Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_U\DATA\VU050118\ Data File : VU023565.D Acq On : 01 May 2018 20:15 Operator : MD/SY Sample : J2621-06 Misc : 5.0mL/MSVOA_U/WATER ALS Vial : 22 Sample Multiplier: 1 Quant Time: May 02 04:10:14 2018 Quant Method : W:\HPCHEM1\MSVOA_U\METHOD\SOMULM050118WMA.M Quant Title : VOC Analysis QLast Update : Wed May 02 03:12:05 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) 1,4-Difluorobenzene 5.89 114 350010 50.00 ug/L 0.00 28) Chlorobenzene-d5 9.09 117 321841 50.00 ug/L 0.00 60) 1,4-Dichlorobenzene-d4 11.49 152 162216 50.00 ug/L 0.00 System Monitoring Compounds 4) Vinyl Chloride-d3 1.40 65 97569 39.33 ug/L 0.00 Spiked Amount 50.000 Range 60 - 135 Recovery = 78.66% 7) Chloroethane-d5 1.68 69 77296 40.88 ug/L 0.00 Spiked Amount 50.000 Range 70 - 130 Recovery = 81.76% 11) 1,1-Dichloroethene-d2 2.27 63 144738 29.93 ug/L 0.00 Spiked Amount 50.000 Range 60 - 125 Recovery = 59.86%# 21) 2-Butanone-d5 4.18 46 191027 111.46 ug/L 0.00 Spiked Amount 100.000 Range 40 - 130 Recovery = 111.46% 24) Chloroform-d 4.65 84 188282 45.89 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 91.78% 26) 1,2-Dichloroethane-d4 5.31 65 125634 44.03 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 88.06% 32) Benzene-d6 5.35 84 391895 45.38 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 90.76% 36) 1,2-Dichloropropane-d6 6.34 67 137931 47.69 ug/L 0.00 Spiked Amount 50.000 Range 70 - 120 Recovery = 95.38% 41) Toluene-d8 7.57 98 354267 44.50 ug/L 0.00 Spiked Amount 50.000 Range 80 - 120 Recovery = 89.00% 43) trans-1,3-Dichloropropene- 7.85 79 57291 46.01 ug/L 0.00 Spiked Amount 50.000 Range 60 - 125 Recovery = 92.02% 47) 2-Hexanone-d5 8.31 63 139257 126.79 ug/L 0.00 Spiked Amount 100.000 Range 45 - 130 Recovery = 126.79% 57) 1,1,2,2-Tetrachloroethane- 10.44 84 182526 48.79 ug/L 0.00 Spiked Amount 50.000 Range 65 - 120 Recovery = 97.58% 64) 1,2-Dichlorobenzene-d4 11.87 152 146753 46.37 ug/L 0.00 Spiked Amount 50.000 Range 80 - 120 Recovery = 92.74% Target Compounds Qvalue 13) Acetone 2.32 43 37893 14.88 ug/L 99 15) Methyl Acetate 2.62 43 18056 5.35 ug/L 99 16) Methylene chloride 2.70 84 399479 125.29 ug/L 99 20) cis-1,2-Dichloroethene 4.23 96 47846 15.42 ug/L 99 22) 2-Butanone 4.27 43 16542 5.84 ug/L 96 30) 1,1,1-Trichloroethane 4.92 97 52750 12.94 ug/L 100 34) Trichloroethene 6.19 95 454160 156.29 ug/L 99 42) Toluene 7.64 91 48210 4.10 ug/L 96 45) 1,1,2-Trichloroethane 8.08 97 7751 2.81 ug/L 95 52) Ethylbenzene 9.25 91 331781 26.04 ug/L 100 53) m,p-Xylene 9.38 106 568970 117.07 ug/L 99 54) o-xylene 9.78 106 268035 58.21 ug/L 98 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed