LSC Area Percent Report Data Path : W:\HPCHEM1\MSVOA_U\DATA\VU050718\ Data File : VU023706.D Acq On : 07 May 2018 11:04 Operator : MD/SY Sample : VU0507MBL01 Misc : 5.00g/5mL/100uL/5.0mL/MSVOA_U/MEOH ALS Vial : 3 Sample Multiplier: 1 Integration Parameters: LSCINT.P Integrator: RTE Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 0 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Method : W:\HPCHEM1\MSVOA_U\METHOD\SOMULM050118WMA.M Title : VOC Analysis Signal : TIC: VU023683.D peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total --- ----- ----- ---- ---- --- ------- ------- ------ ------- 1 0.664 18 23 30 rBV 153 173 0.01% 0.001% 2 0.706 33 36 38 rBV2 168 121 0.01% 0.001% 3 0.838 71 77 80 rBV2 227 278 0.02% 0.002% 4 0.934 104 107 111 rVB 196 128 0.01% 0.001% 5 0.989 119 124 130 rVB2 153 209 0.01% 0.002% 6 1.021 130 134 136 rBV2 153 128 0.01% 0.001% 7 1.088 136 155 179 rBV 1510754 1689053 100.00% 13.972% 8 1.185 181 185 191 rVB2 6485 6260 0.37% 0.052% 9 1.400 245 252 281 rVB 179667 186977 11.07% 1.547% 10 1.680 331 339 356 rVB 135449 171632 10.16% 1.420% 11 2.191 494 498 505 rVB5 3350 4338 0.26% 0.036% 12 2.275 512 524 538 rBV 285052 436576 25.85% 3.611% 13 2.481 580 588 598 rBV3 1495 2415 0.14% 0.020% 14 2.619 624 631 636 rBV2 635 728 0.04% 0.006% 15 2.703 651 657 664 rBV2 1005 1197 0.07% 0.010% 16 2.838 692 699 710 rVB2 1352 2358 0.14% 0.020% 17 2.895 710 717 720 rBV2 220 276 0.02% 0.002% 18 2.982 740 744 745 rBV 322 184 0.01% 0.002% 19 3.034 754 760 762 rBV 176 194 0.01% 0.002% 20 3.162 797 800 804 rVB 165 129 0.01% 0.001% 21 3.272 831 834 839 rVB2 177 152 0.01% 0.001% 22 3.400 864 874 881 rVB3 399 643 0.04% 0.005% 23 3.439 881 886 892 rBV2 208 268 0.02% 0.002% 24 3.471 892 896 900 rBV2 134 144 0.01% 0.001% 25 3.545 915 919 921 rBV2 194 136 0.01% 0.001% 26 3.600 930 936 938 rBV2 188 185 0.01% 0.002% 27 3.645 945 950 952 rBV 151 128 0.01% 0.001% 28 3.677 956 960 963 rBV2 97 99 0.01% 0.001% 29 3.735 975 978 981 rVB 187 99 0.01% 0.001% 30 3.760 981 986 992 rBV2 177 217 0.01% 0.002% 31 3.802 996 999 1001 rVV 176 99 0.01% 0.001% 32 3.979 1049 1054 1057 rBV2 251 277 0.02% 0.002% 33 4.175 1097 1115 1146 rBV 115763 308907 18.29% 2.555% 34 4.551 1228 1232 1238 rVB2 262 304 0.02% 0.003% 35 4.651 1243 1263 1287 rBV 212643 509273 30.15% 4.213% 36 4.854 1321 1326 1330 rBV3 606 685 0.04% 0.006% 37 4.889 1330 1337 1346 rVB3 712 1345 0.08% 0.011% 38 4.963 1354 1360 1361 rBV 210 197 0.01% 0.002% 39 5.175 1423 1426 1430 rVB2 123 100 0.01% 0.001% 40 5.204 1431 1435 1441 rBV2 181 169 0.01% 0.001% 41 5.342 1453 1478 1517 rBV2 439306 1335946 79.09% 11.051% 42 5.641 1566 1571 1575 rBV3 251 248 0.01% 0.002% 43 5.664 1576 1578 1581 rVV3 240 182 0.01% 0.002% 44 5.680 1581 1583 1587 rVB 463 246 0.01% 0.002% 45 5.747 1600 1604 1605 rBV 189 130 0.01% 0.001% 46 5.889 1630 1648 1676 rBV 427093 855088 50.63% 7.073% 47 6.043 1694 1696 1701 rVB3 352 251 0.01% 0.002% 48 6.111 1714 1717 1718 rBV 228 108 0.01% 0.001% 49 6.149 1726 1729 1730 rBV 186 115 0.01% 0.001% 50 6.175 1732 1737 1748 rVV5 1546 2581 0.15% 0.021% 51 6.281 1765 1770 1772 rBV2 170 107 0.01% 0.001% 52 6.336 1772 1787 1815 rBV 296850 607271 35.95% 5.023% 53 6.548 1850 1853 1855 rVB3 175 121 0.01% 0.001% 54 6.564 1855 1858 1861 rBV 232 138 0.01% 0.001% 55 6.645 1879 1883 1886 rVB 125 98 0.01% 0.001% 56 6.786 1923 1927 1933 rBV2 111 152 0.01% 0.001% 57 6.834 1938 1942 1944 rBV 143 126 0.01% 0.001% 58 6.863 1944 1951 1954 rBV2 597 579 0.03% 0.005% 59 6.944 1968 1976 1981 rVB2 147 260 0.02% 0.002% 60 6.969 1981 1984 1988 rVB2 161 122 0.01% 0.001% 61 7.082 2016 2019 2023 rVB2 188 117 0.01% 0.001% 62 7.133 2032 2035 2040 rVB 138 108 0.01% 0.001% 63 7.230 2053 2065 2099 rBV 158842 291335 17.25% 2.410% 64 7.567 2156 2170 2192 rBV 609288 1053192 62.35% 8.712% 65 7.853 2247 2259 2293 rBV 107127 188641 11.17% 1.560% 66 8.178 2356 2360 2370 rVB3 461 705 0.04% 0.006% 67 8.233 2374 2377 2379 rBV 211 142 0.01% 0.001% 68 8.313 2389 2402 2433 rBV 389840 676066 40.03% 5.592% 69 8.632 2498 2501 2503 rBV 401 314 0.02% 0.003% 70 8.808 2553 2556 2559 rBV2 203 178 0.01% 0.001% 71 9.091 2630 2644 2673 rBV 630762 1043238 61.76% 8.630% 72 9.259 2691 2696 2702 rVV3 886 1091 0.06% 0.009% 73 9.384 2726 2735 2747 rBV5 1505 2981 0.18% 0.025% 74 9.529 2776 2780 2785 rVB2 190 208 0.01% 0.002% 75 9.609 2802 2805 2809 rVB 160 145 0.01% 0.001% 76 9.738 2842 2845 2848 rBV 182 137 0.01% 0.001% 77 9.786 2855 2860 2864 rBV2 577 648 0.04% 0.005% 78 9.844 2873 2878 2882 rBV2 225 267 0.02% 0.002% 79 10.027 2932 2935 2937 rBV2 179 117 0.01% 0.001% 80 10.168 2975 2979 2982 rBV2 375 318 0.02% 0.003% 81 10.381 3042 3045 3048 rBV2 158 104 0.01% 0.001% 82 10.435 3048 3062 3083 rBV 407094 652102 38.61% 5.394% 83 10.680 3135 3138 3143 rBV 273 190 0.01% 0.002% 84 11.053 3252 3254 3261 rVB2 274 223 0.01% 0.002% 85 11.088 3262 3265 3268 rBV2 198 128 0.01% 0.001% 86 11.422 3364 3369 3370 rBV3 729 612 0.04% 0.005% 87 11.487 3377 3389 3413 rBV 640001 1020666 60.43% 8.443% 88 11.644 3436 3438 3442 rVB2 317 181 0.01% 0.001% 89 11.667 3442 3445 3449 rBV2 236 212 0.01% 0.002% 90 11.731 3460 3465 3467 rBV2 233 220 0.01% 0.002% 91 11.863 3493 3506 3526 rBV 620437 1010731 59.84% 8.361% 92 12.027 3553 3557 3561 rBV2 379 307 0.02% 0.003% 93 12.130 3585 3589 3592 rBV 316 297 0.02% 0.002% 94 12.213 3614 3615 3623 rVB2 234 172 0.01% 0.001% 95 12.898 3821 3828 3836 rVB4 1409 2156 0.13% 0.018% 96 13.281 3943 3947 3956 rBV2 350 498 0.03% 0.004% 97 13.519 4015 4021 4031 rVB2 1361 2072 0.12% 0.017% 98 13.757 4090 4095 4104 rBV3 1483 2199 0.13% 0.018% 99 14.001 4163 4171 4182 rBV3 2534 4327 0.26% 0.036% 100 14.245 4243 4247 4252 rBV2 705 837 0.05% 0.007% Sum of corrected areas: 12088832