LSC Area Percent Report Data Path : W:\HPCHEM1\MSVOA_U\DATA\VU050618\ Data File : VU023686.D Acq On : 06 May 2018 12:49 Operator : MD/SY Sample : J2721-18 Misc : 3.72g/5.0mL/100ul/5.0mL/MSVOA_U/MEOH ALS Vial : 6 Sample Multiplier: 1 Integration Parameters: LSCINT.P Integrator: RTE Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 0 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Method : W:\HPCHEM1\MSVOA_U\METHOD\SOMULM050118WMA.M Title : VOC Analysis Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total --- ----- ----- ---- ---- --- ------- ------- ------ ------- 1 1.082 135 153 175 rBV 1114820 1256472 4.48% 0.463% 2 1.268 206 211 236 rVB 10287 18293 0.07% 0.007% 3 1.394 243 250 270 rVB 123899 166134 0.59% 0.061% 4 1.641 322 327 340 rBV 70348 84921 0.30% 0.031% 5 2.236 501 512 526 rBV 228956 355170 1.27% 0.131% 6 3.275 823 835 849 rBV3 6940 14287 0.05% 0.005% 7 4.194 1107 1121 1169 rVV 78766 277928 0.99% 0.102% 8 4.648 1243 1262 1292 rVB 169970 438222 1.56% 0.162% 9 4.976 1351 1364 1378 rVV3 9323 20625 0.07% 0.008% 10 5.207 1423 1436 1453 rBV4 12808 31005 0.11% 0.011% 11 5.336 1453 1476 1508 rVV2 407334 1160527 4.14% 0.428% 12 5.612 1551 1562 1587 rVB7 7420 17183 0.06% 0.006% 13 5.776 1599 1613 1632 rBV 37889 75418 0.27% 0.028% 14 5.886 1632 1647 1675 rBV 406174 864092 3.08% 0.319% 15 6.181 1726 1739 1749 rBV7 3875 8359 0.03% 0.003% 16 6.265 1752 1765 1772 rVV4 9056 19303 0.07% 0.007% 17 6.332 1773 1786 1800 rVV 247186 531951 1.90% 0.196% 18 6.410 1802 1810 1823 rVV3 84094 178699 0.64% 0.066% 19 6.471 1823 1829 1838 rVV3 15033 27765 0.10% 0.010% 20 6.529 1839 1847 1862 rVB3 19393 36206 0.13% 0.013% 21 6.638 1872 1881 1893 rVB5 6615 13405 0.05% 0.005% 22 6.731 1893 1910 1925 rVB6 15665 37853 0.14% 0.014% 23 6.902 1950 1963 1984 rVB7 13918 34934 0.12% 0.013% 24 7.101 2016 2025 2034 rBV3 13600 23913 0.09% 0.009% 25 7.178 2040 2049 2056 rBV 72257 120517 0.43% 0.044% 26 7.230 2057 2065 2081 rVB2 142729 286385 1.02% 0.106% 27 7.342 2091 2100 2120 rVB 65470 133256 0.48% 0.049% 28 7.529 2144 2158 2161 rBV2 117352 185682 0.66% 0.068% 29 7.567 2162 2170 2181 rVV 556491 1035238 3.69% 0.382% 30 7.641 2181 2193 2229 rVB 1639259 3163236 11.29% 1.167% 31 7.821 2239 2249 2256 rBV 222260 369105 1.32% 0.136% 32 7.918 2271 2279 2293 rVB2 73983 135835 0.48% 0.050% 33 8.046 2306 2319 2331 rBV2 59888 108739 0.39% 0.040% 34 8.229 2365 2376 2390 rBV 100041 172773 0.62% 0.064% 35 8.329 2393 2407 2434 rBV 435794 828975 2.96% 0.306% 36 8.458 2437 2447 2450 rBV 70449 110273 0.39% 0.041% 37 8.545 2466 2474 2485 rVB 147430 250476 0.89% 0.092% 38 8.609 2485 2494 2503 rBV 73553 122931 0.44% 0.045% 39 8.760 2532 2541 2549 rBV4 15726 26501 0.09% 0.010% 40 8.818 2549 2559 2563 rBV 63096 100480 0.36% 0.037% 41 8.911 2580 2588 2603 rVB2 278829 479698 1.71% 0.177% 42 9.033 2615 2626 2635 rBV 214594 352031 1.26% 0.130% 43 9.098 2635 2646 2664 rVV 620732 1116500 3.98% 0.412% 44 9.255 2682 2695 2719 rBV 3247235 5798969 20.70% 2.139% 45 9.384 2720 2735 2748 rVV 16018726 28020034 100.00% 10.334% 46 9.445 2749 2754 2782 rVB 952829 1502513 5.36% 0.554% 47 9.570 2782 2793 2807 rBV3 30718 56742 0.20% 0.021% 48 9.657 2812 2820 2826 rBV3 14938 24894 0.09% 0.009% 49 9.721 2827 2840 2848 rBV4 171886 329913 1.18% 0.122% 50 9.786 2848 2860 2883 rVB 6698647 11244746 40.13% 4.147% 51 9.956 2895 2913 2923 rBV3 225142 439338 1.57% 0.162% 52 10.049 2934 2942 2950 rBV3 170414 275921 0.98% 0.102% 53 10.172 2969 2980 2990 rBV 212535 359753 1.28% 0.133% 54 10.445 3053 3065 3076 rBV2 447184 959357 3.42% 0.354% 55 10.593 3103 3111 3121 rBV 282989 425898 1.52% 0.157% 56 10.686 3131 3140 3157 rBV 1268586 2776954 9.91% 1.024% 57 10.779 3158 3169 3174 rVV 808158 1358622 4.85% 0.501% 58 10.818 3175 3181 3203 rVB 1320345 1900998 6.78% 0.701% 59 10.979 3221 3231 3240 rBV 585780 942141 3.36% 0.347% 60 11.120 3268 3275 3276 rBV 243850 244436 0.87% 0.090% 61 11.155 3277 3286 3299 rVB 4171483 6314298 22.53% 2.329% 62 11.297 3315 3330 3335 rBV2 190545 446859 1.59% 0.165% 63 11.397 3353 3361 3366 rBV3 211738 348802 1.24% 0.129% 64 11.432 3367 3372 3381 rVV 452444 649852 2.32% 0.240% 65 11.487 3381 3389 3399 rVV3 945208 1457193 5.20% 0.537% 66 11.577 3408 3417 3426 rBV 3079785 4506660 16.08% 1.662% 67 11.786 3467 3482 3485 rBV3 2504166 4610787 16.46% 1.700% 68 11.815 3486 3491 3500 rVB 5373596 7443121 26.56% 2.745% 69 11.882 3500 3512 3532 rVB3 9499711 19687933 70.26% 7.261% 70 11.988 3536 3545 3551 rBV 467916 709562 2.53% 0.262% 71 12.033 3551 3559 3561 rBV 766976 924124 3.30% 0.341% 72 12.062 3562 3568 3584 rVB 2643472 3925235 14.01% 1.448% 73 12.152 3585 3596 3601 rBV 6367565 9943190 35.49% 3.667% 74 12.258 3617 3629 3652 rVB 13059742 20420121 72.88% 7.531% 75 12.390 3652 3670 3690 rBV6 1572849 5282784 18.85% 1.948% 76 12.499 3691 3704 3712 rBV3 708585 1332324 4.75% 0.491% 77 12.557 3712 3722 3733 rVB 3656117 5586066 19.94% 2.060% 78 12.657 3734 3753 3761 rBV 9927857 15765261 56.26% 5.814% 79 12.712 3761 3770 3785 rVB 14697179 21705441 77.46% 8.005% 80 12.792 3786 3795 3800 rBV 1657392 2425475 8.66% 0.895% 81 12.827 3801 3806 3810 rBV 1094714 1308425 4.67% 0.483% 82 12.969 3840 3850 3862 rVB2 5726297 8675336 30.96% 3.199% 83 13.036 3862 3871 3879 rBV2 1102254 1587686 5.67% 0.586% 84 13.091 3879 3888 3891 rVV3 1973744 2875910 10.26% 1.061% 85 13.130 3892 3900 3926 rVB3 10768527 20709965 73.91% 7.638% 86 13.242 3926 3935 3944 rBV 2269966 3224932 11.51% 1.189% 87 13.297 3945 3952 3960 rVB2 517622 763343 2.72% 0.282% 88 13.409 3978 3987 3996 rBV2 506929 856148 3.06% 0.316% 89 13.461 3998 4003 4009 rVB 190128 232828 0.83% 0.086% 90 13.512 4009 4019 4025 rBV2 2701716 4359307 15.56% 1.608% 91 13.644 4052 4060 4070 rVB 1358691 2048335 7.31% 0.755% 92 13.705 4071 4079 4081 rBV2 204991 252187 0.90% 0.093% 93 13.750 4082 4093 4103 rVB 10447793 16182507 57.75% 5.968% 94 13.966 4148 4160 4170 rBV5 390772 893865 3.19% 0.330% 95 14.155 4209 4219 4234 rVB 562414 896447 3.20% 0.331% 96 14.342 4266 4277 4302 rVB3 261487 575672 2.05% 0.212% 97 14.480 4311 4320 4331 rBV 180329 292058 1.04% 0.108% 98 14.541 4332 4339 4355 rVB2 93375 151977 0.54% 0.056% 99 14.882 4435 4445 4460 rBV 158550 251529 0.90% 0.093% 100 15.065 4494 4502 4518 rVB2 40187 75802 0.27% 0.028% Sum of corrected areas: 271151872