LSC Area Percent Report Data Path : W:\HPCHEM1\MSVOA_U\DATA\VU050218\ Data File : VU023570.D Acq On : 02 May 2018 10:58 Operator : MD/SY Sample : VU0502MBL01 Misc : 5.00g/5.0mL/100uL/5.0mL/MSVOA_U/MEOH ALS Vial : 3 Sample Multiplier: 1 Integration Parameters: LSCINT.P Integrator: RTE Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 0 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Method : W:\HPCHEM1\MSVOA_U\METHOD\SOMULM050118WMA.M Title : VOC Analysis Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total --- ----- ----- ---- ---- --- ------- ------- ------ ------- 1 0.645 14 17 22 rBV2 118 117 0.01% 0.001% 2 0.876 84 89 91 rBV2 157 149 0.01% 0.001% 3 0.924 103 104 108 rVB 174 97 0.00% 0.001% 4 0.944 108 110 111 rBV 111 61 0.00% 0.001% 5 0.957 111 114 116 rVV 87 61 0.00% 0.001% 6 0.973 116 119 122 rVV 157 122 0.01% 0.001% 7 1.021 131 134 137 rBV2 99 73 0.00% 0.001% 8 1.088 137 155 179 rBV 2045875 2335357 100.00% 20.350% 9 1.400 246 252 262 rBV 148282 152424 6.53% 1.328% 10 1.680 333 339 356 rVB 112271 141637 6.06% 1.234% 11 2.275 513 524 536 rBV 253947 383610 16.43% 3.343% 12 2.481 583 588 597 rVB3 1671 2526 0.11% 0.022% 13 2.522 597 601 604 rBV2 239 238 0.01% 0.002% 14 2.574 615 617 621 rVB2 323 241 0.01% 0.002% 15 2.619 624 631 642 rVB2 668 1058 0.05% 0.009% 16 2.664 642 645 646 rBV 243 119 0.01% 0.001% 17 2.706 652 658 663 rVB3 959 1190 0.05% 0.010% 18 2.735 663 667 671 rBV2 152 127 0.01% 0.001% 19 2.802 685 688 689 rBV 162 99 0.00% 0.001% 20 2.834 690 698 700 rBV 1485 1692 0.07% 0.015% 21 2.892 714 716 718 rVB2 197 58 0.00% 0.001% 22 2.989 740 746 750 rVB4 580 725 0.03% 0.006% 23 3.140 791 793 796 rBV2 122 77 0.00% 0.001% 24 3.336 850 854 859 rBV2 178 180 0.01% 0.002% 25 3.387 867 870 874 rVB2 228 170 0.01% 0.001% 26 3.436 883 885 886 rBV 167 87 0.00% 0.001% 27 3.487 898 901 909 rBV2 144 168 0.01% 0.001% 28 3.548 917 920 922 rBV 185 99 0.00% 0.001% 29 3.670 956 958 961 rVB 140 69 0.00% 0.001% 30 3.696 963 966 968 rVB 159 93 0.00% 0.001% 31 3.854 1012 1015 1019 rVB 190 142 0.01% 0.001% 32 4.178 1100 1116 1146 rBV 111583 295468 12.65% 2.575% 33 4.651 1246 1263 1292 rBV 189905 444908 19.05% 3.877% 34 4.786 1304 1305 1310 rVB3 358 217 0.01% 0.002% 35 4.889 1331 1337 1347 rBV3 610 933 0.04% 0.008% 36 5.017 1374 1377 1379 rBV 94 64 0.00% 0.001% 37 5.181 1425 1428 1430 rBV 151 98 0.00% 0.001% 38 5.214 1435 1438 1442 rVB2 141 94 0.00% 0.001% 39 5.345 1454 1479 1517 rBV2 381621 1165248 49.90% 10.154% 40 5.644 1568 1572 1574 rBV3 317 308 0.01% 0.003% 41 5.757 1601 1607 1610 rBV2 400 464 0.02% 0.004% 42 5.837 1621 1632 1633 rBV2 2305 3168 0.14% 0.028% 43 5.889 1635 1648 1685 rVV 370207 765890 32.80% 6.674% 44 6.336 1771 1787 1808 rBV 261959 532805 22.81% 4.643% 45 6.522 1843 1845 1848 rVB2 238 114 0.00% 0.001% 46 6.558 1853 1856 1857 rBV 199 90 0.00% 0.001% 47 6.603 1866 1870 1873 rBV2 307 217 0.01% 0.002% 48 6.689 1895 1897 1900 rVB2 204 115 0.00% 0.001% 49 6.789 1924 1928 1933 rBV2 218 242 0.01% 0.002% 50 6.818 1933 1937 1942 rBV 167 151 0.01% 0.001% 51 6.857 1945 1949 1950 rBV2 367 240 0.01% 0.002% 52 6.998 1990 1993 1995 rBV 130 88 0.00% 0.001% 53 7.014 1995 1998 2003 rVV2 181 176 0.01% 0.002% 54 7.130 2031 2034 2036 rBV2 160 102 0.00% 0.001% 55 7.230 2053 2065 2100 rBV 139982 257570 11.03% 2.244% 56 7.390 2109 2115 2120 rVB2 597 666 0.03% 0.006% 57 7.413 2120 2122 2128 rBV2 400 350 0.01% 0.003% 58 7.570 2156 2171 2212 rBV 513845 923077 39.53% 8.044% 59 7.853 2247 2259 2277 rBV 99334 171388 7.34% 1.493% 60 8.021 2310 2311 2313 rBV 199 82 0.00% 0.001% 61 8.046 2317 2319 2322 rBV 167 97 0.00% 0.001% 62 8.066 2322 2325 2328 rBV2 240 122 0.01% 0.001% 63 8.162 2353 2355 2357 rBV 121 85 0.00% 0.001% 64 8.223 2370 2374 2376 rBV2 174 149 0.01% 0.001% 65 8.313 2390 2402 2439 rBV 369232 637073 27.28% 5.551% 66 8.500 2459 2460 2466 rVB3 319 223 0.01% 0.002% 67 8.558 2476 2478 2482 rVB 145 57 0.00% 0.000% 68 8.583 2483 2486 2488 rBV 181 126 0.01% 0.001% 69 8.625 2496 2499 2502 rBV3 371 307 0.01% 0.003% 70 8.731 2528 2532 2539 rBV2 493 769 0.03% 0.007% 71 9.095 2632 2645 2684 rBV 541104 916131 39.23% 7.983% 72 9.368 2728 2730 2731 rBV 245 89 0.00% 0.001% 73 9.448 2752 2755 2759 rVB2 196 139 0.01% 0.001% 74 9.869 2884 2886 2887 rBV 146 69 0.00% 0.001% 75 10.435 3050 3062 3085 rVB 361710 575033 24.62% 5.011% 76 10.516 3085 3087 3090 rBV 247 140 0.01% 0.001% 77 10.606 3111 3115 3116 rBV2 277 206 0.01% 0.002% 78 11.426 3363 3370 3376 rBV3 974 1392 0.06% 0.012% 79 11.487 3377 3389 3411 rBV 556719 881065 37.73% 7.678% 80 11.863 3494 3506 3526 rBV 535833 867231 37.13% 7.557% 81 12.294 3637 3640 3646 rBV 408 261 0.01% 0.002% 82 12.895 3821 3827 3837 rVB3 1520 2123 0.09% 0.018% 83 13.519 4013 4021 4032 rBV3 1653 2629 0.11% 0.023% 84 13.753 4091 4094 4095 rBV2 759 464 0.02% 0.004% 85 14.001 4164 4171 4181 rBV5 1759 2731 0.12% 0.024% Sum of corrected areas: 11475910