Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_U\DATA\VU050618\ Data File : VU023691.D Acq On : 06 May 2018 15:30 Operator : MD/SY Sample : J2721-04DL 200X Misc : 5.36g/5.0mL/100ul/5.0mL/MSVOA_U/MEOH ALS Vial : 11 Sample Multiplier: 1 Quant Time: May 07 01:55:17 2018 Quant Method : W:\HPCHEM1\MSVOA_U\METHOD\SOMULM050118WMA.M Quant Title : VOC Analysis QLast Update : Mon May 07 00:51:10 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) 1,4-Difluorobenzene 5.89 114 400924 50.00 ug/L 0.00 28) Chlorobenzene-d5 9.09 117 368698 50.00 ug/L 0.00 60) 1,4-Dichlorobenzene-d4 11.49 152 187931 50.00 ug/L 0.00 System Monitoring Compounds 4) Vinyl Chloride-d3 1.40 65 113390 39.90 ug/L 0.00 Spiked Amount 50.000 Range 60 - 135 Recovery = 79.80% 7) Chloroethane-d5 1.68 69 91912 42.44 ug/L 0.00 Spiked Amount 50.000 Range 70 - 130 Recovery = 84.88% 11) 1,1-Dichloroethene-d2 2.27 63 170683 30.81 ug/L 0.00 Spiked Amount 50.000 Range 60 - 125 Recovery = 61.62% 21) 2-Butanone-d5 4.18 46 201291 102.53 ug/L 0.00 Spiked Amount 100.000 Range 40 - 130 Recovery = 102.53% 24) Chloroform-d 4.65 84 208332 44.33 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 88.66% 26) 1,2-Dichloroethane-d4 5.31 65 142019 43.45 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 86.90% 32) Benzene-d6 5.35 84 458609 46.36 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 92.72% 36) 1,2-Dichloropropane-d6 6.34 67 151216 45.64 ug/L 0.00 Spiked Amount 50.000 Range 70 - 120 Recovery = 91.28% 41) Toluene-d8 7.57 98 411551 45.13 ug/L 0.00 Spiked Amount 50.000 Range 80 - 120 Recovery = 90.26% 43) trans-1,3-Dichloropropene- 7.85 79 60942 42.72 ug/L 0.00 Spiked Amount 50.000 Range 60 - 125 Recovery = 85.44% 47) 2-Hexanone-d5 8.31 63 144334 114.71 ug/L 0.00 Spiked Amount 100.000 Range 45 - 130 Recovery = 114.71% 57) 1,1,2,2-Tetrachloroethane- 10.44 84 199752 46.61 ug/L 0.00 Spiked Amount 50.000 Range 65 - 120 Recovery = 93.22% 64) 1,2-Dichlorobenzene-d4 11.86 152 173289 47.27 ug/L 0.00 Spiked Amount 50.000 Range 80 - 120 Recovery = 94.54% Target Compounds Qvalue 29) Cyclohexane 5.00 56 15472 2.84 ug/L # 54 35) Methylcyclohexane 6.42 83 13734 2.64 ug/L 91 42) Toluene 7.64 91 326036 24.21 ug/L 100 52) Ethylbenzene 9.26 91 46997 3.22 ug/L 96 53) m,p-Xylene 9.38 106 64389 11.56 ug/L 98 54) o-xylene 9.78 106 30141 5.71 ug/L 96 56) Isopropylbenzene 10.17 105 17186 1.24 ug/L 98 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed