LSC Area Percent Report Data Path : W:\HPCHEM1\MSVOA_U\DATA\VU050118\ Data File : VU023551.D Acq On : 01 May 2018 13:44 Operator : MD/SY Sample : VU0501MBL01 Misc : 5.00g/5.0mL/100uL/5.0mL/MSVOA_U/MEOH ALS Vial : 8 Sample Multiplier: 1 Integration Parameters: LSCINT.P Integrator: RTE Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 0 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Method : W:\HPCHEM1\MSVOA_U\METHOD\SOMULM050118WMA.M Title : VOC Analysis Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total --- ----- ----- ---- ---- --- ------- ------- ------ ------- 1 0.677 25 27 34 rVV2 246 214 0.01% 0.002% 2 0.918 99 102 105 rBV 184 186 0.01% 0.001% 3 1.089 135 155 179 rBV 2176643 2462246 100.00% 19.370% 4 1.400 246 252 264 rBV 186255 189448 7.69% 1.490% 5 1.683 333 340 354 rVB 136400 169713 6.89% 1.335% 6 2.275 513 524 538 rBV 299862 455722 18.51% 3.585% 7 2.478 578 587 599 rVB2 5217 8455 0.34% 0.067% 8 2.616 625 630 642 rVB2 579 1071 0.04% 0.008% 9 2.706 650 658 666 rVB3 1963 3139 0.13% 0.025% 10 2.741 666 669 674 rBV2 197 214 0.01% 0.002% 11 2.825 693 695 697 rBV 514 328 0.01% 0.003% 12 2.841 697 700 707 rVB3 829 1097 0.04% 0.009% 13 2.889 712 715 716 rBV 286 184 0.01% 0.001% 14 2.982 739 744 756 rVB4 1879 2934 0.12% 0.023% 15 3.108 781 783 787 rVB2 316 203 0.01% 0.002% 16 3.127 787 789 791 rBV2 297 194 0.01% 0.002% 17 3.201 808 812 818 rBV2 243 232 0.01% 0.002% 18 3.471 891 896 901 rBV2 399 504 0.02% 0.004% 19 3.539 915 917 922 rBV2 153 172 0.01% 0.001% 20 3.915 1025 1034 1036 rBV2 181 275 0.01% 0.002% 21 3.941 1040 1042 1046 rVV2 281 185 0.01% 0.001% 22 3.989 1053 1057 1062 rVB2 242 251 0.01% 0.002% 23 4.108 1092 1094 1100 rVB2 202 218 0.01% 0.002% 24 4.175 1100 1115 1143 rBV 112780 297561 12.08% 2.341% 25 4.365 1170 1174 1177 rBV3 442 430 0.02% 0.003% 26 4.506 1214 1218 1223 rBV2 313 328 0.01% 0.003% 27 4.532 1223 1226 1229 rVB3 358 191 0.01% 0.002% 28 4.555 1229 1233 1235 rBV2 335 306 0.01% 0.002% 29 4.654 1242 1264 1291 rBV2 198196 513389 20.85% 4.039% 30 4.876 1331 1333 1336 rBV3 235 194 0.01% 0.002% 31 4.895 1336 1339 1346 rVB3 498 490 0.02% 0.004% 32 4.950 1353 1356 1360 rBV 361 258 0.01% 0.002% 33 4.992 1360 1369 1371 rBV3 525 568 0.02% 0.004% 34 5.085 1393 1398 1402 rVB2 210 232 0.01% 0.002% 35 5.137 1410 1414 1415 rBV 260 168 0.01% 0.001% 36 5.194 1429 1432 1436 rVB2 207 177 0.01% 0.001% 37 5.223 1436 1441 1447 rBV2 251 385 0.02% 0.003% 38 5.346 1454 1479 1514 rBV2 447206 1362567 55.34% 10.719% 39 5.539 1537 1539 1542 rVB2 322 197 0.01% 0.002% 40 5.674 1575 1581 1584 rVB4 343 400 0.02% 0.003% 41 5.744 1600 1603 1606 rBV3 308 241 0.01% 0.002% 42 5.799 1616 1620 1623 rBV 189 187 0.01% 0.001% 43 5.889 1634 1648 1688 rBV 372615 781331 31.73% 6.147% 44 6.108 1713 1716 1724 rVB 364 388 0.02% 0.003% 45 6.146 1724 1728 1732 rBV3 223 221 0.01% 0.002% 46 6.182 1735 1739 1740 rBV3 1354 918 0.04% 0.007% 47 6.227 1750 1753 1756 rBV4 406 258 0.01% 0.002% 48 6.336 1772 1787 1811 rBV 300141 612813 24.89% 4.821% 49 6.506 1838 1840 1844 rVB2 376 183 0.01% 0.001% 50 6.596 1859 1868 1870 rBV2 439 466 0.02% 0.004% 51 6.667 1888 1890 1894 rVB2 336 193 0.01% 0.002% 52 6.950 1973 1978 1982 rVV2 181 172 0.01% 0.001% 53 7.143 2034 2038 2039 rBV3 537 382 0.02% 0.003% 54 7.230 2053 2065 2092 rVV 166181 302674 12.29% 2.381% 55 7.571 2156 2171 2222 rBV 592678 1121302 45.54% 8.821% 56 7.802 2241 2243 2246 rVB2 409 222 0.01% 0.002% 57 7.854 2246 2259 2287 rBV 111850 199374 8.10% 1.568% 58 7.992 2300 2302 2305 rVV2 312 214 0.01% 0.002% 59 8.053 2319 2321 2328 rBV3 267 256 0.01% 0.002% 60 8.088 2328 2332 2334 rBV2 313 204 0.01% 0.002% 61 8.130 2342 2345 2348 rVB2 376 205 0.01% 0.002% 62 8.233 2371 2377 2382 rBV3 600 632 0.03% 0.005% 63 8.313 2390 2402 2435 rBV 353693 651462 26.46% 5.125% 64 8.596 2487 2490 2494 rBV3 315 265 0.01% 0.002% 65 8.751 2534 2538 2539 rBV2 287 191 0.01% 0.002% 66 8.792 2548 2551 2558 rBV2 218 228 0.01% 0.002% 67 8.857 2567 2571 2573 rVB2 289 234 0.01% 0.002% 68 8.873 2573 2576 2580 rVB 277 166 0.01% 0.001% 69 8.985 2606 2611 2613 rBV2 235 227 0.01% 0.002% 70 9.030 2619 2625 2631 rBV2 901 1071 0.04% 0.008% 71 9.095 2631 2645 2686 rVV 545235 954093 38.75% 7.506% 72 9.255 2693 2695 2702 rVB2 972 819 0.03% 0.006% 73 9.387 2727 2736 2743 rVB2 865 1382 0.06% 0.011% 74 9.419 2743 2746 2750 rBV 245 204 0.01% 0.002% 75 9.525 2776 2779 2782 rBV 205 168 0.01% 0.001% 76 9.763 2850 2853 2855 rBV 210 173 0.01% 0.001% 77 9.799 2860 2864 2866 rVB3 604 495 0.02% 0.004% 78 9.953 2908 2912 2915 rBV2 215 207 0.01% 0.002% 79 10.024 2931 2934 2936 rBV 277 176 0.01% 0.001% 80 10.169 2973 2979 2981 rBV3 542 550 0.02% 0.004% 81 10.265 3006 3009 3015 rBV2 252 246 0.01% 0.002% 82 10.435 3049 3062 3085 rVV 387526 620948 25.22% 4.885% 83 10.587 3106 3109 3113 rBV 366 241 0.01% 0.002% 84 10.754 3157 3161 3163 rBV 301 200 0.01% 0.002% 85 10.770 3163 3166 3172 rVV2 315 212 0.01% 0.002% 86 10.828 3181 3184 3190 rBV2 186 220 0.01% 0.002% 87 11.098 3266 3268 3272 rVB2 344 206 0.01% 0.002% 88 11.124 3272 3276 3278 rBV2 217 211 0.01% 0.002% 89 11.165 3286 3289 3292 rBV2 289 177 0.01% 0.001% 90 11.326 3333 3339 3344 rBV2 260 369 0.01% 0.003% 91 11.426 3362 3370 3377 rBV5 2350 3366 0.14% 0.026% 92 11.487 3377 3389 3416 rVB 580109 932915 37.89% 7.339% 93 11.863 3494 3506 3534 rBV 618255 1016351 41.28% 7.995% 94 12.898 3820 3828 3838 rVB3 3530 5227 0.21% 0.041% 95 13.091 3886 3888 3890 rBV2 296 172 0.01% 0.001% 96 13.323 3955 3960 3962 rBV2 409 388 0.02% 0.003% 97 13.512 4012 4019 4031 rBV5 3805 6509 0.26% 0.051% 98 13.574 4036 4038 4041 rBV 324 211 0.01% 0.002% 99 13.757 4088 4095 4108 rVB3 3044 5486 0.22% 0.043% 100 13.995 4162 4169 4179 rBV3 4965 7963 0.32% 0.063% Sum of corrected areas: 12711591