LSC Area Percent Report Data Path : W:\HPCHEM1\MSVOA_U\Data\VU050718\ Data File : VU023723.D Acq On : 07 May 2018 19:29 Operator : MD/SY Sample : J2725-15 Misc : 5.0mL/MSVOA_U/WATER ALS Vial : 21 Sample Multiplier: 1 Integration Parameters: LSCINT.P Integrator: RTE Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 0 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Method : W:\HPCHEM1\MSVOA_U\METHOD\SOMULM050118WMA.M Title : VOC Analysis Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total --- ----- ----- ---- ---- --- ------- ------- ------ ------- 1 0.931 102 106 111 rBV2 233 270 0.01% 0.001% 2 1.088 148 155 171 rBV 556979 646869 14.29% 3.111% 3 1.185 180 185 198 rBV2 11885 18390 0.41% 0.088% 4 1.288 207 217 227 rBV 166632 472191 10.43% 2.271% 5 1.400 248 252 258 rVB 129081 114172 2.52% 0.549% 6 1.680 335 339 365 rVB 132212 195427 4.32% 0.940% 7 2.272 512 523 536 rBV 256378 386126 8.53% 1.857% 8 2.403 561 564 568 rBV3 388 381 0.01% 0.002% 9 2.445 568 577 586 rBV2 6736 12097 0.27% 0.058% 10 3.580 927 930 937 rVB 205 229 0.01% 0.001% 11 3.625 937 944 950 rBV2 161 217 0.00% 0.001% 12 3.969 1043 1051 1055 rBV 550 711 0.02% 0.003% 13 4.178 1101 1116 1153 rBV 127316 336131 7.43% 1.617% 14 4.558 1232 1234 1242 rVB2 300 373 0.01% 0.002% 15 4.654 1245 1264 1289 rBV 195863 461255 10.19% 2.219% 16 4.873 1330 1332 1334 rBV 393 255 0.01% 0.001% 17 4.992 1365 1369 1378 rBV4 674 770 0.02% 0.004% 18 5.345 1454 1479 1492 rBV2 397700 1212864 26.80% 5.834% 19 5.644 1567 1572 1582 rVB5 821 1471 0.03% 0.007% 20 5.751 1600 1605 1611 rBV3 277 384 0.01% 0.002% 21 5.786 1611 1616 1628 rBV3 641 1014 0.02% 0.005% 22 5.889 1632 1648 1677 rBV 432313 874624 19.33% 4.207% 23 6.194 1739 1743 1750 rBV4 658 857 0.02% 0.004% 24 6.336 1770 1787 1808 rBV 268248 552604 12.21% 2.658% 25 6.503 1837 1839 1849 rVB4 378 326 0.01% 0.002% 26 6.725 1904 1908 1911 rVV 207 196 0.00% 0.001% 27 6.744 1911 1914 1917 rVV 185 192 0.00% 0.001% 28 6.776 1921 1924 1930 rVV2 247 321 0.01% 0.002% 29 6.860 1944 1950 1951 rBV2 712 673 0.01% 0.003% 30 7.233 2054 2066 2096 rVV 146258 262073 5.79% 1.261% 31 7.387 2107 2114 2124 rVB4 887 1268 0.03% 0.006% 32 7.570 2156 2171 2185 rBV 546263 959824 21.21% 4.617% 33 7.641 2187 2193 2213 rVB 34920 63258 1.40% 0.304% 34 7.776 2229 2235 2241 rVB3 985 1419 0.03% 0.007% 35 7.853 2248 2259 2280 rBV 97791 166752 3.68% 0.802% 36 8.117 2334 2341 2343 rBV2 224 248 0.01% 0.001% 37 8.178 2353 2360 2361 rBV2 575 554 0.01% 0.003% 38 8.233 2373 2377 2383 rBV2 574 604 0.01% 0.003% 39 8.313 2390 2402 2433 rBV 434135 740987 16.37% 3.564% 40 9.001 2610 2616 2618 rBV 219 217 0.00% 0.001% 41 9.095 2632 2645 2683 rBV 635865 1061724 23.46% 5.107% 42 9.255 2683 2695 2714 rVV 112097 180785 3.99% 0.870% 43 9.381 2725 2734 2756 rVB 22499 38711 0.86% 0.186% 44 9.741 2841 2846 2850 rBV3 586 563 0.01% 0.003% 45 9.786 2850 2860 2872 rBV2 23441 38322 0.85% 0.184% 46 10.172 2968 2980 2990 rBV 12413 19478 0.43% 0.094% 47 10.435 3049 3062 3083 rBV 407809 638019 14.10% 3.069% 48 10.593 3101 3111 3129 rVB 8375 13358 0.30% 0.064% 49 10.712 3131 3148 3158 rVV 22575 41709 0.92% 0.201% 50 10.776 3161 3168 3177 rVB 5952 8570 0.19% 0.041% 51 10.975 3221 3230 3239 rVV2 8451 12780 0.28% 0.061% 52 11.104 3267 3270 3273 rBV 346 221 0.00% 0.001% 53 11.156 3278 3286 3296 rVV2 2993 4115 0.09% 0.020% 54 11.406 3353 3364 3377 rBV 27444 47579 1.05% 0.229% 55 11.487 3377 3389 3408 rVV 700402 1105251 24.42% 5.316% 56 11.573 3409 3416 3429 rVB2 8518 13547 0.30% 0.065% 57 11.770 3465 3477 3494 rBV 202919 333175 7.36% 1.603% 58 11.863 3494 3506 3530 rVV 620399 987749 21.83% 4.751% 59 11.985 3533 3544 3561 rVV 107282 166138 3.67% 0.799% 60 12.059 3564 3567 3577 rVB3 1564 2004 0.04% 0.010% 61 12.152 3589 3596 3602 rBV3 2334 3120 0.07% 0.015% 62 12.255 3619 3628 3636 rBV2 11006 15387 0.34% 0.074% 63 12.358 3648 3660 3673 rBV 138253 210705 4.66% 1.013% 64 12.483 3691 3699 3708 rBV7 3052 5270 0.12% 0.025% 65 12.545 3714 3718 3720 rBV2 761 609 0.01% 0.003% 66 12.599 3723 3735 3745 rVV 72960 113165 2.50% 0.544% 67 12.654 3747 3752 3757 rVV2 5203 6547 0.14% 0.031% 68 12.705 3757 3768 3784 rVV2 83536 179147 3.96% 0.862% 69 12.779 3785 3791 3802 rVB2 19164 29930 0.66% 0.144% 70 12.927 3833 3837 3841 rBV3 931 847 0.02% 0.004% 71 12.969 3842 3850 3858 rBV 14742 20825 0.46% 0.100% 72 13.123 3882 3898 3909 rBV4 21920 39210 0.87% 0.189% 73 13.191 3909 3919 3930 rVB3 24579 37903 0.84% 0.182% 74 13.294 3942 3951 3962 rVB4 23646 37804 0.84% 0.182% 75 13.461 3995 4003 4011 rBV2 9500 16004 0.35% 0.077% 76 13.554 4024 4032 4045 rBV 17803 30387 0.67% 0.146% 77 13.744 4077 4091 4113 rBV 871654 1454013 32.13% 6.994% 78 13.863 4115 4128 4137 rBV 211050 346016 7.65% 1.664% 79 14.008 4167 4173 4182 rVB4 8850 12801 0.28% 0.062% 80 14.059 4184 4189 4202 rVB6 5301 8243 0.18% 0.040% 81 14.155 4212 4219 4225 rBV5 3228 5067 0.11% 0.024% 82 14.339 4267 4276 4289 rBV3 10250 18915 0.42% 0.091% 83 14.435 4301 4306 4311 rBV4 1659 1972 0.04% 0.009% 84 14.538 4329 4338 4354 rVB3 49146 79840 1.76% 0.384% 85 14.683 4377 4383 4391 rBV6 3817 5123 0.11% 0.025% 86 14.824 4414 4427 4437 rBV 60936 101215 2.24% 0.487% 87 15.065 4491 4502 4517 rBV2 191820 337896 7.47% 1.625% 88 15.567 4649 4658 4664 rBV2 25761 42440 0.94% 0.204% 89 15.612 4665 4672 4685 rVB 90367 136347 3.01% 0.656% 90 15.676 4685 4692 4699 rBV4 7029 9870 0.22% 0.047% 91 15.782 4723 4725 4726 rBV 865 368 0.01% 0.002% 92 15.840 4734 4743 4753 rVB 30155 46701 1.03% 0.225% 93 15.917 4759 4767 4774 rBV6 8228 14327 0.32% 0.069% 94 16.062 4803 4812 4822 rVB4 28054 47136 1.04% 0.227% 95 16.265 4866 4875 4879 rBV2 27650 43972 0.97% 0.211% 96 16.435 4918 4928 4939 rBV 67865 105120 2.32% 0.506% 97 16.528 4947 4957 4970 rBV 40733 67724 1.50% 0.326% 98 16.741 5010 5023 5045 rBV 2880005 4525613 100.00% 21.767% 99 16.921 5070 5079 5092 rVB 96277 149555 3.30% 0.719% 100 17.043 5106 5117 5144 rVB 164466 281191 6.21% 1.352% Sum of corrected areas: 20790717