LSC Area Percent Report Data Path : W:\HPCHEM1\MSVOA_U\DATA\VU050618\ Data File : VU023683.D Acq On : 06 May 2018 11:26 Operator : MD/SY Sample : VU0506MBL01 Misc : 5.00g/5.0mL/100ul/5.0mL/MSVOA_U/MEOH ALS Vial : 3 Sample Multiplier: 1 Integration Parameters: LSCINT.P Integrator: RTE Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 0 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Method : W:\HPCHEM1\MSVOA_U\METHOD\SOMULM050118WMA.M Title : VOC Analysis Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total --- ----- ----- ---- ---- --- ------- ------- ------ ------- 1 0.815 67 70 74 rVB2 124 111 0.01% 0.001% 2 0.863 79 85 88 rVV2 133 159 0.01% 0.001% 3 1.005 127 129 136 rVB 110 93 0.01% 0.001% 4 1.089 136 155 175 rBV 1358165 1520957 100.00% 14.245% 5 1.182 181 184 190 rVB 6317 5401 0.36% 0.051% 6 1.400 245 252 262 rBV 162476 168241 11.06% 1.576% 7 1.680 331 339 359 rVB 123238 154891 10.18% 1.451% 8 2.272 512 523 537 rBV 273597 417530 27.45% 3.910% 9 2.478 583 587 597 rVB3 2096 3008 0.20% 0.028% 10 2.519 597 600 603 rVB2 311 202 0.01% 0.002% 11 2.539 603 606 610 rBV3 287 321 0.02% 0.003% 12 2.616 625 630 633 rBV2 555 597 0.04% 0.006% 13 2.677 646 649 651 rVB2 207 120 0.01% 0.001% 14 2.696 651 655 656 rBV2 882 558 0.04% 0.005% 15 2.777 676 680 683 rBV2 173 141 0.01% 0.001% 16 2.841 690 700 710 rBV 1407 2771 0.18% 0.026% 17 2.937 727 730 735 rVB2 165 133 0.01% 0.001% 18 2.995 739 748 751 rVV5 568 800 0.05% 0.007% 19 3.043 761 763 765 rBV2 125 74 0.00% 0.001% 20 3.117 782 786 787 rBV 185 81 0.01% 0.001% 21 3.172 801 803 806 rBV2 144 85 0.01% 0.001% 22 3.285 835 838 843 rBV2 180 140 0.01% 0.001% 23 3.474 893 897 900 rBV 154 129 0.01% 0.001% 24 3.561 921 924 928 rBV2 125 111 0.01% 0.001% 25 3.619 938 942 946 rVB2 131 107 0.01% 0.001% 26 3.728 972 976 979 rBV2 240 207 0.01% 0.002% 27 3.822 1000 1005 1009 rBV2 141 176 0.01% 0.002% 28 3.876 1019 1022 1023 rBV 162 114 0.01% 0.001% 29 4.043 1070 1074 1076 rBV2 517 405 0.03% 0.004% 30 4.175 1099 1115 1144 rBV 104485 278681 18.32% 2.610% 31 4.371 1173 1176 1184 rBV5 437 491 0.03% 0.005% 32 4.407 1185 1187 1192 rVB3 411 253 0.02% 0.002% 33 4.529 1222 1225 1229 rVB3 193 152 0.01% 0.001% 34 4.564 1233 1236 1239 rVB 253 177 0.01% 0.002% 35 4.590 1239 1244 1246 rBV2 247 200 0.01% 0.002% 36 4.651 1246 1263 1290 rBV 192544 460519 30.28% 4.313% 37 4.879 1330 1334 1345 rVB4 521 949 0.06% 0.009% 38 4.979 1362 1365 1375 rVB 318 447 0.03% 0.004% 39 5.027 1377 1380 1382 rBV2 149 91 0.01% 0.001% 40 5.075 1392 1395 1396 rBV 127 74 0.00% 0.001% 41 5.114 1402 1407 1413 rVB2 161 203 0.01% 0.002% 42 5.153 1417 1419 1423 rVB 136 75 0.00% 0.001% 43 5.342 1454 1478 1521 rBV2 395488 1190343 78.26% 11.148% 44 5.538 1535 1539 1543 rVB2 541 439 0.03% 0.004% 45 5.619 1561 1564 1567 rBV2 176 124 0.01% 0.001% 46 5.661 1575 1577 1590 rVB3 394 434 0.03% 0.004% 47 5.719 1592 1595 1601 rVB2 167 163 0.01% 0.002% 48 5.751 1601 1605 1607 rBV 274 269 0.02% 0.003% 49 5.889 1633 1648 1672 rBV 365217 734864 48.32% 6.882% 50 6.165 1730 1734 1735 rBV3 747 439 0.03% 0.004% 51 6.188 1735 1741 1755 rVB8 1629 3201 0.21% 0.030% 52 6.333 1771 1786 1818 rBV 265439 547496 36.00% 5.128% 53 6.583 1859 1864 1867 rBV2 153 140 0.01% 0.001% 54 6.606 1867 1871 1873 rBV2 120 95 0.01% 0.001% 55 6.664 1886 1889 1891 rBV 117 82 0.01% 0.001% 56 6.741 1909 1913 1916 rBV2 188 215 0.01% 0.002% 57 6.805 1930 1933 1937 rBV2 122 94 0.01% 0.001% 58 6.854 1945 1948 1949 rBV 222 122 0.01% 0.001% 59 6.940 1971 1975 1979 rBV 146 122 0.01% 0.001% 60 6.960 1979 1981 1984 rVV2 136 82 0.01% 0.001% 61 6.989 1984 1990 2001 rVV2 167 293 0.02% 0.003% 62 7.037 2001 2005 2013 rVB2 168 218 0.01% 0.002% 63 7.075 2014 2017 2022 rBV 142 144 0.01% 0.001% 64 7.124 2025 2032 2034 rBV2 210 250 0.02% 0.002% 65 7.230 2052 2065 2086 rBV 135554 248020 16.31% 2.323% 66 7.394 2114 2116 2119 rVB3 341 193 0.01% 0.002% 67 7.458 2130 2136 2138 rBV 333 261 0.02% 0.002% 68 7.471 2138 2140 2143 rVB2 291 139 0.01% 0.001% 69 7.571 2156 2171 2223 rBV 510196 935537 61.51% 8.762% 70 7.854 2248 2259 2282 rBV 93877 164914 10.84% 1.545% 71 8.185 2355 2362 2371 rVB2 321 531 0.03% 0.005% 72 8.313 2389 2402 2441 rBV 334739 598639 39.36% 5.607% 73 8.574 2480 2483 2487 rVB2 311 200 0.01% 0.002% 74 8.593 2487 2489 2491 rBV2 143 84 0.01% 0.001% 75 8.612 2493 2495 2498 rBV2 191 147 0.01% 0.001% 76 8.628 2498 2500 2503 rBV2 316 218 0.01% 0.002% 77 8.757 2537 2540 2543 rBV2 223 126 0.01% 0.001% 78 8.847 2564 2568 2570 rBV 358 370 0.02% 0.003% 79 9.095 2632 2645 2685 rBV 536126 921456 60.58% 8.630% 80 9.259 2693 2696 2700 rBV2 307 257 0.02% 0.002% 81 9.336 2717 2720 2722 rBV 363 175 0.01% 0.002% 82 9.384 2729 2735 2742 rVB2 422 558 0.04% 0.005% 83 9.471 2758 2762 2765 rBV 158 114 0.01% 0.001% 84 9.490 2766 2768 2771 rBV 133 90 0.01% 0.001% 85 9.799 2862 2864 2870 rVB3 550 491 0.03% 0.005% 86 9.824 2870 2872 2875 rBV2 182 133 0.01% 0.001% 87 10.181 2981 2983 2987 rVB2 306 156 0.01% 0.001% 88 10.435 3049 3062 3084 rVB 356127 570888 37.53% 5.347% 89 10.519 3086 3088 3090 rBV 227 90 0.01% 0.001% 90 10.773 3164 3167 3169 rBV 197 139 0.01% 0.001% 91 11.278 3320 3324 3330 rBV 264 311 0.02% 0.003% 92 11.422 3365 3369 3377 rVB4 1086 1318 0.09% 0.012% 93 11.487 3377 3389 3416 rBV 532925 854552 56.19% 8.003% 94 11.722 3460 3462 3467 rVB3 411 231 0.02% 0.002% 95 11.863 3493 3506 3524 rBV 535430 869580 57.17% 8.144% 96 12.895 3821 3827 3835 rVB4 1728 2394 0.16% 0.022% 97 13.438 3993 3996 4000 rBV 333 308 0.02% 0.003% 98 13.519 4013 4021 4029 rVB3 1812 2592 0.17% 0.024% 99 13.914 4141 4144 4146 rBV2 272 180 0.01% 0.002% 100 13.998 4165 4170 4178 rVB4 2023 2331 0.15% 0.022% Sum of corrected areas: 10677327