LSC Area Percent Report Data Path : W:\HPCHEM1\MSVOA_U\DATA\VU050618\ Data File : VU023690.D Acq On : 06 May 2018 15:04 Operator : MD/SY Sample : J2721-01DL 200X Misc : 6.42g/5.0mL/100ul/5.0mL/MSVOA_U/MEOH ALS Vial : 10 Sample Multiplier: 1 Integration Parameters: LSCINT.P Integrator: RTE Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 0 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Method : W:\HPCHEM1\MSVOA_U\METHOD\SOMULM050118WMA.M Title : VOC Analysis Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total --- ----- ----- ---- ---- --- ------- ------- ------ ------- 1 1.089 134 155 178 rBV 1263559 1428930 100.00% 9.481% 2 1.182 180 184 192 rVB2 7392 7368 0.52% 0.049% 3 1.397 245 251 267 rVB 170146 174709 12.23% 1.159% 4 1.680 331 339 356 rVB 128201 161630 11.31% 1.072% 5 2.188 494 497 505 rVB5 3135 3786 0.26% 0.025% 6 2.272 512 523 538 rBV 271181 413530 28.94% 2.744% 7 2.703 650 657 665 rVB4 755 1015 0.07% 0.007% 8 2.838 689 699 713 rVB2 2061 4173 0.29% 0.028% 9 2.998 741 749 753 rBV4 493 595 0.04% 0.004% 10 3.310 837 846 856 rVB5 1441 2627 0.18% 0.017% 11 4.018 1061 1066 1073 rBV2 779 1077 0.08% 0.007% 12 4.178 1100 1116 1156 rBV 119845 320599 22.44% 2.127% 13 4.651 1246 1263 1299 rBV 203252 484852 33.93% 3.217% 14 4.992 1357 1369 1382 rVB5 4382 9858 0.69% 0.065% 15 5.079 1389 1396 1398 rBV3 1211 1392 0.10% 0.009% 16 5.220 1430 1440 1453 rBV4 5081 11530 0.81% 0.077% 17 5.342 1454 1478 1514 rBV2 428419 1286130 90.01% 8.534% 18 5.555 1539 1544 1551 rVB5 1027 1317 0.09% 0.009% 19 5.616 1557 1563 1565 rBV3 1106 1018 0.07% 0.007% 20 5.789 1605 1617 1633 rVB2 14149 28587 2.00% 0.190% 21 5.889 1634 1648 1690 rBV 441593 896575 62.74% 5.949% 22 6.178 1730 1738 1748 rVB3 2121 3286 0.23% 0.022% 23 6.336 1772 1787 1803 rBV 283593 578328 40.47% 3.837% 24 6.532 1844 1848 1849 rBV2 900 624 0.04% 0.004% 25 6.645 1878 1883 1889 rVB5 1126 1075 0.08% 0.007% 26 6.738 1905 1912 1914 rBV3 1371 1496 0.10% 0.010% 27 6.895 1958 1961 1963 rBV3 824 616 0.04% 0.004% 28 7.104 2018 2026 2033 rBV5 1051 1542 0.11% 0.010% 29 7.185 2041 2051 2055 rBV3 5701 8988 0.63% 0.060% 30 7.230 2055 2065 2087 rVB 152674 275365 19.27% 1.827% 31 7.346 2093 2101 2109 rVB4 3313 5390 0.38% 0.036% 32 7.567 2149 2170 2183 rBV 583984 1037112 72.58% 6.882% 33 7.641 2184 2193 2223 rVB 150791 277842 19.44% 1.844% 34 7.854 2240 2259 2275 rBV2 104264 205542 14.38% 1.364% 35 8.050 2314 2320 2328 rVB4 1381 1868 0.13% 0.012% 36 8.172 2352 2358 2361 rBV3 460 572 0.04% 0.004% 37 8.233 2370 2377 2380 rBV5 622 580 0.04% 0.004% 38 8.313 2390 2402 2435 rBV 398018 695715 48.69% 4.616% 39 8.490 2454 2457 2466 rVB5 2385 2710 0.19% 0.018% 40 8.548 2466 2475 2484 rVB6 4907 8053 0.56% 0.053% 41 8.612 2485 2495 2506 rBV4 2111 4158 0.29% 0.028% 42 8.821 2554 2560 2564 rBV4 1285 1320 0.09% 0.009% 43 8.863 2566 2573 2577 rVV7 1334 1837 0.13% 0.012% 44 8.915 2581 2589 2598 rVB5 5927 9872 0.69% 0.066% 45 9.037 2619 2627 2632 rBV3 4323 5782 0.40% 0.038% 46 9.095 2632 2645 2682 rVB 641138 1074971 75.23% 7.133% 47 9.252 2682 2694 2714 rBV 261377 426511 29.85% 2.830% 48 9.378 2719 2733 2749 rVV 533742 878305 61.47% 5.828% 49 9.445 2749 2754 2768 rVB2 11993 19607 1.37% 0.130% 50 9.718 2832 2839 2846 rBV4 1746 2463 0.17% 0.016% 51 9.783 2847 2859 2879 rVV 188414 303027 21.21% 2.011% 52 9.953 2905 2912 2920 rVV3 3074 4094 0.29% 0.027% 53 10.050 2934 2942 2949 rVV5 2451 3680 0.26% 0.024% 54 10.088 2950 2954 2968 rVB4 1364 2167 0.15% 0.014% 55 10.172 2968 2980 2991 rBV3 4486 7188 0.50% 0.048% 56 10.259 3001 3007 3015 rBV4 1181 1664 0.12% 0.011% 57 10.326 3016 3028 3033 rBV7 2121 3974 0.28% 0.026% 58 10.355 3033 3037 3049 rVB7 2640 3439 0.24% 0.023% 59 10.435 3049 3062 3080 rBV 391164 628936 44.01% 4.173% 60 10.593 3102 3111 3122 rBV2 7327 11351 0.79% 0.075% 61 10.686 3129 3140 3156 rBV 20724 43046 3.01% 0.286% 62 10.776 3156 3168 3174 rVV 10284 16940 1.19% 0.112% 63 10.818 3174 3181 3193 rVB2 17786 26215 1.83% 0.174% 64 10.979 3221 3231 3238 rBV2 7497 11141 0.78% 0.074% 65 11.079 3256 3262 3266 rBV6 1125 1540 0.11% 0.010% 66 11.117 3268 3274 3278 rVV3 4897 6579 0.46% 0.044% 67 11.152 3278 3285 3297 rVB 40096 59923 4.19% 0.398% 68 11.275 3317 3323 3325 rBV2 1626 1765 0.12% 0.012% 69 11.400 3354 3362 3366 rBV6 2505 3588 0.25% 0.024% 70 11.487 3377 3389 3409 rBV 700527 1111559 77.79% 7.376% 71 11.574 3409 3416 3424 rBV 21149 30424 2.13% 0.202% 72 11.706 3451 3457 3466 rVB3 4240 5925 0.41% 0.039% 73 11.783 3468 3481 3484 rBV4 14863 26301 1.84% 0.175% 74 11.812 3486 3490 3496 rVV 31262 42213 2.95% 0.280% 75 11.863 3496 3506 3530 rVB 646603 1113817 77.95% 7.391% 76 11.982 3537 3543 3549 rBV5 3100 4661 0.33% 0.031% 77 12.027 3550 3557 3562 rBV 21677 29896 2.09% 0.198% 78 12.149 3585 3595 3599 rBV 35546 49823 3.49% 0.331% 79 12.255 3616 3628 3650 rVB 72899 119679 8.38% 0.794% 80 12.361 3653 3661 3664 rBV3 10368 14183 0.99% 0.094% 81 12.496 3692 3703 3710 rBV7 5822 10067 0.70% 0.067% 82 12.554 3713 3721 3732 rVB 20777 32271 2.26% 0.214% 83 12.622 3734 3742 3743 rBV5 4856 5333 0.37% 0.035% 84 12.654 3744 3752 3760 rVV 51083 78107 5.47% 0.518% 85 12.705 3760 3768 3779 rVB 79678 118610 8.30% 0.787% 86 12.789 3787 3794 3799 rBV3 12449 17000 1.19% 0.113% 87 12.824 3801 3805 3809 rVV3 6401 7045 0.49% 0.047% 88 12.969 3841 3850 3863 rVB3 33718 53435 3.74% 0.355% 89 13.033 3863 3870 3878 rBV3 8408 12139 0.85% 0.081% 90 13.091 3879 3888 3890 rBV4 11692 16277 1.14% 0.108% 91 13.127 3891 3899 3916 rVB3 70344 121959 8.53% 0.809% 92 13.242 3926 3935 3943 rBV 12515 17841 1.25% 0.118% 93 13.410 3981 3987 3996 rVB6 2257 3126 0.22% 0.021% 94 13.458 3998 4002 4010 rVB6 1668 1893 0.13% 0.013% 95 13.512 4010 4019 4025 rBV2 14779 24712 1.73% 0.164% 96 13.644 4054 4060 4069 rVB 5652 7627 0.53% 0.051% 97 13.750 4082 4093 4103 rBV 44955 74567 5.22% 0.495% 98 13.969 4153 4161 4169 rBV6 1488 2711 0.19% 0.018% 99 14.149 4209 4217 4218 rBV4 2822 2874 0.20% 0.019% 100 14.898 4447 4450 4465 rVB4 1282 1594 0.11% 0.011% Sum of corrected areas: 15070754