Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_U\DATA\VU050618\ Data File : VU023687.D Acq On : 06 May 2018 13:15 Operator : MD/SY Sample : J2721-04 Misc : 5.36g/5.0mL/100ul/5.0mL/MSVOA_U/MEOH ALS Vial : 7 Sample Multiplier: 1 Quant Time: May 07 09:30:59 2018 Quant Method : W:\HPCHEM1\MSVOA_U\METHOD\SOMULM050118WMA.M Quant Title : VOC Analysis QLast Update : Mon May 07 00:51:10 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) 1,4-Difluorobenzene 5.89 114 400251 50.00 ug/L 0.00 28) Chlorobenzene-d5 9.10 117 402999 50.00 ug/L 0.00 60) 1,4-Dichlorobenzene-d4 11.49 152 221766 50.00 ug/L 0.00 System Monitoring Compounds 4) Vinyl Chloride-d3 1.39 65 109976 38.77 ug/L 0.00 Spiked Amount 50.000 Range 60 - 135 Recovery = 77.54% 7) Chloroethane-d5 1.64 69 56147 25.97 ug/L -0.04 Spiked Amount 50.000 Range 70 - 130 Recovery = 51.94%# 11) 1,1-Dichloroethene-d2 2.24 63 151284 27.35 ug/L -0.04 Spiked Amount 50.000 Range 60 - 125 Recovery = 54.70%# 21) 2-Butanone-d5 4.19 46 197215 100.62 ug/L 0.02 Spiked Amount 100.000 Range 40 - 130 Recovery = 100.62% 24) Chloroform-d 4.65 84 186426 39.74 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 79.48% 26) 1,2-Dichloroethane-d4 5.31 65 128645 39.43 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 78.86% 32) Benzene-d6 5.34 84 418996 38.75 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 77.50% 36) 1,2-Dichloropropane-d6 6.33 67 140518 38.80 ug/L 0.00 Spiked Amount 50.000 Range 70 - 120 Recovery = 77.60% 41) Toluene-d8 7.57 98 456901 45.84 ug/L 0.00 Spiked Amount 50.000 Range 80 - 120 Recovery = 91.68% 43) trans-1,3-Dichloropropene- 7.86 79 64441 41.33 ug/L 0.00 Spiked Amount 50.000 Range 60 - 125 Recovery = 82.66% 47) 2-Hexanone-d5 8.33 63 164949 119.93 ug/L 0.02 Spiked Amount 100.000 Range 45 - 130 Recovery = 119.93% 57) 1,1,2,2-Tetrachloroethane- 10.44 84 222137 47.42 ug/L 0.00 Spiked Amount 50.000 Range 65 - 120 Recovery = 94.84% 64) 1,2-Dichlorobenzene-d4 11.87 152 185694 42.92 ug/L 0.00 Spiked Amount 50.000 Range 80 - 120 Recovery = 85.84% Target Compounds Qvalue 30) 1,1,1-Trichloroethane 4.91 97 15518 3.04 ug/L 100 35) Methylcyclohexane 6.42 83 2973201 522.42 ug/L 91 42) Toluene 7.63 91 28126184m 1910.85 ug/L 52) Ethylbenzene 9.26 91 9876735 619.02 ug/L 98 53) m,p-Xylene 9.39 106 13387645m 2199.87 ug/L 54) o-xylene 9.79 106 6870403 1191.59 ug/L 95 56) Isopropylbenzene 10.17 105 4400216 290.78 ug/L 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed