Quantitation Report (LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_U\DATA\VU050618\ Data File : VU023689.D Acq On : 06 May 2018 14:38 Operator : MD/SY Sample : J2721-18DL 20X Misc : 3.72g/5.0mL/100ul/5.0mL/MSVOA_U/MEOH ALS Vial : 9 Sample Multiplier: 1 Quant Time: May 07 01:49:38 2018 Quant Method : W:\HPCHEM1\MSVOA_U\METHOD\SOMULM050118WMA.M Quant Title : VOC Analysis QLast Update : Mon May 07 00:51:10 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) 1,4-Difluorobenzene 5.89 114 395509 50.00 ug/L 0.00 28) Chlorobenzene-d5 9.09 117 381020 50.00 ug/L 0.00 60) 1,4-Dichlorobenzene-d4 11.49 152 200377 50.00 ug/L 0.00 System Monitoring Compounds 4) Vinyl Chloride-d3 1.40 65 113289 40.41 ug/L 0.00 Spiked Amount 50.000 Range 60 - 135 Recovery = 80.82% 7) Chloroethane-d5 1.67 69 90581 42.39 ug/L 0.00 Spiked Amount 50.000 Range 70 - 130 Recovery = 84.78% 11) 1,1-Dichloroethene-d2 2.27 63 159464 29.18 ug/L 0.00 Spiked Amount 50.000 Range 60 - 125 Recovery = 58.36%# 21) 2-Butanone-d5 4.18 46 187394 96.76 ug/L 0.00 Spiked Amount 100.000 Range 40 - 130 Recovery = 96.76% 24) Chloroform-d 4.65 84 205437 44.32 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 88.64% 26) 1,2-Dichloroethane-d4 5.31 65 138920 43.09 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 86.18% 32) Benzene-d6 5.35 84 443302 43.36 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 86.72% 36) 1,2-Dichloropropane-d6 6.33 67 149476 43.65 ug/L 0.00 Spiked Amount 50.000 Range 70 - 120 Recovery = 87.30% 41) Toluene-d8 7.57 98 403995 42.87 ug/L 0.00 Spiked Amount 50.000 Range 80 - 120 Recovery = 85.74% 43) trans-1,3-Dichloropropene- 7.85 79 60473 41.02 ug/L 0.00 Spiked Amount 50.000 Range 60 - 125 Recovery = 82.04% 47) 2-Hexanone-d5 8.31 63 135619 104.30 ug/L 0.00 Spiked Amount 100.000 Range 45 - 130 Recovery = 104.30% 57) 1,1,2,2-Tetrachloroethane- 10.44 84 193532 43.70 ug/L 0.00 Spiked Amount 50.000 Range 65 - 120 Recovery = 87.40% 64) 1,2-Dichlorobenzene-d4 11.86 152 176021 45.03 ug/L 0.00 Spiked Amount 50.000 Range 80 - 120 Recovery = 90.06% Target Compounds Qvalue 42) Toluene 7.64 91 76622 5.51 ug/L 98 52) Ethylbenzene 9.26 91 119319 7.91 ug/L 99 53) m,p-Xylene 9.38 106 239584 41.64 ug/L 98 54) o-xylene 9.78 106 91313 16.75 ug/L 100 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed