LSC Area Percent Report Data Path : W:\HPCHEM1\MSVOA_U\DATA\VU050218\ Data File : VU023592.D Acq On : 02 May 2018 21:24 Operator : MD/SY Sample : J2621-09 Misc : 5.0mL/MSVOA_U/WATER ALS Vial : 26 Sample Multiplier: 1 Integration Parameters: LSCINT.P Integrator: RTE Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 0 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Method : W:\HPCHEM1\MSVOA_U\METHOD\SOMULM050118WMA.M Title : VOC Analysis Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total --- ----- ----- ---- ---- --- ------- ------- ------ ------- 1 0.986 119 123 129 rVB2 212 245 0.02% 0.002% 2 1.089 148 155 175 rBV 343914 399507 33.38% 2.967% 3 1.182 181 184 191 rVB 8531 7530 0.63% 0.056% 4 1.285 208 216 230 rBV 53139 116759 9.76% 0.867% 5 1.397 245 251 261 rVB 133254 134851 11.27% 1.002% 6 1.680 331 339 352 rVB 102632 130628 10.91% 0.970% 7 2.272 512 523 533 rBV 215865 326765 27.30% 2.427% 8 2.323 533 539 564 rVB 30466 50866 4.25% 0.378% 9 2.455 571 580 581 rBV3 942 1188 0.10% 0.009% 10 2.561 610 613 617 rVB2 286 235 0.02% 0.002% 11 2.619 620 631 643 rVV 17210 30243 2.53% 0.225% 12 2.703 643 657 686 rVV 435364 795528 66.47% 5.909% 13 2.812 689 691 692 rVV 501 235 0.02% 0.002% 14 2.838 692 699 710 rVB4 2001 3853 0.32% 0.029% 15 3.185 793 807 825 rBV2 6523 15253 1.27% 0.113% 16 3.416 866 879 896 rBV7 3641 8721 0.73% 0.065% 17 3.995 1051 1059 1060 rBV2 328 300 0.03% 0.002% 18 4.121 1091 1098 1102 rBV2 568 720 0.06% 0.005% 19 4.182 1102 1117 1139 rBV 131766 351988 29.41% 2.614% 20 4.535 1223 1227 1230 rVB 256 230 0.02% 0.002% 21 4.580 1238 1241 1246 rVB 276 231 0.02% 0.002% 22 4.651 1246 1263 1293 rBV 187658 444177 37.11% 3.299% 23 4.921 1329 1347 1364 rBV2 39515 96605 8.07% 0.718% 24 5.346 1453 1479 1513 rBV2 391706 1192620 99.65% 8.858% 25 5.600 1553 1558 1560 rBV3 416 358 0.03% 0.003% 26 5.632 1566 1568 1572 rVB2 413 231 0.02% 0.002% 27 5.674 1578 1581 1585 rBV4 338 293 0.02% 0.002% 28 5.796 1603 1619 1620 rBV2 15155 30219 2.52% 0.224% 29 5.892 1637 1649 1687 rVB 398911 808523 67.56% 6.005% 30 6.191 1727 1742 1772 rVV 615964 1196805 100.00% 8.889% 31 6.336 1774 1787 1812 rVB 265171 526834 44.02% 3.913% 32 6.619 1867 1875 1891 rVB3 7824 15242 1.27% 0.113% 33 6.715 1901 1905 1907 rBV4 1062 923 0.08% 0.007% 34 6.854 1943 1948 1956 rBV3 759 1071 0.09% 0.008% 35 6.953 1974 1979 1983 rBV2 228 238 0.02% 0.002% 36 7.030 1996 2003 2008 rVB3 385 547 0.05% 0.004% 37 7.137 2033 2036 2040 rBV 302 237 0.02% 0.002% 38 7.233 2053 2066 2088 rBV 136116 247776 20.70% 1.840% 39 7.468 2129 2139 2149 rBV2 12200 20707 1.73% 0.154% 40 7.571 2157 2171 2186 rBV 495064 860564 71.91% 6.392% 41 7.854 2247 2259 2281 rBV 95252 166261 13.89% 1.235% 42 8.034 2310 2315 2317 rBV3 426 323 0.03% 0.002% 43 8.075 2317 2328 2344 rVB2 19309 33030 2.76% 0.245% 44 8.165 2347 2356 2357 rBV4 1480 1453 0.12% 0.011% 45 8.236 2374 2378 2384 rBV4 624 728 0.06% 0.005% 46 8.313 2390 2402 2432 rBV 460199 783086 65.43% 5.816% 47 8.577 2481 2484 2489 rVB3 322 252 0.02% 0.002% 48 8.622 2489 2498 2508 rVB5 838 1556 0.13% 0.012% 49 8.780 2540 2547 2551 rVB3 305 383 0.03% 0.003% 50 8.847 2558 2568 2575 rBV3 1978 3023 0.25% 0.022% 51 9.095 2632 2645 2672 rBV 579583 964201 80.56% 7.162% 52 9.214 2673 2682 2687 rVV2 29933 48220 4.03% 0.358% 53 9.255 2688 2695 2711 rVV 76955 120420 10.06% 0.894% 54 9.378 2721 2733 2746 rVV 328166 530444 44.32% 3.940% 55 9.448 2747 2755 2773 rVB 39930 69192 5.78% 0.514% 56 9.574 2789 2794 2795 rBV3 285 253 0.02% 0.002% 57 9.661 2818 2821 2825 rVB2 366 287 0.02% 0.002% 58 9.783 2847 2859 2875 rBV 198231 315923 26.40% 2.347% 59 9.969 2912 2917 2920 rBV3 627 712 0.06% 0.005% 60 10.146 2967 2972 2973 rBV4 1038 903 0.08% 0.007% 61 10.175 2976 2981 2990 rVB3 2538 3313 0.28% 0.025% 62 10.226 2991 2997 3007 rVB6 1778 2921 0.24% 0.022% 63 10.284 3007 3015 3025 rVB4 1057 1786 0.15% 0.013% 64 10.435 3043 3062 3077 rBV 394590 629584 52.61% 4.676% 65 10.496 3077 3081 3092 rVB6 3493 4873 0.41% 0.036% 66 10.583 3100 3108 3117 rBV4 5003 8461 0.71% 0.063% 67 10.686 3134 3140 3145 rBV3 1635 2028 0.17% 0.015% 68 10.738 3151 3156 3165 rBV4 680 844 0.07% 0.006% 69 10.834 3179 3186 3193 rVB4 2098 2941 0.25% 0.022% 70 10.972 3226 3229 3231 rBV2 387 307 0.03% 0.002% 71 11.085 3260 3264 3265 rBV2 586 416 0.03% 0.003% 72 11.152 3278 3285 3293 rBV3 2488 3211 0.27% 0.024% 73 11.201 3293 3300 3312 rVB3 4537 6651 0.56% 0.049% 74 11.259 3314 3318 3320 rBV2 468 341 0.03% 0.003% 75 11.326 3333 3339 3345 rVB4 945 1127 0.09% 0.008% 76 11.426 3366 3370 3375 rBV3 512 471 0.04% 0.003% 77 11.490 3378 3390 3411 rBV 600123 944749 78.94% 7.017% 78 11.596 3417 3423 3430 rVB6 3159 3759 0.31% 0.028% 79 11.683 3446 3450 3453 rBV2 271 262 0.02% 0.002% 80 11.750 3461 3471 3489 rBV3 28865 55371 4.63% 0.411% 81 11.866 3494 3507 3524 rVV 532866 859787 71.84% 6.386% 82 12.017 3551 3554 3557 rBV2 517 315 0.03% 0.002% 83 12.133 3586 3590 3591 rBV 447 262 0.02% 0.002% 84 12.217 3611 3616 3619 rBV3 1400 1471 0.12% 0.011% 85 12.471 3688 3695 3696 rBV3 1157 1323 0.11% 0.010% 86 12.574 3720 3727 3738 rBV4 6593 10543 0.88% 0.078% 87 12.619 3739 3741 3749 rVB4 2261 2225 0.19% 0.017% 88 12.844 3805 3811 3820 rVB6 1406 1642 0.14% 0.012% 89 12.902 3820 3829 3837 rBV3 13800 21115 1.76% 0.157% 90 13.037 3866 3871 3877 rBV3 456 542 0.05% 0.004% 91 13.062 3877 3879 3882 rBV2 420 319 0.03% 0.002% 92 13.188 3911 3918 3928 rBV4 5167 6585 0.55% 0.049% 93 13.377 3970 3977 3991 rBV6 9664 15868 1.33% 0.118% 94 13.471 4004 4006 4009 rBV2 292 217 0.02% 0.002% 95 13.512 4017 4019 4020 rBV 511 235 0.02% 0.002% 96 13.680 4067 4071 4075 rBV3 689 685 0.06% 0.005% 97 13.754 4086 4094 4102 rBV5 936 1721 0.14% 0.013% 98 13.799 4104 4108 4109 rBV3 793 528 0.04% 0.004% 99 14.017 4174 4176 4178 rBV 365 231 0.02% 0.002% 100 14.654 4367 4374 4383 rVB4 3002 3977 0.33% 0.030% Sum of corrected areas: 13463503