Quantitation Report (LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_U\DATA\VU050618\ Data File : VU023686.D Acq On : 06 May 2018 12:49 Operator : MD/SY Sample : J2721-18 Misc : 3.72g/5.0mL/100ul/5.0mL/MSVOA_U/MEOH ALS Vial : 6 Sample Multiplier: 1 Quant Time: May 07 01:17:06 2018 Quant Method : W:\HPCHEM1\MSVOA_U\METHOD\SOMULM050118WMA.M Quant Title : VOC Analysis QLast Update : Mon May 07 00:51:10 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) 1,4-Difluorobenzene 5.89 114 376392 50.00 ug/L 0.00 28) Chlorobenzene-d5 9.10 117 391594 50.00 ug/L 0.00 60) 1,4-Dichlorobenzene-d4 11.49 152 213353 50.00 ug/L 0.00 System Monitoring Compounds 4) Vinyl Chloride-d3 1.39 65 102391 38.38 ug/L 0.00 Spiked Amount 50.000 Range 60 - 135 Recovery = 76.76% 7) Chloroethane-d5 1.64 69 52203 25.67 ug/L -0.04 Spiked Amount 50.000 Range 70 - 130 Recovery = 51.34%# 11) 1,1-Dichloroethene-d2 2.24 63 137101 26.36 ug/L -0.04 Spiked Amount 50.000 Range 60 - 125 Recovery = 52.72%# 21) 2-Butanone-d5 4.19 46 174944 94.92 ug/L 0.02 Spiked Amount 100.000 Range 40 - 130 Recovery = 94.92% 24) Chloroform-d 4.65 84 177993 40.35 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 80.70% 26) 1,2-Dichloroethane-d4 5.31 65 125066 40.76 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 81.52% 32) Benzene-d6 5.34 84 399714 38.04 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 76.08% 36) 1,2-Dichloropropane-d6 6.33 67 135035 38.37 ug/L 0.00 Spiked Amount 50.000 Range 70 - 120 Recovery = 76.74% 41) Toluene-d8 7.57 98 388961 40.16 ug/L 0.00 Spiked Amount 50.000 Range 80 - 120 Recovery = 80.32% 43) trans-1,3-Dichloropropene- 7.86 79 57917 38.23 ug/L 0.00 Spiked Amount 50.000 Range 60 - 125 Recovery = 76.46% 47) 2-Hexanone-d5 8.33 63 138322 103.50 ug/L 0.02 Spiked Amount 100.000 Range 45 - 130 Recovery = 103.50% 57) 1,1,2,2-Tetrachloroethane- 10.44 84 195961 43.05 ug/L 0.00 Spiked Amount 50.000 Range 65 - 120 Recovery = 86.10% 64) 1,2-Dichlorobenzene-d4 11.87 152 172614 41.47 ug/L 0.00 Spiked Amount 50.000 Range 80 - 120 Recovery = 82.94% Target Compounds Qvalue 35) Methylcyclohexane 6.41 83 34849 6.30 ug/L 98 42) Toluene 7.64 91 1333352 93.22 ug/L 99 46) Tetrachloroethene 8.23 164 15479 5.37 ug/L 98 52) Ethylbenzene 9.26 91 2501983 161.38 ug/L 99 53) m,p-Xylene 9.38 106 4817552 814.68 ug/L 96 54) o-xylene 9.79 106 1882459 336.00 ug/L 99 56) Isopropylbenzene 10.17 105 136184 9.26 ug/L 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed