LSC Area Percent Report Data Path : W:\HPCHEM1\MSVOA_U\DATA\VU050618\ Data File : VU023692.D Acq On : 06 May 2018 15:57 Operator : MD/SY Sample : J2691-02ME Misc : 6.36g/5.0mL/100ul/5.0mL/MSVOA_U/MEOH ALS Vial : 12 Sample Multiplier: 1 Integration Parameters: LSCINT.P Integrator: RTE Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 0 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Method : W:\HPCHEM1\MSVOA_U\METHOD\SOMULM050118WMA.M Title : VOC Analysis Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total --- ----- ----- ---- ---- --- ------- ------- ------ ------- 1 1.082 133 153 175 rBV 1121201 1271896 100.00% 7.712% 2 1.175 177 182 190 rVV 6341 6993 0.55% 0.042% 3 1.268 205 211 223 rBV2 8630 13393 1.05% 0.081% 4 1.394 242 250 271 rVB 134055 177247 13.94% 1.075% 5 1.606 288 316 317 rBV10 16769 48426 3.81% 0.294% 6 1.641 320 327 342 rVV 79340 119499 9.40% 0.725% 7 2.233 500 511 526 rBV 242900 376524 29.60% 2.283% 8 2.831 685 697 713 rBV2 6129 13280 1.04% 0.081% 9 4.194 1105 1121 1170 rBV 89517 319815 25.14% 1.939% 10 4.648 1242 1262 1293 rBV 180268 462631 36.37% 2.805% 11 4.976 1350 1364 1381 rBV6 7742 18153 1.43% 0.110% 12 5.207 1423 1436 1454 rBV3 8871 22220 1.75% 0.135% 13 5.333 1454 1475 1509 rVV2 422108 1225125 96.32% 7.428% 14 5.471 1509 1518 1531 rVB8 4754 11834 0.93% 0.072% 15 5.615 1552 1563 1578 rVB6 8234 19383 1.52% 0.118% 16 5.776 1597 1613 1627 rVB2 18837 36934 2.90% 0.224% 17 5.886 1632 1647 1686 rBV 418928 909666 71.52% 5.516% 18 6.181 1728 1739 1748 rBV10 3928 8044 0.63% 0.049% 19 6.252 1750 1761 1772 rVV5 3888 9136 0.72% 0.055% 20 6.333 1772 1786 1800 rVV 258214 556112 43.72% 3.372% 21 6.410 1801 1810 1823 rVV2 51827 116485 9.16% 0.706% 22 6.471 1823 1829 1838 rVV7 4732 8949 0.70% 0.054% 23 6.532 1838 1848 1859 rVB4 4717 9633 0.76% 0.058% 24 6.734 1898 1911 1922 rBV5 7945 16310 1.28% 0.099% 25 6.898 1944 1962 1973 rBV7 9907 20752 1.63% 0.126% 26 7.178 2034 2049 2055 rBV3 15130 26932 2.12% 0.163% 27 7.230 2055 2065 2085 rVB 135449 267960 21.07% 1.625% 28 7.342 2091 2100 2110 rBV2 8623 14357 1.13% 0.087% 29 7.567 2146 2170 2183 rBV 558242 1054559 82.91% 6.394% 30 7.638 2183 2192 2207 rVB 205552 375651 29.53% 2.278% 31 7.821 2240 2249 2252 rVV 30587 43331 3.41% 0.263% 32 7.853 2252 2259 2272 rVV 90018 178971 14.07% 1.085% 33 7.918 2272 2279 2293 rVB3 16382 29331 2.31% 0.178% 34 8.050 2307 2320 2332 rBV4 7436 13253 1.04% 0.080% 35 8.326 2393 2406 2436 rBV 405147 773881 60.84% 4.692% 36 8.545 2465 2474 2484 rVB 15993 26323 2.07% 0.160% 37 8.609 2484 2494 2504 rBV2 10125 17724 1.39% 0.107% 38 8.850 2564 2569 2579 rVV4 6381 13273 1.04% 0.080% 39 8.911 2580 2588 2599 rVB4 9292 16697 1.31% 0.101% 40 9.033 2617 2626 2633 rBV2 7273 11848 0.93% 0.072% 41 9.098 2633 2646 2669 rVV 627136 1132887 89.07% 6.869% 42 9.255 2684 2695 2709 rBV 66571 114119 8.97% 0.692% 43 9.381 2719 2734 2747 rBV 302618 531494 41.79% 3.223% 44 9.445 2747 2754 2772 rVB2 22746 38626 3.04% 0.234% 45 9.721 2825 2840 2848 rVV9 9357 19672 1.55% 0.119% 46 9.786 2848 2860 2879 rVV 179833 309395 24.33% 1.876% 47 9.956 2904 2913 2922 rVB3 13606 21873 1.72% 0.133% 48 10.049 2935 2942 2948 rVV5 9343 15685 1.23% 0.095% 49 10.091 2949 2955 2967 rVB3 11333 19326 1.52% 0.117% 50 10.172 2967 2980 2989 rBV3 8120 16287 1.28% 0.099% 51 10.258 3002 3007 3016 rVV4 5867 8530 0.67% 0.052% 52 10.326 3016 3028 3033 rVV8 6593 11831 0.93% 0.072% 53 10.358 3034 3038 3051 rVB5 8229 16513 1.30% 0.100% 54 10.438 3051 3063 3076 rBV 425287 705653 55.48% 4.279% 55 10.493 3076 3080 3088 rVB5 12100 16463 1.29% 0.100% 56 10.596 3104 3112 3119 rBV 8691 13222 1.04% 0.080% 57 10.689 3132 3141 3155 rVV2 31296 68346 5.37% 0.414% 58 10.776 3155 3168 3173 rVV4 28153 53360 4.20% 0.324% 59 10.818 3173 3181 3191 rVB2 73838 109755 8.63% 0.665% 60 10.975 3222 3230 3237 rBV3 16832 27587 2.17% 0.167% 61 11.078 3252 3262 3267 rBV5 10741 16865 1.33% 0.102% 62 11.117 3267 3274 3279 rVV2 30612 43160 3.39% 0.262% 63 11.152 3279 3285 3295 rVB 67051 103071 8.10% 0.625% 64 11.278 3314 3324 3329 rBV4 14992 27068 2.13% 0.164% 65 11.397 3353 3361 3368 rBV4 20847 35340 2.78% 0.214% 66 11.490 3379 3390 3409 rVV 805265 1258044 98.91% 7.628% 67 11.577 3410 3417 3423 rVV2 37757 50781 3.99% 0.308% 68 11.615 3424 3429 3440 rVV4 14727 26651 2.10% 0.162% 69 11.670 3441 3446 3452 rVV4 13034 16503 1.30% 0.100% 70 11.705 3452 3457 3470 rVB7 16932 27431 2.16% 0.166% 71 11.786 3472 3482 3486 rBV5 25169 42014 3.30% 0.255% 72 11.815 3487 3491 3496 rVV 28116 33934 2.67% 0.206% 73 11.866 3496 3507 3525 rVB 714069 1198519 94.23% 7.267% 74 12.027 3549 3557 3565 rBV2 87284 130090 10.23% 0.789% 75 12.152 3588 3596 3599 rBV 22685 29588 2.33% 0.179% 76 12.184 3600 3606 3614 rVV5 33192 55200 4.34% 0.335% 77 12.255 3614 3628 3637 rVB2 60310 121148 9.52% 0.735% 78 12.368 3653 3663 3668 rBV5 33820 65291 5.13% 0.396% 79 12.506 3697 3706 3715 rBV8 20545 44386 3.49% 0.269% 80 12.618 3731 3741 3745 rBV7 37236 63360 4.98% 0.384% 81 12.654 3746 3752 3761 rVB4 66607 103737 8.16% 0.629% 82 12.708 3761 3769 3787 rBV5 52071 120186 9.45% 0.729% 83 12.789 3787 3794 3801 rBV2 42434 62500 4.91% 0.379% 84 12.885 3820 3824 3828 rBV2 7288 9024 0.71% 0.055% 85 12.969 3844 3850 3863 rVB2 38529 60322 4.74% 0.366% 86 13.040 3864 3872 3880 rBV6 21933 39315 3.09% 0.238% 87 13.091 3881 3888 3891 rBV3 20072 27172 2.14% 0.165% 88 13.130 3892 3900 3908 rBV3 106920 166993 13.13% 1.013% 89 13.242 3928 3935 3941 rBV 31362 43757 3.44% 0.265% 90 13.287 3942 3949 3980 rVB 44544 149025 11.72% 0.904% 91 13.413 3982 3988 3996 rVB5 16329 23891 1.88% 0.145% 92 13.461 3996 4003 4010 rBV4 25080 33845 2.66% 0.205% 93 13.512 4011 4019 4025 rBV3 44591 69997 5.50% 0.424% 94 13.641 4054 4059 4066 rVB2 21656 27739 2.18% 0.168% 95 13.744 4084 4091 4100 rVB3 39038 68251 5.37% 0.414% 96 13.795 4100 4107 4115 rVB7 21491 30317 2.38% 0.184% 97 14.143 4208 4215 4223 rBV4 34709 54838 4.31% 0.332% 98 14.348 4270 4279 4291 rVB10 23780 46406 3.65% 0.281% 99 15.856 4743 4748 4758 rVB4 18528 27744 2.18% 0.168% 100 16.203 4851 4856 4867 rVB6 16567 26055 2.05% 0.158% Sum of corrected areas: 16492713