Data Path : W:\HPCHEM1\MSVOA_U\Data\VU050618\ Quantitation Report (LSC Reviewed) Data File : VU023693.D Acq On : 06 May 2018 16:23 Operator : MD/SY Sample : J2691-22ME Misc : 2.94g/5.0mL/100ul/5.0mL/MSVOA_U/MEOH ALS Vial : 13 Sample Multiplier: 1 Quant Time: May 22 18:29:04 2018 Quant Method : W:\HPCHEM1\MSVOA_U\METHOD\SOMULM050118WMA.M Quant Title : VOC Analysis QLast Update : Mon May 07 00:51:10 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) 1,4-Difluorobenzene 5.89 114 414018 50.00 ug/L 0.00 28) Chlorobenzene-d5 9.10 117 403549 50.00 ug/L 0.00 60) 1,4-Dichlorobenzene-d4 11.49 152 219379 50.00 ug/L 0.00 System Monitoring Compounds 4) Vinyl Chloride-d3 1.39 65 111621 38.04 ug/L 0.00 Spiked Amount 50.000 Range 60 - 135 Recovery = 76.08% 7) Chloroethane-d5 1.64 69 53240 23.80 ug/L -0.04 Spiked Amount 50.000 Range 70 - 130 Recovery = 47.60%# 11) 1,1-Dichloroethene-d2 2.23 63 150735 26.35 ug/L -0.05 Spiked Amount 50.000 Range 60 - 125 Recovery = 52.70%# 21) 2-Butanone-d5 4.20 46 235944 116.38 ug/L 0.02 Spiked Amount 100.000 Range 40 - 130 Recovery = 116.38% 24) Chloroform-d 4.65 84 189440 39.04 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 78.08% 26) 1,2-Dichloroethane-d4 5.31 65 135856 40.25 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 80.50% 32) Benzene-d6 5.34 84 434729 40.15 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 80.30% 36) 1,2-Dichloropropane-d6 6.33 67 145586 40.14 ug/L 0.00 Spiked Amount 50.000 Range 70 - 120 Recovery = 80.28% 41) Toluene-d8 7.57 98 448045 44.89 ug/L 0.00 Spiked Amount 50.000 Range 80 - 120 Recovery = 89.78% 43) trans-1,3-Dichloropropene- 7.86 79 61033 39.09 ug/L 0.00 Spiked Amount 50.000 Range 60 - 125 Recovery = 78.18% 47) 2-Hexanone-d5 8.33 63 192729 139.94 ug/L 0.02 Spiked Amount 100.000 Range 45 - 130 Recovery = 139.94%# 57) 1,1,2,2-Tetrachloroethane- 10.44 84 223696 47.69 ug/L 0.00 Spiked Amount 50.000 Range 65 - 120 Recovery = 95.38% 64) 1,2-Dichlorobenzene-d4 11.87 152 182686 42.69 ug/L 0.00 Spiked Amount 50.000 Range 80 - 120 Recovery = 85.38% Target Compounds Qvalue 29) Cyclohexane 4.98 56 236793 39.70 ug/L # 83 35) Methylcyclohexane 6.41 83 1707966 299.70 ug/L 98 42) Toluene 7.64 91 18319699m 1242.91 ug/L 52) Ethylbenzene 9.26 91 19439813m 1216.73 ug/L 53) m,p-Xylene 9.39 106 18088517m 2968.27 ug/L 54) o-xylene 9.79 106 6897358 1194.63 ug/L 94 56) Isopropylbenzene 10.17 105 601648 39.70 ug/L 100 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed