LSC Area Percent Report Data Path : W:\HPCHEM1\MSVOA_U\Data\VU050618\ Data File : VU023685.D Acq On : 06 May 2018 12:22 Operator : MD/SY Sample : J2721-01 Misc : 6.42g/5.0mL/100ul/5.0mL/MSVOA_U/MEOH ALS Vial : 5 Sample Multiplier: 1 Integration Parameters: LSCINT.P Integrator: RTE Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 0 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Method : W:\HPCHEM1\MSVOA_U\METHOD\SOMULM050118WMA.M Title : VOC Analysis Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total --- ----- ----- ---- ---- --- ------- ------- ------ ------- 1 1.082 134 153 176 rBV 1182424 1337714 0.83% 0.159% 2 3.278 819 836 862 rVV 267736 567438 0.35% 0.068% 3 4.648 1244 1262 1279 rBV 200238 534027 0.33% 0.064% 4 4.979 1344 1365 1381 rVV3 561553 1355493 0.85% 0.161% 5 5.210 1417 1437 1457 rBV 566397 1401168 0.87% 0.167% 6 5.336 1457 1476 1500 rVB2 496494 1421454 0.89% 0.169% 7 5.474 1503 1519 1531 rVV3 210343 486696 0.30% 0.058% 8 5.615 1552 1563 1589 rVB 321175 728561 0.45% 0.087% 9 5.776 1594 1613 1634 rBV 3063385 5955395 3.72% 0.708% 10 5.886 1634 1647 1676 rVB 324932 692552 0.43% 0.082% 11 6.332 1775 1786 1794 rVV 293723 602325 0.38% 0.072% 12 6.413 1795 1811 1823 rVV 3155141 6927141 4.32% 0.824% 13 6.471 1823 1829 1838 rVV 258290 471188 0.29% 0.056% 14 6.529 1838 1847 1860 rVB2 337937 652095 0.41% 0.078% 15 6.734 1894 1911 1929 rVB2 451272 987950 0.62% 0.118% 16 6.902 1948 1963 1986 rVB3 443247 916103 0.57% 0.109% 17 7.104 2015 2026 2034 rBV 288502 532743 0.33% 0.063% 18 7.178 2034 2049 2057 rBV 1844435 3348043 2.09% 0.398% 19 7.220 2058 2062 2080 rVB4 622182 1095096 0.68% 0.130% 20 7.342 2090 2100 2120 rVB 1230692 2547256 1.59% 0.303% 21 7.529 2143 2158 2165 rBV2 1584790 3129978 1.95% 0.372% 22 7.648 2180 2195 2208 rBV2 26986859 49966790 31.18% 5.944% 23 7.824 2239 2250 2269 rVB 6413254 10375128 6.47% 1.234% 24 7.921 2269 2280 2295 rVB2 873458 1616636 1.01% 0.192% 25 8.049 2303 2320 2331 rBV 407151 744652 0.46% 0.089% 26 8.230 2365 2376 2388 rVB 356738 601799 0.38% 0.072% 27 8.332 2389 2408 2431 rBV 1115949 2198864 1.37% 0.262% 28 8.458 2433 2447 2451 rBV 598174 1003973 0.63% 0.119% 29 8.548 2465 2475 2485 rVB 1111980 1928328 1.20% 0.229% 30 8.609 2485 2494 2503 rBV2 539286 923230 0.58% 0.110% 31 8.818 2549 2559 2565 rVV 509047 881105 0.55% 0.105% 32 8.866 2565 2574 2580 rVV6 495351 1197433 0.75% 0.142% 33 8.914 2580 2589 2602 rVB2 2247572 3860434 2.41% 0.459% 34 9.037 2615 2627 2637 rBV 1710061 2852593 1.78% 0.339% 35 9.101 2637 2647 2658 rVB 460760 823323 0.51% 0.098% 36 9.268 2682 2699 2720 rBV2 44103552 87244106 54.45% 10.378% 37 9.406 2721 2742 2751 rVV3 69616462 160235713 100.00% 19.061% 38 9.451 2751 2756 2783 rVB2 3725644 5640144 3.52% 0.671% 39 9.725 2828 2841 2849 rBV3 666595 1229142 0.77% 0.146% 40 9.795 2849 2863 2883 rVB2 38281552 67566015 42.17% 8.038% 41 9.956 2895 2913 2923 rBV3 961134 1879236 1.17% 0.224% 42 10.049 2934 2942 2950 rVV 879617 1629440 1.02% 0.194% 43 10.094 2951 2956 2967 rVB 532922 820661 0.51% 0.098% 44 10.172 2968 2980 2990 rBV 1272656 2148129 1.34% 0.256% 45 10.262 3001 3008 3016 rVV2 439285 790235 0.49% 0.094% 46 10.326 3016 3028 3033 rVV2 703459 1379905 0.86% 0.164% 47 10.358 3033 3038 3053 rVB 774597 1298436 0.81% 0.154% 48 10.455 3053 3068 3076 rBV2 949422 2239394 1.40% 0.266% 49 10.496 3077 3081 3090 rVB5 449849 612392 0.38% 0.073% 50 10.596 3101 3112 3121 rBV 1642295 2590421 1.62% 0.308% 51 10.689 3131 3141 3156 rBV 4604941 9935039 6.20% 1.182% 52 10.779 3156 3169 3175 rVV2 2785445 5077535 3.17% 0.604% 53 10.821 3175 3182 3193 rVB 5159627 7383197 4.61% 0.878% 54 10.979 3221 3231 3239 rBV 1994951 3153038 1.97% 0.375% 55 11.120 3267 3275 3278 rVV 1217335 1573767 0.98% 0.187% 56 11.155 3278 3286 3298 rVB 10654588 16171915 10.09% 1.924% 57 11.297 3313 3330 3335 rBV2 599546 1601126 1.00% 0.190% 58 11.336 3336 3342 3353 rVV2 939794 1890496 1.18% 0.225% 59 11.403 3354 3363 3367 rVV3 949347 1585921 0.99% 0.189% 60 11.435 3368 3373 3381 rVV 1175870 1939477 1.21% 0.231% 61 11.487 3382 3389 3397 rVV3 1279792 2183308 1.36% 0.260% 62 11.535 3398 3404 3409 rVV2 857667 1362110 0.85% 0.162% 63 11.580 3409 3418 3425 rVV 6042903 9457886 5.90% 1.125% 64 11.615 3426 3429 3440 rVV 1064594 1498645 0.94% 0.178% 65 11.673 3441 3447 3450 rVV2 336445 468611 0.29% 0.056% 66 11.709 3451 3458 3468 rVV2 1036557 1650218 1.03% 0.196% 67 11.786 3468 3482 3485 rVV3 3779752 7072003 4.41% 0.841% 68 11.818 3486 3492 3500 rVV 8750474 13221561 8.25% 1.573% 69 11.882 3500 3512 3528 rVB4 14460838 30953786 19.32% 3.682% 70 11.988 3536 3545 3551 rBV 910996 1433688 0.89% 0.171% 71 12.033 3551 3559 3563 rVV 4399178 6050255 3.78% 0.720% 72 12.062 3564 3568 3586 rVB 4857862 6963962 4.35% 0.828% 73 12.155 3586 3597 3602 rBV 8993563 14582207 9.10% 1.735% 74 12.188 3602 3607 3616 rVB 10422868 14322145 8.94% 1.704% 75 12.262 3617 3630 3640 rBV 18166752 27922952 17.43% 3.322% 76 12.393 3653 3671 3691 rBV6 3608597 13202665 8.24% 1.571% 77 12.499 3691 3704 3713 rBV4 1662052 3443507 2.15% 0.410% 78 12.561 3713 3723 3733 rVB 6050551 9571929 5.97% 1.139% 79 12.660 3733 3754 3762 rBV 14536942 25133966 15.69% 2.990% 80 12.715 3762 3771 3786 rVB 21177918 31958120 19.94% 3.802% 81 12.792 3786 3795 3801 rBV 3497929 5203931 3.25% 0.619% 82 12.827 3801 3806 3811 rVV 2388621 3282503 2.05% 0.390% 83 12.860 3811 3816 3823 rVB 3093661 3859079 2.41% 0.459% 84 12.972 3841 3851 3862 rVB2 9730203 14836494 9.26% 1.765% 85 13.040 3863 3872 3879 rBV2 2779939 3994029 2.49% 0.475% 86 13.094 3879 3889 3892 rVV3 3649960 5599703 3.49% 0.666% 87 13.133 3893 3901 3927 rVB3 18310956 35448104 22.12% 4.217% 88 13.242 3927 3935 3944 rBV 3667840 5251072 3.28% 0.625% 89 13.297 3945 3952 3960 rVB3 833372 1271898 0.79% 0.151% 90 13.413 3979 3988 3996 rBV2 982708 1616331 1.01% 0.192% 91 13.461 3997 4003 4010 rVB 490105 630932 0.39% 0.075% 92 13.515 4010 4020 4026 rBV3 4449291 7513354 4.69% 0.894% 93 13.644 4046 4060 4070 rVB2 2000814 3499316 2.18% 0.416% 94 13.750 4082 4093 4103 rVV 11621008 18279334 11.41% 2.174% 95 13.792 4103 4106 4116 rVB 462668 567228 0.35% 0.067% 96 13.969 4149 4161 4170 rBV5 547654 1233223 0.77% 0.147% 97 14.152 4208 4218 4233 rBV2 735863 1398847 0.87% 0.166% 98 14.342 4266 4277 4291 rBV4 392071 884098 0.55% 0.105% 99 14.480 4312 4320 4330 rBV 304452 486115 0.30% 0.058% 100 14.879 4434 4444 4457 rBV 611150 1040009 0.65% 0.124% Sum of corrected areas: 840628708