LSC Area Percent Report Data Path : W:\HPCHEM1\MSVOA_U\DATA\VU050718\ Data File : VU023712.D Acq On : 07 May 2018 13:43 Operator : MD/SY Sample : J2691-22MEDL 50X Misc : 2.94g/5.0mL/100uL/5.0mL/MSVOA_U/MEOH ALS Vial : 9 Sample Multiplier: 1 Integration Parameters: LSCINT.P Integrator: RTE Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 0 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Method : W:\HPCHEM1\MSVOA_U\METHOD\SOMULM050118WMA.M Title : VOC Analysis Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total --- ----- ----- ---- ---- --- ------- ------- ------ ------- 1 1.088 136 155 176 rBV 1366272 1529558 71.78% 7.011% 2 1.182 180 184 190 rVB 6678 6264 0.29% 0.029% 3 1.397 245 251 270 rVB 153458 159723 7.50% 0.732% 4 1.680 330 339 356 rVB 114959 149207 7.00% 0.684% 5 1.886 400 403 410 rVB3 3251 3171 0.15% 0.015% 6 2.272 512 523 537 rBV 269041 407161 19.11% 1.866% 7 2.841 688 700 713 rVB 2094 4128 0.19% 0.019% 8 2.998 740 749 758 rVB2 1834 3750 0.18% 0.017% 9 3.304 833 844 861 rVB3 5120 10378 0.49% 0.048% 10 4.098 1079 1091 1101 rBV4 2709 6115 0.29% 0.028% 11 4.178 1102 1116 1145 rBV 112797 295920 13.89% 1.356% 12 4.651 1245 1263 1285 rBV 194313 463398 21.75% 2.124% 13 4.992 1357 1369 1384 rBV4 10665 25227 1.18% 0.116% 14 5.082 1384 1397 1411 rVB5 2852 6366 0.30% 0.029% 15 5.223 1426 1441 1454 rBV2 10007 23635 1.11% 0.108% 16 5.342 1455 1478 1514 rVV2 397163 1193396 56.00% 5.470% 17 5.554 1538 1544 1555 rVB6 3119 5826 0.27% 0.027% 18 5.628 1556 1567 1580 rVB7 6658 13772 0.65% 0.063% 19 5.789 1599 1617 1634 rBV3 36834 74131 3.48% 0.340% 20 5.889 1634 1648 1694 rBV 398644 821113 38.53% 3.764% 21 6.185 1731 1740 1748 rBV5 2131 3562 0.17% 0.016% 22 6.336 1773 1787 1801 rBV 267771 543854 25.52% 2.493% 23 6.419 1804 1813 1826 rVB2 64441 132111 6.20% 0.606% 24 6.532 1843 1848 1861 rVB6 5186 10007 0.47% 0.046% 25 6.644 1874 1883 1892 rVB4 3922 7274 0.34% 0.033% 26 6.741 1900 1913 1925 rBV7 7368 15540 0.73% 0.071% 27 6.905 1955 1964 1982 rVB5 7867 14859 0.70% 0.068% 28 7.111 2015 2028 2035 rBV4 4111 7827 0.37% 0.036% 29 7.185 2036 2051 2056 rBV3 18259 32432 1.52% 0.149% 30 7.230 2056 2065 2084 rVB 145762 263920 12.39% 1.210% 31 7.345 2093 2101 2123 rVB 15058 33568 1.58% 0.154% 32 7.570 2147 2171 2182 rBV 559646 1019662 47.85% 4.674% 33 7.641 2182 2193 2208 rVB 492012 851201 39.95% 3.902% 34 7.824 2241 2250 2253 rBV 57587 80820 3.79% 0.370% 35 7.921 2272 2280 2292 rVB3 17049 32085 1.51% 0.147% 36 8.050 2311 2320 2333 rVB5 7587 13193 0.62% 0.060% 37 8.233 2369 2377 2383 rBV4 3223 4758 0.22% 0.022% 38 8.313 2389 2402 2436 rBV 389699 675978 31.72% 3.098% 39 8.548 2466 2475 2486 rVB2 19063 32549 1.53% 0.149% 40 8.612 2486 2495 2505 rBV3 8774 16987 0.80% 0.078% 41 8.757 2535 2540 2550 rVB5 1732 2794 0.13% 0.013% 42 8.818 2550 2559 2564 rBV2 5488 8666 0.41% 0.040% 43 8.911 2582 2588 2600 rVB3 15434 25186 1.18% 0.115% 44 9.037 2617 2627 2633 rBV2 11961 19678 0.92% 0.090% 45 9.095 2633 2645 2667 rVV 597150 980411 46.01% 4.494% 46 9.252 2682 2694 2711 rBV 580705 930912 43.69% 4.267% 47 9.377 2719 2733 2748 rBV 1299612 2130902 100.00% 9.767% 48 9.448 2749 2755 2774 rVB2 33837 54622 2.56% 0.250% 49 9.722 2827 2840 2848 rBV7 9982 19490 0.91% 0.089% 50 9.783 2848 2859 2883 rVB 447356 703840 33.03% 3.226% 51 9.956 2895 2913 2923 rVB6 12533 25342 1.19% 0.116% 52 10.049 2934 2942 2950 rBV6 9749 16296 0.76% 0.075% 53 10.172 2968 2980 2991 rBV 15199 25418 1.19% 0.117% 54 10.226 2991 2997 3001 rBV3 2106 2948 0.14% 0.014% 55 10.258 3002 3007 3015 rVB6 4069 6046 0.28% 0.028% 56 10.435 3050 3062 3075 rBV 385615 617354 28.97% 2.830% 57 10.593 3101 3111 3119 rBV 18252 27766 1.30% 0.127% 58 10.686 3131 3140 3155 rBV 58370 123415 5.79% 0.566% 59 10.776 3157 3168 3174 rVV2 42354 71586 3.36% 0.328% 60 10.818 3175 3181 3192 rVB 45290 64202 3.01% 0.294% 61 10.975 3221 3230 3238 rBV 27289 43741 2.05% 0.200% 62 11.078 3255 3262 3267 rBV7 3665 4998 0.23% 0.023% 63 11.117 3267 3274 3276 rBV 13668 14277 0.67% 0.065% 64 11.152 3277 3285 3310 rVB 144778 239612 11.24% 1.098% 65 11.287 3312 3327 3328 rBV7 7991 12208 0.57% 0.056% 66 11.403 3354 3363 3366 rBV5 9152 13427 0.63% 0.062% 67 11.487 3378 3389 3403 rBV 662709 1044273 49.01% 4.787% 68 11.574 3408 3416 3425 rVV 71971 102236 4.80% 0.469% 69 11.783 3468 3481 3483 rBV5 52101 78471 3.68% 0.360% 70 11.811 3486 3490 3497 rVV 129721 175441 8.23% 0.804% 71 11.866 3497 3507 3527 rVB4 754493 1436552 67.42% 6.585% 72 11.985 3537 3544 3550 rBV3 14030 19923 0.93% 0.091% 73 12.027 3550 3557 3561 rBV 37854 50940 2.39% 0.233% 74 12.059 3562 3567 3584 rVB 82840 124169 5.83% 0.569% 75 12.149 3585 3595 3600 rBV 146112 230075 10.80% 1.055% 76 12.255 3617 3628 3637 rBV 300033 443450 20.81% 2.033% 77 12.393 3651 3671 3690 rBV7 64839 231851 10.88% 1.063% 78 12.496 3692 3703 3712 rBV4 31975 59316 2.78% 0.272% 79 12.554 3712 3721 3732 rVB 100943 162005 7.60% 0.743% 80 12.654 3732 3752 3760 rBV 236618 406282 19.07% 1.862% 81 12.705 3760 3768 3786 rVB 375444 572745 26.88% 2.625% 82 12.789 3786 3794 3799 rBV 55132 80210 3.76% 0.368% 83 12.824 3800 3805 3809 rBV 30439 33680 1.58% 0.154% 84 12.969 3842 3850 3862 rVB2 125748 189823 8.91% 0.870% 85 13.033 3862 3870 3878 rBV2 34765 50239 2.36% 0.230% 86 13.088 3878 3887 3890 rBV2 58614 83332 3.91% 0.382% 87 13.127 3891 3899 3926 rVB4 296237 596464 27.99% 2.734% 88 13.242 3927 3935 3943 rBV 50047 74242 3.48% 0.340% 89 13.409 3979 3987 3996 rBV3 15015 24153 1.13% 0.111% 90 13.461 3998 4003 4009 rVB4 7205 9130 0.43% 0.042% 91 13.512 4009 4019 4025 rBV3 68521 115808 5.43% 0.531% 92 13.612 4046 4050 4053 rBV2 5592 5566 0.26% 0.026% 93 13.644 4054 4060 4070 rVB 30103 43383 2.04% 0.199% 94 13.705 4073 4079 4081 rBV4 3313 3614 0.17% 0.017% 95 13.747 4082 4092 4103 rBV 96182 154459 7.25% 0.708% 96 13.969 4152 4161 4170 rBV4 6259 12158 0.57% 0.056% 97 14.017 4171 4176 4183 rVB3 3271 4387 0.21% 0.020% 98 14.155 4209 4219 4228 rBV4 7815 11912 0.56% 0.055% 99 14.339 4269 4276 4277 rBV3 3430 3135 0.15% 0.014% 100 14.480 4315 4320 4330 rVB3 2598 3877 0.18% 0.018% Sum of corrected areas: 21816864