Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_U\DATA\VU050618\ Data File : VU023692.D Acq On : 06 May 2018 15:57 Operator : MD/SY Sample : J2691-02ME Misc : 6.36g/5.0mL/100ul/5.0mL/MSVOA_U/MEOH ALS Vial : 12 Sample Multiplier: 1 Quant Time: May 07 01:58:54 2018 Quant Method : W:\HPCHEM1\MSVOA_U\METHOD\SOMULM050118WMA.M Quant Title : VOC Analysis QLast Update : Mon May 07 00:51:10 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) 1,4-Difluorobenzene 5.89 114 395593 50.00 ug/L 0.00 28) Chlorobenzene-d5 9.10 117 386438 50.00 ug/L 0.00 60) 1,4-Dichlorobenzene-d4 11.49 152 210561 50.00 ug/L 0.00 System Monitoring Compounds 4) Vinyl Chloride-d3 1.39 65 107975 38.51 ug/L 0.00 Spiked Amount 50.000 Range 60 - 135 Recovery = 77.02% 7) Chloroethane-d5 1.64 69 54303 25.41 ug/L -0.04 Spiked Amount 50.000 Range 70 - 130 Recovery = 50.82%# 11) 1,1-Dichloroethene-d2 2.23 63 145632 26.64 ug/L -0.04 Spiked Amount 50.000 Range 60 - 125 Recovery = 53.28%# 21) 2-Butanone-d5 4.19 46 200033 103.26 ug/L 0.02 Spiked Amount 100.000 Range 40 - 130 Recovery = 103.26% 24) Chloroform-d 4.65 84 188728 40.70 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 81.40% 26) 1,2-Dichloroethane-d4 5.31 65 133982 41.55 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 83.10% 32) Benzene-d6 5.34 84 422075 40.71 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 81.42% 36) 1,2-Dichloropropane-d6 6.33 67 143235 41.24 ug/L 0.00 Spiked Amount 50.000 Range 70 - 120 Recovery = 82.48% 41) Toluene-d8 7.57 98 392153 41.03 ug/L 0.00 Spiked Amount 50.000 Range 80 - 120 Recovery = 82.06% 43) trans-1,3-Dichloropropene- 7.85 79 60532 40.49 ug/L 0.00 Spiked Amount 50.000 Range 60 - 125 Recovery = 80.98% 47) 2-Hexanone-d5 8.33 63 156791 118.89 ug/L 0.01 Spiked Amount 100.000 Range 45 - 130 Recovery = 118.89% 57) 1,1,2,2-Tetrachloroethane- 10.44 84 212059 47.21 ug/L 0.00 Spiked Amount 50.000 Range 65 - 120 Recovery = 94.42% 64) 1,2-Dichlorobenzene-d4 11.87 152 179996 43.82 ug/L 0.00 Spiked Amount 50.000 Range 80 - 120 Recovery = 87.64% Target Compounds Qvalue 35) Methylcyclohexane 6.41 83 20627 3.78 ug/L 93 42) Toluene 7.64 91 167320 11.85 ug/L 99 52) Ethylbenzene 9.26 91 47834 3.13 ug/L 99 53) m,p-Xylene 9.38 106 88707 15.20 ug/L 97 54) o-xylene 9.79 106 50474 9.13 ug/L 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed