LSC Area Percent Report Data Path : W:\HPCHEM1\MSVOA_U\DATA\VU050618\ Data File : VU023691.D Acq On : 06 May 2018 15:30 Operator : MD/SY Sample : J2721-04DL 200X Misc : 5.36g/5.0mL/100ul/5.0mL/MSVOA_U/MEOH ALS Vial : 11 Sample Multiplier: 1 Integration Parameters: LSCINT.P Integrator: RTE Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 0 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Method : W:\HPCHEM1\MSVOA_U\METHOD\SOMULM050118WMA.M Title : VOC Analysis Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total --- ----- ----- ---- ---- --- ------- ------- ------ ------- 1 1.089 135 155 178 rBV 1358952 1524533 100.00% 9.461% 2 1.182 180 184 191 rVB 8023 8100 0.53% 0.050% 3 1.397 245 251 267 rVB 173350 178465 11.71% 1.107% 4 1.680 331 339 357 rVB 131225 165138 10.83% 1.025% 5 2.272 512 523 536 rBV 294962 447979 29.38% 2.780% 6 2.613 625 629 639 rVB2 486 941 0.06% 0.006% 7 2.703 651 657 659 rBV2 628 639 0.04% 0.004% 8 2.838 690 699 711 rVB2 1311 2627 0.17% 0.016% 9 3.002 741 750 758 rBV4 1151 1840 0.12% 0.011% 10 3.307 835 845 857 rBV5 4117 8260 0.54% 0.051% 11 4.098 1080 1091 1102 rBV7 2799 6367 0.42% 0.040% 12 4.178 1102 1116 1144 rBV 122890 321350 21.08% 1.994% 13 4.384 1176 1180 1183 rBV4 390 398 0.03% 0.002% 14 4.651 1246 1263 1284 rBV 209474 493686 32.38% 3.064% 15 4.895 1329 1339 1344 rBV2 668 1289 0.08% 0.008% 16 4.992 1352 1369 1385 rBV2 69020 158371 10.39% 0.983% 17 5.082 1386 1397 1419 rVB3 21224 52801 3.46% 0.328% 18 5.223 1424 1441 1456 rBV2 110114 260068 17.06% 1.614% 19 5.342 1457 1478 1509 rVV2 441949 1324132 86.85% 8.217% 20 5.487 1513 1523 1535 rVV3 25582 58689 3.85% 0.364% 21 5.558 1539 1545 1556 rVV3 13868 27371 1.80% 0.170% 22 5.625 1557 1566 1583 rVB4 16158 34913 2.29% 0.217% 23 5.786 1599 1616 1635 rBV 181315 361354 23.70% 2.242% 24 5.889 1635 1648 1699 rVB 452063 933547 61.23% 5.793% 25 6.120 1715 1720 1730 rVB3 678 972 0.06% 0.006% 26 6.182 1730 1739 1745 rBV2 2109 3601 0.24% 0.022% 27 6.275 1757 1768 1773 rBV2 5005 8640 0.57% 0.054% 28 6.336 1774 1787 1801 rBV 287095 573450 37.61% 3.559% 29 6.535 1841 1849 1862 rVB3 12880 23886 1.57% 0.148% 30 6.645 1873 1883 1893 rVB3 6773 12894 0.85% 0.080% 31 6.735 1899 1911 1924 rVB6 8136 18332 1.20% 0.114% 32 6.863 1943 1951 1956 rBV4 877 1347 0.09% 0.008% 33 6.908 1956 1965 1982 rVB6 3920 9328 0.61% 0.058% 34 7.047 2002 2008 2010 rBV4 917 864 0.06% 0.005% 35 7.108 2018 2027 2036 rBV2 7081 12533 0.82% 0.078% 36 7.185 2042 2051 2056 rBV 25007 39941 2.62% 0.248% 37 7.230 2056 2065 2083 rVB 163958 293522 19.25% 1.821% 38 7.346 2093 2101 2124 rVB2 22697 51463 3.38% 0.319% 39 7.567 2148 2170 2182 rBV 612069 1089362 71.46% 6.760% 40 7.641 2183 2193 2210 rVB 427612 742415 48.70% 4.607% 41 7.854 2240 2259 2271 rBV2 105666 223521 14.66% 1.387% 42 8.050 2313 2320 2329 rVB4 3138 5001 0.33% 0.031% 43 8.230 2369 2376 2387 rVB3 1859 2707 0.18% 0.017% 44 8.313 2389 2402 2438 rBV 407803 716323 46.99% 4.445% 45 8.548 2465 2475 2484 rVB2 10322 17695 1.16% 0.110% 46 8.609 2486 2494 2504 rBV2 6075 9684 0.64% 0.060% 47 8.760 2533 2541 2547 rVB5 930 1007 0.07% 0.006% 48 8.815 2552 2558 2564 rBV3 3453 4979 0.33% 0.031% 49 8.915 2580 2589 2599 rVB3 7309 12577 0.82% 0.078% 50 9.037 2618 2627 2632 rBV4 5471 8351 0.55% 0.052% 51 9.091 2632 2644 2672 rVV 631483 1071486 70.28% 6.649% 52 9.255 2684 2695 2713 rVB 66605 107480 7.05% 0.667% 53 9.378 2719 2733 2748 rBV 226905 380559 24.96% 2.362% 54 9.448 2748 2755 2768 rVB2 14901 23134 1.52% 0.144% 55 9.722 2833 2840 2847 rBV5 2115 3309 0.22% 0.021% 56 9.783 2848 2859 2880 rVB 111710 181301 11.89% 1.125% 57 9.956 2902 2913 2924 rVB6 3829 6861 0.45% 0.043% 58 10.050 2933 2942 2949 rBV4 3904 5628 0.37% 0.035% 59 10.098 2951 2957 2964 rVB6 1334 1819 0.12% 0.011% 60 10.172 2969 2980 2992 rBV2 26761 40958 2.69% 0.254% 61 10.259 3001 3007 3011 rBV2 1195 1403 0.09% 0.009% 62 10.329 3018 3029 3033 rBV6 2278 3861 0.25% 0.024% 63 10.435 3049 3062 3078 rBV 406191 640549 42.02% 3.975% 64 10.593 3100 3111 3124 rBV 60373 93730 6.15% 0.582% 65 10.683 3128 3139 3158 rVV 134317 298399 19.57% 1.852% 66 10.776 3158 3168 3176 rVV 52926 84764 5.56% 0.526% 67 10.818 3176 3181 3191 rVB2 18784 25708 1.69% 0.160% 68 10.924 3207 3214 3220 rBV4 1223 1908 0.13% 0.012% 69 10.976 3220 3230 3250 rVB 50294 80514 5.28% 0.500% 70 11.152 3267 3285 3299 rBV 190346 298490 19.58% 1.852% 71 11.291 3317 3328 3329 rBV7 2285 2996 0.20% 0.019% 72 11.333 3336 3341 3353 rVB7 3247 4785 0.31% 0.030% 73 11.403 3354 3363 3365 rBV5 2828 4052 0.27% 0.025% 74 11.432 3368 3372 3377 rVB3 3512 3743 0.25% 0.023% 75 11.487 3377 3389 3407 rBV 712332 1120800 73.52% 6.955% 76 11.574 3407 3416 3426 rBV 40773 59950 3.93% 0.372% 77 11.667 3440 3445 3449 rBV4 971 1209 0.08% 0.008% 78 11.705 3450 3457 3465 rVB4 2921 4291 0.28% 0.027% 79 11.776 3469 3479 3484 rBV4 9512 16471 1.08% 0.102% 80 11.812 3486 3490 3495 rVV2 12663 16503 1.08% 0.102% 81 11.863 3495 3506 3526 rVB 649012 1062222 69.68% 6.592% 82 12.027 3549 3557 3564 rBV2 18313 26822 1.76% 0.166% 83 12.152 3587 3596 3600 rBV 11564 16981 1.11% 0.105% 84 12.255 3616 3628 3637 rBV 23547 35366 2.32% 0.219% 85 12.361 3654 3661 3666 rBV4 3782 6003 0.39% 0.037% 86 12.554 3714 3721 3733 rVB4 5351 8334 0.55% 0.052% 87 12.615 3733 3740 3744 rBV5 1475 2074 0.14% 0.013% 88 12.654 3744 3752 3760 rVV2 13117 19159 1.26% 0.119% 89 12.705 3760 3768 3778 rVV 18946 27052 1.77% 0.168% 90 12.795 3790 3796 3800 rBV4 1264 1411 0.09% 0.009% 91 12.831 3801 3807 3810 rBV5 1744 2002 0.13% 0.012% 92 12.969 3841 3850 3859 rVB4 6517 8738 0.57% 0.054% 93 13.040 3866 3872 3878 rBV5 1195 1524 0.10% 0.009% 94 13.101 3881 3891 3892 rBV4 1975 2952 0.19% 0.018% 95 13.127 3892 3899 3911 rVB4 16776 26028 1.71% 0.162% 96 13.242 3930 3935 3942 rVB4 2128 2631 0.17% 0.016% 97 13.284 3942 3948 3956 rBV6 1422 2031 0.13% 0.013% 98 13.516 4013 4020 4027 rBV5 2967 5075 0.33% 0.031% 99 13.750 4086 4093 4106 rVB 8559 13315 0.87% 0.083% 100 14.101 4199 4202 4207 rBV2 749 755 0.05% 0.005% Sum of corrected areas: 16114389