LSC Area Percent Report Data Path : W:\HPCHEM1\MSVOA_U\DATA\VU050618\ Data File : VU023693.D Acq On : 06 May 2018 16:23 Operator : MD/SY Sample : J2691-22ME Misc : 2.94g/5.0mL/100ul/5.0mL/MSVOA_U/MEOH ALS Vial : 13 Sample Multiplier: 1 Integration Parameters: LSCINT.P Integrator: RTE Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 0 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Method : W:\HPCHEM1\MSVOA_U\METHOD\SOMULM050118WMA.M Title : VOC Analysis Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total --- ----- ----- ---- ---- --- ------- ------- ------ ------- 1 1.082 134 153 175 rBV 1209214 1390789 1.30% 0.196% 2 3.272 816 834 859 rVV 317496 674206 0.63% 0.095% 3 4.976 1343 1364 1380 rBV4 679627 1668889 1.56% 0.235% 4 5.207 1417 1436 1457 rBV 662187 1682522 1.57% 0.237% 5 5.333 1458 1475 1501 rVB2 450465 1269276 1.18% 0.179% 6 5.471 1501 1518 1530 rBV2 275447 632194 0.59% 0.089% 7 5.616 1551 1563 1595 rVB 437176 988651 0.92% 0.139% 8 5.776 1595 1613 1634 rBV 2646005 5177348 4.82% 0.730% 9 5.889 1634 1648 1677 rVB 437083 966437 0.90% 0.136% 10 6.333 1775 1786 1794 rVV 258984 534950 0.50% 0.075% 11 6.410 1794 1810 1823 rVV 3882516 8529701 7.95% 1.203% 12 6.529 1838 1847 1860 rVB2 363972 692184 0.65% 0.098% 13 6.638 1870 1881 1894 rVB 267743 503880 0.47% 0.071% 14 6.734 1894 1911 1928 rVB3 519577 1138590 1.06% 0.161% 15 6.902 1948 1963 1987 rVB3 519208 1086378 1.01% 0.153% 16 7.101 2015 2025 2033 rBV 296146 538294 0.50% 0.076% 17 7.178 2034 2049 2057 rBV 1511112 2741927 2.56% 0.387% 18 7.220 2058 2062 2080 rVB4 531869 978272 0.91% 0.138% 19 7.339 2090 2099 2119 rVB 1055475 2240564 2.09% 0.316% 20 7.529 2143 2158 2165 rBV2 1696565 3376348 3.15% 0.476% 21 7.648 2180 2195 2208 rBV2 24536151 46420890 43.26% 6.546% 22 7.821 2239 2249 2268 rVB 4461106 7278928 6.78% 1.026% 23 7.918 2269 2279 2301 rVB2 995106 1876137 1.75% 0.265% 24 8.046 2305 2319 2330 rBV 460165 839535 0.78% 0.118% 25 8.230 2365 2376 2389 rVB 296696 508118 0.47% 0.072% 26 8.332 2389 2408 2431 rBV 1052309 2123951 1.98% 0.299% 27 8.458 2433 2447 2451 rBV 485774 849009 0.79% 0.120% 28 8.548 2465 2475 2485 rVB 1136609 1924837 1.79% 0.271% 29 8.609 2485 2494 2503 rBV 645205 1104080 1.03% 0.156% 30 8.818 2549 2559 2564 rVV 433324 735732 0.69% 0.104% 31 8.853 2564 2570 2580 rVV3 493803 1206673 1.12% 0.170% 32 8.911 2580 2588 2602 rVB3 1492331 2577045 2.40% 0.363% 33 9.033 2615 2626 2637 rBV 1161601 1941511 1.81% 0.274% 34 9.101 2637 2647 2659 rVB 604088 1071965 1.00% 0.151% 35 9.265 2682 2698 2720 rVV2 27616987 51888935 48.36% 7.317% 36 9.397 2721 2739 2749 rVV3 53983565 107306900 100.00% 15.131% 37 9.448 2749 2755 2782 rVB2 2743089 4551260 4.24% 0.642% 38 9.725 2827 2841 2849 rBV4 779501 1555231 1.45% 0.219% 39 9.792 2849 2862 2883 rVB 24170198 40874530 38.09% 5.764% 40 9.956 2894 2913 2923 rBV3 1099883 2208942 2.06% 0.311% 41 10.049 2934 2942 2950 rVV3 972692 1858396 1.73% 0.262% 42 10.094 2950 2956 2967 rVB2 722540 1178245 1.10% 0.166% 43 10.175 2968 2981 2990 rBV 962177 1729883 1.61% 0.244% 44 10.262 3001 3008 3016 rVV2 523831 943138 0.88% 0.133% 45 10.326 3016 3028 3033 rVV3 695601 1378031 1.28% 0.194% 46 10.358 3034 3038 3053 rVB2 766091 1229791 1.15% 0.173% 47 10.458 3053 3069 3075 rBV3 1014629 2252441 2.10% 0.318% 48 10.496 3076 3081 3091 rVB4 659726 980905 0.91% 0.138% 49 10.596 3102 3112 3120 rBV 1238368 1951314 1.82% 0.275% 50 10.689 3131 3141 3156 rVV 4339540 9472472 8.83% 1.336% 51 10.779 3156 3169 3175 rVV2 2975166 5794294 5.40% 0.817% 52 10.821 3175 3182 3192 rVB 4708067 6817195 6.35% 0.961% 53 10.979 3222 3231 3239 rBV 1907167 3076080 2.87% 0.434% 54 11.078 3255 3262 3268 rBV4 362952 498964 0.46% 0.070% 55 11.120 3268 3275 3278 rBV 1397264 1743373 1.62% 0.246% 56 11.159 3278 3287 3298 rVB 9488059 14788711 13.78% 2.085% 57 11.300 3313 3331 3335 rBV2 695897 1877876 1.75% 0.265% 58 11.336 3337 3342 3353 rVV3 1078953 2125845 1.98% 0.300% 59 11.403 3354 3363 3368 rVV3 1068514 1939660 1.81% 0.274% 60 11.435 3368 3373 3382 rVV 1337970 2287878 2.13% 0.323% 61 11.487 3382 3389 3397 rVV3 1478309 2552899 2.38% 0.360% 62 11.538 3398 3405 3409 rVV2 926092 1468748 1.37% 0.207% 63 11.577 3409 3417 3425 rVV 5487446 8672339 8.08% 1.223% 64 11.615 3426 3429 3440 rVV 1062476 1557838 1.45% 0.220% 65 11.673 3441 3447 3451 rVV2 430080 673080 0.63% 0.095% 66 11.709 3451 3458 3468 rVV2 1001817 1628250 1.52% 0.230% 67 11.786 3469 3482 3485 rVV2 3360297 5749198 5.36% 0.811% 68 11.818 3486 3492 3500 rVV 8276157 12517488 11.67% 1.765% 69 11.885 3500 3513 3527 rVB3 14343426 30143441 28.09% 4.250% 70 11.988 3537 3545 3551 rBV 919842 1416963 1.32% 0.200% 71 12.033 3551 3559 3563 rVV 3828439 5309238 4.95% 0.749% 72 12.062 3564 3568 3586 rVB 5098485 7454228 6.95% 1.051% 73 12.155 3586 3597 3602 rBV 8954601 14617988 13.62% 2.061% 74 12.188 3602 3607 3616 rVB 10427347 14378160 13.40% 2.027% 75 12.262 3617 3630 3639 rBV 17358197 26432882 24.63% 3.727% 76 12.393 3653 3671 3691 rBV6 4161235 14675787 13.68% 2.069% 77 12.503 3692 3705 3713 rBV4 2204206 4245263 3.96% 0.599% 78 12.561 3713 3723 3733 rVB 6249564 10201294 9.51% 1.438% 79 12.660 3733 3754 3762 rBV 14525110 25580823 23.84% 3.607% 80 12.715 3762 3771 3787 rVB 21207717 32811671 30.58% 4.627% 81 12.792 3787 3795 3801 rBV 3406634 5188943 4.84% 0.732% 82 12.827 3801 3806 3811 rVV 2578469 3403405 3.17% 0.480% 83 12.860 3811 3816 3823 rVB 3389695 4179740 3.90% 0.589% 84 12.972 3842 3851 3863 rVB2 7964945 12293816 11.46% 1.734% 85 13.040 3863 3872 3879 rBV2 2566755 3607472 3.36% 0.509% 86 13.091 3879 3888 3892 rVV3 3889345 5908845 5.51% 0.833% 87 13.133 3893 3901 3927 rVB3 17539826 34625030 32.27% 4.882% 88 13.242 3927 3935 3944 rBV 3551063 5113354 4.77% 0.721% 89 13.297 3945 3952 3960 rVV4 646626 1022328 0.95% 0.144% 90 13.413 3979 3988 3996 rBV2 1073905 1768396 1.65% 0.249% 91 13.461 3997 4003 4010 rVB 524333 676120 0.63% 0.095% 92 13.516 4010 4020 4026 rBV3 4775702 8075236 7.53% 1.139% 93 13.644 4047 4060 4071 rVB2 2137003 3774726 3.52% 0.532% 94 13.750 4082 4093 4102 rVV 7749081 12192334 11.36% 1.719% 95 13.792 4102 4106 4117 rVB 547327 759258 0.71% 0.107% 96 13.969 4149 4161 4170 rBV4 568005 1234228 1.15% 0.174% 97 14.152 4208 4218 4234 rBV2 725152 1387037 1.29% 0.196% 98 14.345 4267 4278 4291 rBV4 409430 912226 0.85% 0.129% 99 14.483 4312 4321 4330 rBV 329026 527205 0.49% 0.074% 100 14.879 4435 4444 4456 rBV 513333 871439 0.81% 0.123% Sum of corrected areas: 709188817