LSC Area Percent Report Data Path : W:\HPCHEM1\MSVOA_U\Data\VU050718\ Data File : VU023717.D Acq On : 07 May 2018 15:54 Operator : MD/SY Sample : J2725-05 Misc : 5.0mL/MSVOA_U/WATER ALS Vial : 14 Sample Multiplier: 1 Integration Parameters: LSCINT.P Integrator: RTE Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 0 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Method : W:\HPCHEM1\MSVOA_U\METHOD\SOMULM050118WMA.M Title : VOC Analysis Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total --- ----- ----- ---- ---- --- ------- ------- ------ ------- 1 1.089 134 155 172 rBV 1737382 1922693 0.93% 0.566% 2 1.185 181 185 186 rBV 13744 10377 0.01% 0.003% 3 1.330 213 230 245 rBV 227069 1011995 0.49% 0.298% 4 2.272 512 523 533 rBV 264513 400803 0.19% 0.118% 5 2.323 534 539 550 rVB 25143 37204 0.02% 0.011% 6 2.445 568 577 580 rBV 7128 10392 0.01% 0.003% 7 2.478 581 587 597 rVB 17737 27770 0.01% 0.008% 8 3.805 986 1000 1017 rVV4 6504 14939 0.01% 0.004% 9 4.111 1080 1095 1101 rBV9 2114 5345 0.00% 0.002% 10 4.178 1101 1116 1140 rBV 144606 373285 0.18% 0.110% 11 4.651 1245 1263 1287 rBV 195858 458910 0.22% 0.135% 12 4.892 1330 1338 1342 rBV4 620 1102 0.00% 0.000% 13 4.998 1360 1371 1384 rVB6 4804 11256 0.01% 0.003% 14 5.346 1452 1479 1482 rBV2 421545 1044375 0.50% 0.308% 15 5.394 1484 1494 1548 rVB 3601642 7674953 3.70% 2.260% 16 5.645 1561 1572 1591 rVB 48769 102038 0.05% 0.030% 17 5.793 1610 1618 1624 rBV5 1263 2020 0.00% 0.001% 18 5.889 1634 1648 1683 rBV 382759 774115 0.37% 0.228% 19 6.336 1762 1787 1805 rBV 278738 569632 0.27% 0.168% 20 7.233 2053 2066 2088 rBV 149753 269732 0.13% 0.079% 21 7.471 2134 2140 2150 rVB3 2236 3576 0.00% 0.001% 22 7.571 2156 2171 2181 rBV 538023 950501 0.46% 0.280% 23 7.641 2181 2193 2226 rVB 5968781 10742002 5.18% 3.163% 24 7.854 2249 2259 2275 rVB 105731 179072 0.09% 0.053% 25 7.944 2277 2287 2302 rVB 43260 73290 0.04% 0.022% 26 8.313 2388 2402 2434 rBV 493584 875378 0.42% 0.258% 27 8.461 2442 2448 2465 rVB3 13382 24515 0.01% 0.007% 28 8.583 2482 2486 2497 rVB5 959 1291 0.00% 0.000% 29 9.095 2632 2645 2681 rBV 542070 951562 0.46% 0.280% 30 9.252 2681 2694 2718 rBV 1187427 2012950 0.97% 0.593% 31 9.378 2720 2733 2766 rVB 3186273 5346028 2.58% 1.574% 32 9.548 2778 2786 2802 rVB 25226 43179 0.02% 0.013% 33 9.625 2805 2810 2813 rBV5 999 958 0.00% 0.000% 34 9.738 2835 2845 2847 rBV2 14509 17425 0.01% 0.005% 35 9.783 2848 2859 2888 rVB 1721847 2777947 1.34% 0.818% 36 9.895 2890 2894 2895 rBV3 1815 1080 0.00% 0.000% 37 10.014 2923 2931 2943 rVB 9156 14989 0.01% 0.004% 38 10.085 2946 2953 2963 rVB5 2386 4008 0.00% 0.001% 39 10.172 2963 2980 2998 rBV 62448 106326 0.05% 0.031% 40 10.435 3048 3062 3079 rBV 399680 647216 0.31% 0.191% 41 10.513 3079 3086 3098 rVB4 7046 10114 0.00% 0.003% 42 10.593 3100 3111 3124 rBV 34657 54766 0.03% 0.016% 43 10.686 3126 3140 3158 rBV 354645 801219 0.39% 0.236% 44 10.776 3158 3168 3184 rVB 309370 466146 0.22% 0.137% 45 10.898 3198 3206 3216 rVB6 3459 5622 0.00% 0.002% 46 10.976 3219 3230 3256 rVB 108448 185993 0.09% 0.055% 47 11.152 3270 3285 3301 rBV 762888 1167655 0.56% 0.344% 48 11.271 3313 3322 3323 rBV6 1474 2340 0.00% 0.001% 49 11.329 3334 3340 3348 rVB3 3762 5088 0.00% 0.001% 50 11.403 3350 3363 3378 rBV 3875217 6019132 2.90% 1.772% 51 11.487 3378 3389 3405 rVB 676771 1061765 0.51% 0.313% 52 11.577 3405 3417 3428 rBV 287664 468228 0.23% 0.138% 53 11.770 3461 3477 3495 rBV 7562887 11869973 5.73% 3.495% 54 11.866 3496 3507 3527 rVB2 636127 1083214 0.52% 0.319% 55 11.985 3530 3544 3561 rBV 6887550 10582190 5.11% 3.116% 56 12.066 3563 3569 3577 rVB2 19678 29002 0.01% 0.009% 57 12.152 3588 3596 3600 rBV 15066 21024 0.01% 0.006% 58 12.255 3619 3628 3634 rBV 53134 80603 0.04% 0.024% 59 12.291 3635 3639 3649 rVB 40737 52308 0.03% 0.015% 60 12.358 3649 3660 3682 rVB 289500 453986 0.22% 0.134% 61 12.477 3682 3697 3710 rBV4 64086 133311 0.06% 0.039% 62 12.574 3714 3727 3730 rBV 480629 713465 0.34% 0.210% 63 12.699 3746 3766 3775 rBV 1272819 2540933 1.23% 0.748% 64 12.969 3840 3850 3866 rVB 307835 482502 0.23% 0.142% 65 13.127 3879 3899 3910 rBV2 447650 802129 0.39% 0.236% 66 13.191 3910 3919 3933 rVB 153217 239357 0.12% 0.070% 67 13.297 3939 3952 3966 rVB2 310299 506784 0.24% 0.149% 68 13.394 3973 3982 3990 rBV4 19059 35019 0.02% 0.010% 69 13.451 3992 4000 4011 rVV2 39433 83498 0.04% 0.025% 70 13.516 4013 4020 4029 rVV7 32037 57598 0.03% 0.017% 71 13.567 4031 4036 4042 rVV2 17564 29004 0.01% 0.009% 72 13.615 4045 4051 4072 rVB4 59231 113763 0.05% 0.033% 73 13.789 4078 4105 4117 rBV2 73208048 207259924 100.00% 61.029% 74 13.876 4121 4132 4152 rVV 5576448 8595858 4.15% 2.531% 75 14.014 4167 4175 4182 rBV3 45061 71653 0.03% 0.021% 76 14.059 4183 4189 4200 rVB4 49696 77063 0.04% 0.023% 77 14.159 4211 4220 4228 rBV2 32951 52958 0.03% 0.016% 78 14.352 4268 4280 4288 rBV4 28360 64644 0.03% 0.019% 79 14.538 4330 4338 4352 rVB3 72418 121929 0.06% 0.036% 80 14.734 4394 4399 4409 rVB7 7518 10223 0.00% 0.003% 81 14.824 4411 4427 4434 rVV 165426 293174 0.14% 0.086% 82 14.885 4434 4446 4469 rVV 11690658 18274726 8.82% 5.381% 83 14.995 4471 4480 4490 rVV 188287 312755 0.15% 0.092% 84 15.069 4490 4503 4528 rVB 6076305 9579552 4.62% 2.821% 85 15.220 4543 4550 4567 rVB4 8996 15836 0.01% 0.005% 86 15.567 4645 4658 4662 rBV3 54464 103972 0.05% 0.031% 87 15.612 4662 4672 4685 rVB 1124974 1705306 0.82% 0.502% 88 15.683 4686 4694 4711 rVB9 24890 59591 0.03% 0.018% 89 15.805 4715 4732 4740 rBV 414832 692681 0.33% 0.204% 90 15.918 4755 4767 4789 rVB 541262 941427 0.45% 0.277% 91 16.062 4802 4812 4819 rBV 572257 918675 0.44% 0.271% 92 16.101 4819 4824 4841 rVB 440968 665504 0.32% 0.196% 93 16.290 4865 4883 4905 rBV2 164522 399778 0.19% 0.118% 94 16.435 4918 4928 4945 rBV 159182 246573 0.12% 0.073% 95 16.535 4946 4959 4975 rBV3 154672 292521 0.14% 0.086% 96 16.638 4983 4991 5001 rVB2 33970 53152 0.03% 0.016% 97 16.744 5011 5024 5043 rBV 5159464 7948224 3.83% 2.340% 98 16.917 5069 5078 5091 rBV2 164402 259830 0.13% 0.077% 99 17.043 5104 5117 5136 rBV 571005 922445 0.45% 0.272% 100 17.342 5204 5210 5215 rBV5 10903 16196 0.01% 0.005% Sum of corrected areas: 339610130