Data Path : W:\HPCHEM1\MSVOA_U\Data\VU050718\ Quantitation Report (LSC Reviewed) Data File : VU023712.D Acq On : 07 May 2018 13:43 Operator : MD/SY Sample : J2691-22MEDL 50X Misc : 2.94g/5.0mL/100uL/5.0mL/MSVOA_U/MEOH ALS Vial : 9 Sample Multiplier: 1 Quant Time: May 08 04:42:09 2018 Quant Method : W:\HPCHEM1\MSVOA_U\METHOD\SOMULM050118WMA.M Quant Title : VOC Analysis QLast Update : Mon May 07 00:51:10 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) 1,4-Difluorobenzene 5.89 114 355901 50.00 ug/L 0.00 28) Chlorobenzene-d5 9.09 117 334425 50.00 ug/L 0.00 60) 1,4-Dichlorobenzene-d4 11.49 152 175080 50.00 ug/L 0.00 System Monitoring Compounds 4) Vinyl Chloride-d3 1.40 65 100860 39.98 ug/L 0.00 Spiked Amount 50.000 Range 60 - 135 Recovery = 79.96% 7) Chloroethane-d5 1.68 69 84136 43.76 ug/L 0.00 Spiked Amount 50.000 Range 70 - 130 Recovery = 87.52% 11) 1,1-Dichloroethene-d2 2.27 63 154623 31.44 ug/L 0.00 Spiked Amount 50.000 Range 60 - 125 Recovery = 62.88% 21) 2-Butanone-d5 4.18 46 184039 105.60 ug/L 0.00 Spiked Amount 100.000 Range 40 - 130 Recovery = 105.60% 24) Chloroform-d 4.65 84 193836 46.47 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 92.94% 26) 1,2-Dichloroethane-d4 5.31 65 131426 45.30 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 90.60% 32) Benzene-d6 5.35 84 409978 45.69 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 91.38% 36) 1,2-Dichloropropane-d6 6.34 67 139879 46.54 ug/L 0.00 Spiked Amount 50.000 Range 70 - 120 Recovery = 93.08% 41) Toluene-d8 7.57 98 375327 45.37 ug/L 0.00 Spiked Amount 50.000 Range 80 - 120 Recovery = 90.74% 43) trans-1,3-Dichloropropene- 7.85 79 57944 44.79 ug/L 0.00 Spiked Amount 50.000 Range 60 - 125 Recovery = 89.58% 47) 2-Hexanone-d5 8.31 63 132413 116.02 ug/L 0.00 Spiked Amount 100.000 Range 45 - 130 Recovery = 116.02% 57) 1,1,2,2-Tetrachloroethane- 10.44 84 188832 48.57 ug/L 0.00 Spiked Amount 50.000 Range 65 - 120 Recovery = 97.14% 64) 1,2-Dichlorobenzene-d4 11.86 152 162423 47.55 ug/L 0.00 Spiked Amount 50.000 Range 80 - 120 Recovery = 95.10% Target Compounds Qvalue 35) Methylcyclohexane 6.42 83 26806 5.68 ug/L 95 42) Toluene 7.64 91 372643 30.51 ug/L 99 52) Ethylbenzene 9.26 91 403408 30.47 ug/L 99 53) m,p-Xylene 9.38 106 365623 72.40 ug/L 99 54) o-xylene 9.78 106 116666 24.38 ug/L 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed