LSC Area Percent Report Data Path : W:\HPCHEM1\MSVOA_U\DATA\VU050618\ Data File : VU023687.D Acq On : 06 May 2018 13:15 Operator : MD/SY Sample : J2721-04 Misc : 5.36g/5.0mL/100ul/5.0mL/MSVOA_U/MEOH ALS Vial : 7 Sample Multiplier: 1 Integration Parameters: LSCINT.P Integrator: RTE Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 0 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Method : W:\HPCHEM1\MSVOA_U\METHOD\SOMULM050118WMA.M Title : VOC Analysis Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total --- ----- ----- ---- ---- --- ------- ------- ------ ------- 1 1.079 136 152 173 rBV 1224562 1385828 1.14% 0.138% 2 3.278 817 836 866 rBV 938748 1993585 1.64% 0.199% 3 4.075 1066 1084 1106 rVV 690364 1891298 1.56% 0.188% 4 4.722 1272 1285 1315 rVB 565617 1582438 1.30% 0.158% 5 4.985 1345 1367 1381 rBV 16303885 38927903 32.02% 3.880% 6 5.075 1381 1395 1417 rVB 4932267 12141299 9.99% 1.210% 7 5.223 1418 1441 1463 rBV 25517066 61290307 50.42% 6.108% 8 5.336 1465 1476 1495 rVB2 412224 1040078 0.86% 0.104% 9 5.480 1502 1521 1533 rBV3 5151537 12172280 10.01% 1.213% 10 5.551 1533 1543 1553 rVV2 2975510 6515203 5.36% 0.649% 11 5.622 1553 1565 1596 rVB 3527342 8237436 6.78% 0.821% 12 5.799 1596 1620 1638 rBV 38482788 85417601 70.27% 8.513% 13 5.889 1638 1648 1656 rBV 377622 677276 0.56% 0.067% 14 5.943 1656 1665 1678 rBV4 460281 956909 0.79% 0.095% 15 6.268 1755 1766 1778 rVB 1488545 2951219 2.43% 0.294% 16 6.413 1792 1811 1822 rVV4 6640575 16508108 13.58% 1.645% 17 6.474 1822 1830 1839 rVV 2375314 4407266 3.63% 0.439% 18 6.532 1839 1848 1860 rVB 3533526 6590909 5.42% 0.657% 19 6.641 1871 1882 1894 rVB 1609187 2991771 2.46% 0.298% 20 6.728 1894 1909 1927 rVB5 2187839 5212483 4.29% 0.519% 21 6.905 1950 1964 1986 rVB3 1055548 2689515 2.21% 0.268% 22 7.059 1986 2012 2016 rBV6 424394 1092534 0.90% 0.109% 23 7.104 2017 2026 2036 rBV 1989623 3270959 2.69% 0.326% 24 7.185 2037 2051 2058 rBV 7977264 14226183 11.70% 1.418% 25 7.223 2059 2063 2080 rVB 3252501 4777443 3.93% 0.476% 26 7.303 2080 2088 2091 rBV 542108 770642 0.63% 0.077% 27 7.345 2091 2101 2122 rVB 6551714 13916526 11.45% 1.387% 28 7.442 2122 2131 2144 rVB4 316428 728414 0.60% 0.073% 29 7.532 2144 2159 2166 rBV2 3371740 6700044 5.51% 0.668% 30 7.660 2180 2199 2210 rBV3 53912209 121561323 100.00% 12.115% 31 7.718 2210 2217 2230 rVV3 584544 1471941 1.21% 0.147% 32 7.828 2240 2251 2269 rVB 9806323 15887856 13.07% 1.583% 33 7.924 2269 2281 2302 rVB2 2001718 3759553 3.09% 0.375% 34 8.049 2303 2320 2331 rBV 919682 1677204 1.38% 0.167% 35 8.162 2331 2355 2365 rVB4 372442 1013859 0.83% 0.101% 36 8.230 2365 2376 2388 rVB 736213 1233509 1.01% 0.123% 37 8.332 2389 2408 2419 rBV2 1940235 3619265 2.98% 0.361% 38 8.458 2432 2447 2452 rBV 1123214 1970690 1.62% 0.196% 39 8.490 2453 2457 2465 rVV3 972838 1432579 1.18% 0.143% 40 8.548 2465 2475 2485 rVB 2437436 4109272 3.38% 0.410% 41 8.609 2485 2494 2504 rBV 1709849 2945499 2.42% 0.294% 42 8.818 2549 2559 2564 rVV 1157663 1883177 1.55% 0.188% 43 8.853 2565 2570 2580 rVV5 939865 2051094 1.69% 0.204% 44 8.914 2580 2589 2602 rVB2 2945100 5031053 4.14% 0.501% 45 9.037 2615 2627 2637 rBV 2155615 3561220 2.93% 0.355% 46 9.098 2637 2646 2657 rVB 648002 1089778 0.90% 0.109% 47 9.258 2683 2696 2710 rBV 13074619 22723329 18.69% 2.265% 48 9.390 2718 2737 2748 rBV2 41343665 77791290 63.99% 7.753% 49 9.448 2748 2755 2782 rVB 5318685 8599205 7.07% 0.857% 50 9.725 2827 2841 2848 rBV4 865075 1707318 1.40% 0.170% 51 9.792 2849 2862 2882 rVB 24031715 40775604 33.54% 4.064% 52 9.956 2894 2913 2923 rBV3 1455193 2878297 2.37% 0.287% 53 10.049 2923 2942 2950 rVV3 1372369 2815396 2.32% 0.281% 54 10.094 2951 2956 2967 rVV2 654184 1036542 0.85% 0.103% 55 10.175 2968 2981 2992 rVV 6589735 10707259 8.81% 1.067% 56 10.258 2992 3007 3015 rVV4 645622 1507894 1.24% 0.150% 57 10.326 3016 3028 3033 rVV2 969733 1935868 1.59% 0.193% 58 10.358 3034 3038 3053 rVB2 1052521 1727359 1.42% 0.172% 59 10.458 3053 3069 3076 rBV2 1228293 2721296 2.24% 0.271% 60 10.496 3077 3081 3091 rVB4 616345 862328 0.71% 0.086% 61 10.596 3100 3112 3124 rBV 14466300 23179983 19.07% 2.310% 62 10.696 3130 3143 3159 rBV2 29441175 69419787 57.11% 6.919% 63 10.782 3159 3170 3177 rVV 13383836 21254875 17.48% 2.118% 64 10.821 3177 3182 3193 rVB 6205654 8483927 6.98% 0.846% 65 10.982 3221 3232 3251 rVB 12343414 19818846 16.30% 1.975% 66 11.165 3268 3289 3312 rVB2 41451764 71969096 59.20% 7.173% 67 11.300 3315 3331 3335 rBV2 769161 1736635 1.43% 0.173% 68 11.336 3336 3342 3353 rVB2 892120 1572364 1.29% 0.157% 69 11.403 3354 3363 3367 rBV3 1032615 1582768 1.30% 0.158% 70 11.435 3368 3373 3382 rVB 1334434 1907559 1.57% 0.190% 71 11.487 3382 3389 3398 rBV3 1255300 1776162 1.46% 0.177% 72 11.580 3408 3418 3427 rBV 10176662 15034333 12.37% 1.498% 73 11.705 3451 3457 3468 rVB2 731977 1170163 0.96% 0.117% 74 11.776 3468 3479 3485 rBV3 2338497 4422111 3.64% 0.441% 75 11.815 3486 3491 3499 rVV 3370307 4814524 3.96% 0.480% 76 11.876 3499 3510 3527 rVB5 5444248 12712066 10.46% 1.267% 77 12.030 3549 3558 3564 rVV 3349350 5021656 4.13% 0.500% 78 12.062 3564 3568 3586 rVB 1885566 2809655 2.31% 0.280% 79 12.152 3586 3596 3600 rBV 2905749 4190234 3.45% 0.418% 80 12.181 3601 3605 3615 rVB 3317030 4545385 3.74% 0.453% 81 12.258 3617 3629 3638 rBV 5891644 8834004 7.27% 0.880% 82 12.364 3652 3662 3665 rBV 957548 1461172 1.20% 0.146% 83 12.499 3692 3704 3713 rBV5 541781 1139603 0.94% 0.114% 84 12.557 3714 3722 3732 rVB 1647450 2595837 2.14% 0.259% 85 12.622 3732 3742 3744 rBV4 635860 884191 0.73% 0.088% 86 12.654 3744 3752 3760 rVV 3566291 5317032 4.37% 0.530% 87 12.708 3760 3769 3786 rVB 5186145 8121764 6.68% 0.809% 88 12.789 3787 3794 3800 rBV 536187 797042 0.66% 0.079% 89 12.969 3841 3850 3861 rVB2 1822684 2765590 2.28% 0.276% 90 13.036 3862 3871 3879 rBV2 535512 811827 0.67% 0.081% 91 13.088 3879 3887 3890 rVV2 686165 946747 0.78% 0.094% 92 13.126 3891 3899 3926 rVB3 4151157 7930529 6.52% 0.790% 93 13.242 3926 3935 3943 rBV 825589 1166996 0.96% 0.116% 94 13.512 4009 4019 4025 rBV3 1271374 2094839 1.72% 0.209% 95 13.644 4046 4060 4071 rVB2 646274 1094655 0.90% 0.109% 96 13.747 4074 4092 4101 rVV 2269470 3606339 2.97% 0.359% 97 14.152 4208 4218 4234 rVB3 416374 798472 0.66% 0.080% 98 14.345 4266 4278 4301 rBV5 320674 764779 0.63% 0.076% 99 14.480 4311 4320 4331 rBV 433730 706231 0.58% 0.070% 100 14.879 4434 4444 4456 rBV 582679 972945 0.80% 0.097% Sum of corrected areas: 1003384037