 -4.1 118 -0.06 71 Anthracene 40.000 42.227 -5.6 121 -0.07 72 Carbazole 40.000 42.977 -7.4 121 -0.06 73 Di-n-butylphthalate 40.000 43.203 -8.0 125 -0.06 74 C Fluoranthene 40.000 42.880 -7.2 119 -0.07 75 I Chrysene-d12 20.000 20.000 0.0 120 -0.07 76 Benzidine 40.000 45.362 -13.4 130 -0.07 77 Pyrene 40.000 40.457 -1.1 122 -0.07 78 S Terphenyl-d14 80.000 87.207 -9.0 131 -0.06 79 Butylbenzylphthalate 40.000 43.226 -8.1 130 -0.07 80 Benzo(a)anthracene 40.000 43.561 -8.9 126 -0.07 81 3,3'-Dichlorobenzidine 40.000 48.804 -22.0 137 -0.06 82 Chrysene 40.000 40.174 -0.4 126 -0.06 83 Bis(2-ethylhexyl)phthalate 40.000 44.721 -11.8 133 -0.06 84 c Di-n-octyl phthalate 40.000 45.921 -14.8 143 -0.07 85 Indeno(1,2,3-cd)pyrene 40.000 43.584 -9.0 128 -0.10 86 I Perylene-d12 20.000 20.000 0.0 122 -0.07 87 Benzo(b)fluoranthene 40.000 42.637 -6.6 126 -0.07 88 Benzo(k)fluoranthene 40.000 40.669 -1.7 121 -0.07 89 C Benzo(a)pyrene 40.000 42.319 -5.8 124 -0.08 90 Dibenzo(a,h)anthracene 40.000 44.256 -10.6 129 -0.10 91 Benzo(g,h,i)perylene 40.000 42.131 -5.3 125 -0.10 -------------------------------------------------------------------------- (#) = Out of Range SPCC's out = 0 CCC's out = 0 8270-BF020714.M Thu Feb 13 10:43:27 2014