Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_U\DATA\VU050618\ Data File : VU023690.D Acq On : 06 May 2018 15:04 Operator : MD/SY Sample : J2721-01DL 200X Misc : 6.42g/5.0mL/100ul/5.0mL/MSVOA_U/MEOH ALS Vial : 10 Sample Multiplier: 1 Quant Time: May 07 01:53:27 2018 Quant Method : W:\HPCHEM1\MSVOA_U\METHOD\SOMULM050118WMA.M Quant Title : VOC Analysis QLast Update : Mon May 07 00:51:10 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) 1,4-Difluorobenzene 5.89 114 388618 50.00 ug/L 0.00 28) Chlorobenzene-d5 9.09 117 365554 50.00 ug/L 0.00 60) 1,4-Dichlorobenzene-d4 11.49 152 187327 50.00 ug/L 0.00 System Monitoring Compounds 4) Vinyl Chloride-d3 1.40 65 113492 41.20 ug/L 0.00 Spiked Amount 50.000 Range 60 - 135 Recovery = 82.40% 7) Chloroethane-d5 1.68 69 89947 42.84 ug/L 0.00 Spiked Amount 50.000 Range 70 - 130 Recovery = 85.68% 11) 1,1-Dichloroethene-d2 2.27 63 157632 29.35 ug/L 0.00 Spiked Amount 50.000 Range 60 - 125 Recovery = 58.70%# 21) 2-Butanone-d5 4.18 46 195983 102.99 ug/L 0.00 Spiked Amount 100.000 Range 40 - 130 Recovery = 102.99% 24) Chloroform-d 4.65 84 203658 44.71 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 89.42% 26) 1,2-Dichloroethane-d4 5.31 65 138019 43.57 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 87.14% 32) Benzene-d6 5.35 84 442869 45.15 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 90.30% 36) 1,2-Dichloropropane-d6 6.33 67 148625 45.24 ug/L 0.00 Spiked Amount 50.000 Range 70 - 120 Recovery = 90.48% 41) Toluene-d8 7.57 98 399195 44.15 ug/L 0.00 Spiked Amount 50.000 Range 80 - 120 Recovery = 88.30% 43) trans-1,3-Dichloropropene- 7.85 79 60560 42.82 ug/L 0.00 Spiked Amount 50.000 Range 60 - 125 Recovery = 85.64% 47) 2-Hexanone-d5 8.31 63 140796 112.86 ug/L 0.00 Spiked Amount 100.000 Range 45 - 130 Recovery = 112.86% 57) 1,1,2,2-Tetrachloroethane- 10.44 84 194548 45.78 ug/L 0.00 Spiked Amount 50.000 Range 65 - 120 Recovery = 91.56% 64) 1,2-Dichlorobenzene-d4 11.86 152 168997 46.24 ug/L 0.00 Spiked Amount 50.000 Range 80 - 120 Recovery = 92.48% Target Compounds Qvalue 35) Methylcyclohexane 6.42 83 6747 1.31 ug/L 94 42) Toluene 7.64 91 111728 8.37 ug/L 99 52) Ethylbenzene 9.26 91 187464 12.95 ug/L 100 53) m,p-Xylene 9.38 106 150958 27.35 ug/L 97 54) o-xylene 9.78 106 51522 9.85 ug/L 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed