LSC Area Percent Report Data Path : W:\HPCHEM1\MSVOA_U\DATA\VU050618\ Data File : VU023689.D Acq On : 06 May 2018 14:38 Operator : MD/SY Sample : J2721-18DL 20X Misc : 3.72g/5.0mL/100ul/5.0mL/MSVOA_U/MEOH ALS Vial : 9 Sample Multiplier: 1 Integration Parameters: LSCINT.P Integrator: RTE Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 0 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Method : W:\HPCHEM1\MSVOA_U\METHOD\SOMULM050118WMA.M Title : VOC Analysis Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total --- ----- ----- ---- ---- --- ------- ------- ------ ------- 1 1.088 137 155 175 rBV 1318007 1507982 77.47% 6.150% 2 1.182 180 184 191 rVB 8184 8639 0.44% 0.035% 3 1.397 245 251 263 rBV 172352 177523 9.12% 0.724% 4 1.674 329 337 355 rVB 125657 166650 8.56% 0.680% 5 2.188 491 497 506 rVB5 3669 5202 0.27% 0.021% 6 2.272 512 523 537 rBV 276661 417471 21.45% 1.702% 7 2.442 570 576 583 rBV3 348 604 0.03% 0.002% 8 2.706 650 658 663 rVV5 924 1322 0.07% 0.005% 9 2.837 688 699 715 rVB2 3070 5815 0.30% 0.024% 10 4.175 1100 1115 1150 rBV 114545 302106 15.52% 1.232% 11 4.651 1245 1263 1292 rBV 205198 484644 24.90% 1.976% 12 4.886 1330 1336 1348 rVB4 543 1109 0.06% 0.005% 13 4.989 1359 1368 1378 rBV5 1774 3215 0.17% 0.013% 14 5.220 1429 1440 1451 rVB6 2277 4760 0.24% 0.019% 15 5.342 1454 1478 1513 rBV2 436135 1292583 66.40% 5.271% 16 5.786 1607 1616 1633 rVB3 4968 9677 0.50% 0.039% 17 5.889 1633 1648 1678 rBV 458994 918741 47.20% 3.747% 18 6.178 1731 1738 1744 rBV3 1597 2565 0.13% 0.010% 19 6.252 1755 1761 1763 rBV2 378 426 0.02% 0.002% 20 6.333 1772 1786 1805 rBV 283259 576279 29.60% 2.350% 21 6.532 1843 1848 1850 rBV3 833 693 0.04% 0.003% 22 6.741 1904 1913 1917 rVV5 622 813 0.04% 0.003% 23 6.860 1943 1950 1955 rBV3 659 857 0.04% 0.003% 24 7.107 2021 2027 2031 rBV2 715 848 0.04% 0.003% 25 7.185 2042 2051 2054 rVV5 3754 5697 0.29% 0.023% 26 7.230 2054 2065 2085 rVB2 151191 270353 13.89% 1.103% 27 7.349 2092 2102 2111 rVB4 3284 5305 0.27% 0.022% 28 7.567 2150 2170 2183 rBV 587167 1043179 53.59% 4.254% 29 7.641 2184 2193 2209 rVB 100248 181700 9.33% 0.741% 30 7.853 2241 2259 2273 rBV 105619 195777 10.06% 0.798% 31 8.050 2311 2320 2329 rBV4 2608 4209 0.22% 0.017% 32 8.165 2347 2356 2366 rBV3 824 1393 0.07% 0.006% 33 8.233 2370 2377 2387 rVB5 4640 6762 0.35% 0.028% 34 8.313 2390 2402 2431 rBV 386969 666644 34.25% 2.719% 35 8.548 2466 2475 2486 rVB3 8632 14952 0.77% 0.061% 36 8.615 2486 2496 2507 rBV7 4132 8155 0.42% 0.033% 37 8.818 2550 2559 2564 rBV4 3077 5096 0.26% 0.021% 38 8.853 2564 2570 2580 rVV7 3554 6761 0.35% 0.028% 39 8.911 2580 2588 2602 rVB2 11022 18480 0.95% 0.075% 40 9.037 2617 2627 2633 rBV 8291 13012 0.67% 0.053% 41 9.091 2633 2644 2682 rVB 659930 1117193 57.39% 4.556% 42 9.252 2683 2694 2709 rBV 167256 271424 13.94% 1.107% 43 9.377 2720 2733 2747 rBV 838365 1391224 71.47% 5.673% 44 9.448 2748 2755 2772 rVB2 37934 61641 3.17% 0.251% 45 9.567 2787 2792 2793 rBV3 621 542 0.03% 0.002% 46 9.718 2824 2839 2847 rBV7 7377 14202 0.73% 0.058% 47 9.783 2848 2859 2884 rVB 338111 545164 28.01% 2.223% 48 9.953 2896 2912 2924 rVB5 9489 19344 0.99% 0.079% 49 10.011 2924 2930 2933 rBV3 1263 1701 0.09% 0.007% 50 10.046 2933 2941 2949 rBV5 8352 13111 0.67% 0.053% 51 10.172 2969 2980 2990 rBV2 10587 16971 0.87% 0.069% 52 10.217 2990 2994 2995 rBV2 642 440 0.02% 0.002% 53 10.262 3002 3008 3015 rVB6 3023 3946 0.20% 0.016% 54 10.435 3050 3062 3077 rBV 388472 627748 32.25% 2.560% 55 10.593 3101 3111 3121 rBV 13942 22025 1.13% 0.090% 56 10.683 3130 3139 3156 rBV 56129 123913 6.37% 0.505% 57 10.776 3157 3168 3174 rVV 34707 57917 2.98% 0.236% 58 10.818 3174 3181 3194 rVB 50220 74217 3.81% 0.303% 59 10.975 3221 3230 3238 rBV2 25647 39057 2.01% 0.159% 60 11.078 3256 3262 3267 rBV6 2848 3897 0.20% 0.016% 61 11.120 3268 3275 3276 rVV2 11597 12044 0.62% 0.049% 62 11.152 3276 3285 3297 rVB 180666 274922 14.12% 1.121% 63 11.297 3314 3330 3334 rBV4 8570 19009 0.98% 0.078% 64 11.397 3352 3361 3365 rBV5 8202 12863 0.66% 0.052% 65 11.432 3366 3372 3378 rVV 19173 25822 1.33% 0.105% 66 11.487 3378 3389 3407 rVV 763912 1200016 61.65% 4.894% 67 11.573 3407 3416 3425 rBV 137488 200019 10.28% 0.816% 68 11.782 3467 3481 3484 rBV3 117127 206165 10.59% 0.841% 69 11.811 3485 3490 3497 rVV 268735 389110 19.99% 1.587% 70 11.866 3497 3507 3529 rVB4 962907 1946644 100.00% 7.939% 71 11.985 3535 3544 3550 rBV 22530 34267 1.76% 0.140% 72 12.030 3550 3558 3561 rBV 46085 61807 3.18% 0.252% 73 12.059 3562 3567 3584 rVB 124157 183785 9.44% 0.749% 74 12.149 3584 3595 3600 rBV 308374 478631 24.59% 1.952% 75 12.255 3616 3628 3651 rVB 673192 1017908 52.29% 4.151% 76 12.390 3651 3670 3690 rBV7 73351 254477 13.07% 1.038% 77 12.496 3690 3703 3711 rBV4 34610 64312 3.30% 0.262% 78 12.554 3711 3721 3732 rVB 167019 260055 13.36% 1.061% 79 12.654 3733 3752 3760 rBV 484323 762400 39.16% 3.109% 80 12.705 3760 3768 3785 rVB 738958 1095446 56.27% 4.467% 81 12.789 3785 3794 3799 rBV 79697 116122 5.97% 0.474% 82 12.824 3800 3805 3809 rBV 53955 62836 3.23% 0.256% 83 12.969 3840 3850 3862 rVB 272926 416569 21.40% 1.699% 84 13.033 3862 3870 3878 rBV3 50256 75280 3.87% 0.307% 85 13.091 3878 3888 3890 rVV2 92066 128525 6.60% 0.524% 86 13.126 3891 3899 3926 rVB2 535664 1055846 54.24% 4.306% 87 13.242 3926 3935 3944 rBV 105542 156155 8.02% 0.637% 88 13.294 3945 3951 3960 rVB5 23399 37219 1.91% 0.152% 89 13.409 3978 3987 3996 rBV3 22245 37310 1.92% 0.152% 90 13.512 4009 4019 4025 rBV2 119596 202262 10.39% 0.825% 91 13.641 4045 4059 4070 rVB 61447 98244 5.05% 0.401% 92 13.702 4071 4078 4080 rBV2 9080 9286 0.48% 0.038% 93 13.747 4081 4092 4104 rVV 490654 756119 38.84% 3.083% 94 13.843 4118 4122 4124 rBV4 1716 1583 0.08% 0.006% 95 13.962 4148 4159 4169 rBV3 16979 38183 1.96% 0.156% 96 14.155 4209 4219 4233 rBV4 26155 45551 2.34% 0.186% 97 14.339 4266 4276 4290 rBV4 10525 22258 1.14% 0.091% 98 14.483 4313 4321 4329 rBV2 6684 9719 0.50% 0.040% 99 14.538 4334 4338 4349 rVB5 3123 4405 0.23% 0.018% 100 14.895 4443 4449 4457 rVB6 3015 4692 0.24% 0.019% Sum of corrected areas: 24521542