Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_U\DATA\VU050618\ Data File : VU023685.D Acq On : 06 May 2018 12:22 Operator : MD/SY Sample : J2721-01 Misc : 6.42g/5.0mL/100ul/5.0mL/MSVOA_U/MEOH ALS Vial : 5 Sample Multiplier: 1 Quant Time: May 07 09:29:21 2018 Quant Method : W:\HPCHEM1\MSVOA_U\METHOD\SOMULM050118WMA.M Quant Title : VOC Analysis QLast Update : Mon May 07 00:51:10 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) 1,4-Difluorobenzene 5.89 114 297376 50.00 ug/L 0.00 28) Chlorobenzene-d5 9.10 117 300397 50.00 ug/L 0.00 60) 1,4-Dichlorobenzene-d4 11.49 152 171508 50.00 ug/L 0.00 System Monitoring Compounds 4) Vinyl Chloride-d3 1.39 65 122941 58.33 ug/L 0.00 Spiked Amount 50.000 Range 60 - 135 Recovery = 116.66% 7) Chloroethane-d5 1.64 69 64650 40.24 ug/L -0.04 Spiked Amount 50.000 Range 70 - 130 Recovery = 80.48% 11) 1,1-Dichloroethene-d2 2.24 63 166079 40.42 ug/L -0.04 Spiked Amount 50.000 Range 60 - 125 Recovery = 80.84% 21) 2-Butanone-d5 4.19 46 204856 140.68 ug/L 0.02 Spiked Amount 100.000 Range 40 - 130 Recovery = 140.68%# 24) Chloroform-d 4.65 84 211117 60.57 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 121.14% 26) 1,2-Dichloroethane-d4 5.31 65 150923 62.26 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 124.52% 32) Benzene-d6 5.34 84 485214 60.20 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 120.40% 36) 1,2-Dichloropropane-d6 6.33 67 162817 60.31 ug/L 0.00 Spiked Amount 50.000 Range 70 - 120 Recovery = 120.62%# 41) Toluene-d8 7.57 98 492156 66.23 ug/L 0.00 Spiked Amount 50.000 Range 80 - 120 Recovery = 132.46%# 43) trans-1,3-Dichloropropene- 7.86 79 71206 61.27 ug/L 0.00 Spiked Amount 50.000 Range 60 - 125 Recovery = 122.54% 47) 2-Hexanone-d5 8.33 63 177629 173.27 ug/L 0.02 Spiked Amount 100.000 Range 45 - 130 Recovery = 173.27%# 57) 1,1,2,2-Tetrachloroethane- 10.44 84 245062 70.18 ug/L 0.00 Spiked Amount 50.000 Range 65 - 120 Recovery = 140.36%# 64) 1,2-Dichlorobenzene-d4 11.87 152 213128 63.70 ug/L 0.00 Spiked Amount 50.000 Range 80 - 120 Recovery = 127.40%# Target Compounds Qvalue 29) Cyclohexane 4.98 56 179726 40.48 ug/L # 77 35) Methylcyclohexane 6.41 83 1365906 321.98 ug/L 97 42) Toluene 7.64 91 18765509m 1710.35 ug/L 46) Tetrachloroethene 8.23 164 7211 3.26 ug/L 94 52) Ethylbenzene 9.25 91 24017817m 2019.46 ug/L 53) m,p-Xylene 9.39 106 23664220m 5216.67 ug/L 54) o-xylene 9.80 106 11459688m 2666.40 ug/L 56) Isopropylbenzene 10.17 105 801531 71.06 ug/L 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed