LSC Area Percent Report Data Path : W:\HPCHEM1\MSVOA_U\Data\VU050718\ Data File : VU023722.D Acq On : 07 May 2018 19:02 Operator : MD/SY Sample : J2725-14 Misc : 5.0mL/MSVOA_U/WATER ALS Vial : 20 Sample Multiplier: 1 Integration Parameters: LSCINT.P Integrator: RTE Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 0 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Method : W:\HPCHEM1\MSVOA_U\METHOD\SOMULM050118WMA.M Title : VOC Analysis Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total --- ----- ----- ---- ---- --- ------- ------- ------ ------- 1 1.089 147 155 173 rBV 547421 633589 17.23% 3.187% 2 1.182 180 184 188 rBV2 11625 12242 0.33% 0.062% 3 1.333 210 231 245 rBV 162151 802357 21.82% 4.036% 4 1.680 334 339 362 rVB 126191 170536 4.64% 0.858% 5 2.272 513 523 535 rBV 246768 369460 10.05% 1.858% 6 2.449 569 578 585 rBV2 5115 8909 0.24% 0.045% 7 3.960 1042 1048 1051 rBV2 190 201 0.01% 0.001% 8 4.002 1057 1061 1066 rBV3 398 289 0.01% 0.001% 9 4.072 1079 1083 1088 rBV2 205 280 0.01% 0.001% 10 4.178 1099 1116 1151 rBV 123677 327714 8.91% 1.648% 11 4.381 1176 1179 1182 rBV4 468 376 0.01% 0.002% 12 4.558 1231 1234 1237 rBV2 274 197 0.01% 0.001% 13 4.651 1246 1263 1289 rVV 192164 453088 12.32% 2.279% 14 4.805 1308 1311 1314 rBV2 328 209 0.01% 0.001% 15 4.889 1327 1337 1345 rBV5 586 1028 0.03% 0.005% 16 4.998 1364 1371 1378 rVB5 776 956 0.03% 0.005% 17 5.346 1453 1479 1512 rBV2 397519 1278460 34.77% 6.430% 18 5.641 1566 1571 1573 rBV2 598 596 0.02% 0.003% 19 5.789 1613 1617 1618 rBV 468 327 0.01% 0.002% 20 5.889 1633 1648 1684 rBV 426404 856595 23.30% 4.308% 21 6.175 1734 1737 1739 rBV2 337 201 0.01% 0.001% 22 6.191 1739 1742 1748 rVB3 681 700 0.02% 0.004% 23 6.336 1771 1787 1818 rBV 269873 550138 14.96% 2.767% 24 6.870 1943 1953 1956 rBV3 734 1027 0.03% 0.005% 25 7.233 2053 2066 2094 rBV 145380 259943 7.07% 1.307% 26 7.571 2156 2171 2184 rVV 538730 940202 25.57% 4.729% 27 7.641 2186 2193 2208 rVB 32814 60228 1.64% 0.303% 28 7.854 2248 2259 2281 rBV 97299 165959 4.51% 0.835% 29 8.018 2305 2310 2313 rBV2 344 301 0.01% 0.002% 30 8.079 2324 2329 2335 rVB2 214 299 0.01% 0.002% 31 8.178 2356 2360 2365 rBV2 499 492 0.01% 0.002% 32 8.233 2371 2377 2381 rVB3 491 504 0.01% 0.003% 33 8.313 2390 2402 2442 rBV 433080 729521 19.84% 3.669% 34 8.648 2501 2506 2509 rBV3 564 634 0.02% 0.003% 35 8.979 2603 2609 2611 rBV2 208 211 0.01% 0.001% 36 9.091 2631 2644 2682 rBV 623442 1028698 27.98% 5.174% 37 9.252 2682 2694 2713 rBV 102688 166363 4.52% 0.837% 38 9.381 2723 2734 2749 rVB2 21352 36095 0.98% 0.182% 39 9.558 2785 2789 2792 rBV3 387 361 0.01% 0.002% 40 9.738 2841 2845 2849 rVB2 729 703 0.02% 0.004% 41 9.786 2849 2860 2877 rBV 25914 41587 1.13% 0.209% 42 9.892 2889 2893 2897 rBV2 402 469 0.01% 0.002% 43 9.963 2911 2915 2918 rBV2 284 241 0.01% 0.001% 44 10.172 2969 2980 2994 rBV3 12276 17942 0.49% 0.090% 45 10.435 3049 3062 3080 rBV 393483 622941 16.94% 3.133% 46 10.593 3101 3111 3126 rBV2 7378 11392 0.31% 0.057% 47 10.712 3131 3148 3160 rBV 20974 39060 1.06% 0.196% 48 10.776 3160 3168 3177 rVB2 5399 7952 0.22% 0.040% 49 10.976 3221 3230 3244 rVB2 9171 13402 0.36% 0.067% 50 11.152 3277 3285 3297 rVB4 3289 4859 0.13% 0.024% 51 11.406 3354 3364 3377 rBV 30070 49545 1.35% 0.249% 52 11.487 3377 3389 3408 rVV 689927 1067770 29.04% 5.371% 53 11.574 3410 3416 3431 rVB 8936 13201 0.36% 0.066% 54 11.693 3449 3453 3456 rBV2 393 406 0.01% 0.002% 55 11.770 3465 3477 3494 rBV 205886 334454 9.10% 1.682% 56 11.863 3494 3506 3524 rVB 608797 962775 26.19% 4.842% 57 11.985 3533 3544 3561 rBV 113052 176347 4.80% 0.887% 58 12.149 3591 3595 3600 rBV4 1496 1632 0.04% 0.008% 59 12.255 3620 3628 3636 rBV2 10226 14127 0.38% 0.071% 60 12.358 3649 3660 3678 rVB 131419 200174 5.44% 1.007% 61 12.477 3692 3697 3713 rVB6 3259 5216 0.14% 0.026% 62 12.541 3715 3717 3721 rBV3 535 467 0.01% 0.002% 63 12.596 3721 3734 3745 rVV 67196 108049 2.94% 0.543% 64 12.654 3746 3752 3757 rVV3 4747 6273 0.17% 0.032% 65 12.705 3757 3768 3784 rVV2 79992 169392 4.61% 0.852% 66 12.779 3785 3791 3802 rVB2 18353 28922 0.79% 0.145% 67 12.886 3819 3824 3831 rBV3 932 997 0.03% 0.005% 68 12.969 3841 3850 3859 rBV2 15533 23131 0.63% 0.116% 69 13.043 3871 3873 3879 rBV 366 309 0.01% 0.002% 70 13.123 3883 3898 3909 rVV2 20396 36116 0.98% 0.182% 71 13.191 3909 3919 3930 rVB2 24214 36941 1.00% 0.186% 72 13.294 3942 3951 3962 rVB3 24073 37790 1.03% 0.190% 73 13.384 3974 3979 3981 rBV3 577 515 0.01% 0.003% 74 13.458 3994 4002 4011 rBV3 8452 14676 0.40% 0.074% 75 13.554 4025 4032 4045 rBV3 16554 27003 0.73% 0.136% 76 13.612 4046 4050 4056 rVB2 4793 5220 0.14% 0.026% 77 13.670 4066 4068 4077 rVB3 1173 1069 0.03% 0.005% 78 13.744 4077 4091 4114 rBV 1010101 1664237 45.26% 8.371% 79 13.863 4117 4128 4137 rBV 209314 336743 9.16% 1.694% 80 14.011 4167 4174 4182 rVB5 8066 11863 0.32% 0.060% 81 14.062 4183 4190 4202 rVB8 5140 8305 0.23% 0.042% 82 14.159 4211 4220 4227 rBV4 3691 5368 0.15% 0.027% 83 14.339 4267 4276 4289 rBV4 8964 17994 0.49% 0.091% 84 14.435 4302 4306 4309 rBV3 1499 1275 0.03% 0.006% 85 14.538 4329 4338 4354 rVB2 49770 82003 2.23% 0.412% 86 14.680 4378 4382 4393 rVB7 3638 4765 0.13% 0.024% 87 14.824 4415 4427 4437 rBV 54615 92856 2.53% 0.467% 88 15.066 4490 4502 4529 rBV2 199552 351862 9.57% 1.770% 89 15.570 4649 4659 4664 rBV2 25047 39421 1.07% 0.198% 90 15.612 4664 4672 4684 rVV2 80420 125072 3.40% 0.629% 91 15.676 4686 4692 4699 rVB5 5766 8012 0.22% 0.040% 92 15.837 4734 4742 4757 rVB2 26217 40533 1.10% 0.204% 93 15.918 4758 4767 4774 rBV7 7830 14300 0.39% 0.072% 94 16.062 4803 4812 4822 rBV3 26230 43324 1.18% 0.218% 95 16.265 4866 4875 4879 rBV5 22049 35262 0.96% 0.177% 96 16.435 4919 4928 4942 rBV 52840 82327 2.24% 0.414% 97 16.528 4948 4957 4970 rVB2 23414 38144 1.04% 0.192% 98 16.744 5010 5024 5045 rBV 2348597 3676808 100.00% 18.493% 99 16.921 5070 5079 5092 rVB2 72865 113111 3.08% 0.569% 100 17.043 5108 5117 5134 rVB 87022 146173 3.98% 0.735% Sum of corrected areas: 19882109