Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_U\DATA\VU050118\ Data File : VU023566.D Acq On : 01 May 2018 20:42 Operator : MD/SY Sample : J2621-07 Misc : 5.0mL/MSVOA_U/WATER ALS Vial : 23 Sample Multiplier: 1 Quant Time: May 02 04:12:46 2018 Quant Method : W:\HPCHEM1\MSVOA_U\METHOD\SOMULM050118WMA.M Quant Title : VOC Analysis QLast Update : Wed May 02 03:12:05 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) 1,4-Difluorobenzene 5.89 114 356990 50.00 ug/L 0.00 28) Chlorobenzene-d5 9.09 117 332466 50.00 ug/L 0.00 60) 1,4-Dichlorobenzene-d4 11.49 152 167269 50.00 ug/L 0.00 System Monitoring Compounds 4) Vinyl Chloride-d3 1.40 65 96952 38.32 ug/L 0.00 Spiked Amount 50.000 Range 60 - 135 Recovery = 76.64% 7) Chloroethane-d5 1.68 69 78478 40.69 ug/L 0.00 Spiked Amount 50.000 Range 70 - 130 Recovery = 81.38% 11) 1,1-Dichloroethene-d2 2.27 63 147791 29.96 ug/L 0.00 Spiked Amount 50.000 Range 60 - 125 Recovery = 59.92%# 21) 2-Butanone-d5 4.18 46 198005 113.27 ug/L 0.00 Spiked Amount 100.000 Range 40 - 130 Recovery = 113.27% 24) Chloroform-d 4.65 84 190742 45.59 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 91.18% 26) 1,2-Dichloroethane-d4 5.31 65 130068 44.70 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 89.40% 32) Benzene-d6 5.35 84 397868 44.60 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 89.20% 36) 1,2-Dichloropropane-d6 6.34 67 139782 46.78 ug/L 0.00 Spiked Amount 50.000 Range 70 - 120 Recovery = 93.56% 41) Toluene-d8 7.57 98 357563 43.48 ug/L 0.00 Spiked Amount 50.000 Range 80 - 120 Recovery = 86.96% 43) trans-1,3-Dichloropropene- 7.85 79 59293 46.10 ug/L 0.00 Spiked Amount 50.000 Range 60 - 125 Recovery = 92.20% 47) 2-Hexanone-d5 8.31 63 143841 126.77 ug/L 0.00 Spiked Amount 100.000 Range 45 - 130 Recovery = 126.77% 57) 1,1,2,2-Tetrachloroethane- 10.44 84 187944 48.63 ug/L 0.00 Spiked Amount 50.000 Range 65 - 120 Recovery = 97.26% 64) 1,2-Dichlorobenzene-d4 11.87 152 149030 45.67 ug/L 0.00 Spiked Amount 50.000 Range 80 - 120 Recovery = 91.34% Target Compounds Qvalue 13) Acetone 2.32 43 12757 4.91 ug/L 98 15) Methyl Acetate 2.62 43 17654 5.13 ug/L 99 16) Methylene chloride 2.70 84 344498 105.94 ug/L 100 20) cis-1,2-Dichloroethene 4.23 96 11260 3.56 ug/L 98 30) 1,1,1-Trichloroethane 4.92 97 863780 205.12 ug/L 99 34) Trichloroethene 6.19 95 4098308 1365.28 ug/L 97 40) 4-Methyl-2-pentanone 7.47 43 7611 1.86 ug/L 99 42) Toluene 7.64 91 49787 4.10 ug/L 100 45) 1,1,2-Trichloroethane 8.07 97 20054 7.03 ug/L 97 52) Ethylbenzene 9.26 91 389051 29.56 ug/L 100 53) m,p-Xylene 9.38 106 626040 124.70 ug/L 100 54) o-xylene 9.78 106 319499 67.17 ug/L 98 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed