LSC Area Percent Report Data Path : W:\HPCHEM1\MSVOA_U\Data\VU050718\ Data File : VU023715.D Acq On : 07 May 2018 15:02 Operator : MD/SY Sample : J2725-03 Misc : 5.0mL/MSVOA_U/WATER ALS Vial : 12 Sample Multiplier: 1 Integration Parameters: LSCINT.P Integrator: RTE Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 0 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Method : W:\HPCHEM1\MSVOA_U\METHOD\SOMULM050118WMA.M Title : VOC Analysis Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total --- ----- ----- ---- ---- --- ------- ------- ------ ------- 1 1.088 147 155 180 rBV 17561597 25743008 16.41% 7.367% 2 1.182 181 184 201 rVB2 20846 26310 0.02% 0.008% 3 1.397 244 251 264 rVB 148592 156259 0.10% 0.045% 4 1.474 270 275 284 rVB 18358 20624 0.01% 0.006% 5 1.680 331 339 354 rVB 112288 142431 0.09% 0.041% 6 2.130 474 479 488 rVB 4342 6094 0.00% 0.002% 7 2.272 511 523 533 rBV 250229 379056 0.24% 0.108% 8 2.378 551 556 566 rVB4 2590 4050 0.00% 0.001% 9 2.445 569 577 585 rBV 3030 4940 0.00% 0.001% 10 2.554 602 611 620 rVV2 2279 3747 0.00% 0.001% 11 2.683 642 651 662 rVB3 5554 9434 0.01% 0.003% 12 2.792 674 685 702 rBV2 6480 13049 0.01% 0.004% 13 3.808 984 1001 1015 rBV4 4316 9768 0.01% 0.003% 14 4.178 1102 1116 1146 rBV 163657 422000 0.27% 0.121% 15 4.651 1242 1263 1287 rBV 188277 449161 0.29% 0.129% 16 5.001 1354 1372 1385 rVB4 6189 14440 0.01% 0.004% 17 5.397 1452 1495 1557 rBV 17020098 37667871 24.00% 10.779% 18 5.644 1559 1572 1598 rVB 323313 675739 0.43% 0.193% 19 5.792 1608 1618 1634 rVB3 15223 32276 0.02% 0.009% 20 5.889 1634 1648 1676 rBV 413824 816855 0.52% 0.234% 21 6.185 1730 1740 1749 rBV5 1974 3544 0.00% 0.001% 22 6.336 1767 1787 1807 rBV 271720 550800 0.35% 0.158% 23 7.233 2052 2066 2085 rBV 143080 256186 0.16% 0.073% 24 7.467 2131 2139 2152 rVB3 10364 18219 0.01% 0.005% 25 7.570 2156 2171 2181 rBV 509129 907765 0.58% 0.260% 26 7.641 2181 2193 2226 rVB 5987924 10610324 6.76% 3.036% 27 7.853 2250 2259 2275 rVB 104625 177062 0.11% 0.051% 28 7.943 2276 2287 2306 rVB 74043 130119 0.08% 0.037% 29 8.313 2390 2402 2438 rBV 591345 1045399 0.67% 0.299% 30 8.464 2439 2449 2468 rVB 60608 111625 0.07% 0.032% 31 9.094 2620 2645 2680 rBV 577992 1057349 0.67% 0.303% 32 9.255 2681 2695 2715 rBV 1392569 2327430 1.48% 0.666% 33 9.377 2721 2733 2764 rVB 2981224 4944494 3.15% 1.415% 34 9.503 2766 2772 2778 rVV6 10464 16231 0.01% 0.005% 35 9.548 2778 2786 2799 rVB3 29962 51089 0.03% 0.015% 36 9.737 2837 2845 2847 rBV2 14532 17853 0.01% 0.005% 37 9.782 2848 2859 2887 rVV2 1983003 3440740 2.19% 0.985% 38 9.898 2888 2895 2910 rVV2 15524 28035 0.02% 0.008% 39 9.969 2913 2917 2924 rVV4 6355 7946 0.01% 0.002% 40 10.014 2924 2931 2946 rVV2 12060 25983 0.02% 0.007% 41 10.082 2948 2952 2962 rVV3 8134 11392 0.01% 0.003% 42 10.172 2963 2980 2991 rVB2 55313 110327 0.07% 0.032% 43 10.239 2996 3001 3012 rVB7 2464 3960 0.00% 0.001% 44 10.435 3049 3062 3078 rBV 409842 663393 0.42% 0.190% 45 10.512 3079 3086 3096 rVB3 9491 14321 0.01% 0.004% 46 10.593 3100 3111 3123 rBV 31880 57815 0.04% 0.017% 47 10.686 3129 3140 3145 rBV 268505 442979 0.28% 0.127% 48 10.776 3158 3168 3182 rVB 246524 372444 0.24% 0.107% 49 10.905 3197 3208 3219 rBV3 25601 42570 0.03% 0.012% 50 10.975 3219 3230 3255 rVB 95007 186911 0.12% 0.053% 51 11.152 3267 3285 3297 rBV 686540 1079344 0.69% 0.309% 52 11.220 3299 3306 3315 rVV 41358 68250 0.04% 0.020% 53 11.271 3317 3322 3332 rVB4 12373 18120 0.01% 0.005% 54 11.403 3350 3363 3378 rBV 4548013 7036123 4.48% 2.013% 55 11.487 3378 3389 3405 rVV 723136 1136629 0.72% 0.325% 56 11.573 3405 3416 3426 rVV 279540 436836 0.28% 0.125% 57 11.631 3427 3434 3446 rVB 48353 77049 0.05% 0.022% 58 11.770 3463 3477 3496 rBV 7574226 11793569 7.52% 3.375% 59 11.866 3496 3507 3525 rVB 630186 1044141 0.67% 0.299% 60 11.988 3529 3545 3561 rBV 19001683 29935524 19.08% 8.566% 61 12.152 3588 3596 3600 rBV2 13403 19281 0.01% 0.006% 62 12.255 3613 3628 3634 rBV 42293 69560 0.04% 0.020% 63 12.358 3649 3660 3681 rVB 251937 396161 0.25% 0.113% 64 12.477 3687 3697 3711 rBV3 64890 110370 0.07% 0.032% 65 12.570 3711 3726 3748 rBV2 1064073 2551709 1.63% 0.730% 66 12.699 3756 3766 3776 rBV 1222275 2272327 1.45% 0.650% 67 12.969 3840 3850 3866 rVB 247490 376355 0.24% 0.108% 68 13.094 3878 3889 3894 rBV 400351 618713 0.39% 0.177% 69 13.191 3909 3919 3932 rVB 339567 520947 0.33% 0.149% 70 13.297 3939 3952 3967 rVB2 538019 853847 0.54% 0.244% 71 13.393 3972 3982 3990 rBV3 27905 51555 0.03% 0.015% 72 13.445 3990 3998 4009 rBV2 39287 72245 0.05% 0.021% 73 13.618 4042 4052 4072 rBV 160566 308657 0.20% 0.088% 74 13.779 4078 4102 4115 rBV2 63842569 156920290 100.00% 44.904% 75 13.872 4119 4131 4152 rVV 4698880 7229932 4.61% 2.069% 76 14.014 4168 4175 4181 rBV4 30894 48618 0.03% 0.014% 77 14.056 4181 4188 4201 rVB2 99953 154480 0.10% 0.044% 78 14.159 4212 4220 4228 rBV2 26246 42147 0.03% 0.012% 79 14.351 4267 4280 4286 rBV5 24815 55257 0.04% 0.016% 80 14.538 4330 4338 4351 rVB3 59865 99698 0.06% 0.029% 81 14.676 4376 4381 4390 rVB8 9074 14871 0.01% 0.004% 82 14.734 4393 4399 4409 rVV6 10113 15634 0.01% 0.004% 83 14.824 4410 4427 4433 rVV 138328 237587 0.15% 0.068% 84 14.882 4433 4445 4469 rVV 8191417 12564082 8.01% 3.595% 85 14.994 4470 4480 4490 rVV 152623 248845 0.16% 0.071% 86 15.065 4490 4502 4526 rVB 4881563 7650879 4.88% 2.189% 87 15.564 4645 4657 4662 rBV2 44166 82729 0.05% 0.024% 88 15.612 4663 4672 4684 rVB 586778 885715 0.56% 0.253% 89 15.679 4687 4693 4713 rVB9 13396 33084 0.02% 0.009% 90 15.802 4717 4731 4740 rBV 215279 361268 0.23% 0.103% 91 15.917 4755 4767 4790 rVB 298801 522392 0.33% 0.149% 92 16.017 4794 4798 4800 rVV4 4498 4157 0.00% 0.001% 93 16.062 4802 4812 4819 rVV 328013 544081 0.35% 0.156% 94 16.101 4819 4824 4842 rVB 253923 371908 0.24% 0.106% 95 16.293 4866 4884 4906 rVB2 85757 207960 0.13% 0.060% 96 16.435 4918 4928 4943 rVB 85186 132795 0.08% 0.038% 97 16.528 4946 4957 4971 rBV2 113525 207219 0.13% 0.059% 98 16.744 5010 5024 5043 rBV 3376924 5328506 3.40% 1.525% 99 16.917 5070 5078 5091 rVB3 75324 115115 0.07% 0.033% 100 17.043 5106 5117 5138 rVB 180136 299706 0.19% 0.086% Sum of corrected areas: 349457684