LSC Area Percent Report Data Path : W:\HPCHEM1\MSVOA_U\DATA\VU050818\ Data File : VU023742.D Acq On : 08 May 2018 17:24 Operator : MD/SY Sample : J2725-13 50X Misc : 5.0mL/MSVOA_U/WATER ALS Vial : 18 Sample Multiplier: 1 Integration Parameters: LSCINT.P Integrator: RTE Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 0 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Method : W:\HPCHEM1\MSVOA_U\METHOD\SOMULM050818WMA.M Title : VOC Analysis Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total --- ----- ----- ---- ---- --- ------- ------- ------ ------- 1 0.735 39 45 50 rVB2 179 220 0.00% 0.001% 2 0.789 57 62 69 rBV2 127 160 0.00% 0.001% 3 1.088 137 155 178 rBV 1639124 1842045 31.65% 7.716% 4 1.182 180 184 195 rVB2 7134 10337 0.18% 0.043% 5 1.397 245 251 271 rBV 255846 285618 4.91% 1.196% 6 1.680 332 339 362 rVB 183737 239796 4.12% 1.004% 7 2.272 512 523 536 rBV 413843 623550 10.71% 2.612% 8 2.371 551 554 558 rBV4 664 622 0.01% 0.003% 9 2.436 572 574 575 rBV4 341 150 0.00% 0.001% 10 2.477 581 587 597 rVB3 1471 1859 0.03% 0.008% 11 3.394 865 872 879 rVB3 731 1161 0.02% 0.005% 12 3.500 899 905 908 rVB2 142 133 0.00% 0.001% 13 3.667 953 957 962 rVB2 143 134 0.00% 0.001% 14 3.792 993 996 1000 rVB2 219 162 0.00% 0.001% 15 4.178 1101 1116 1155 rBV 170131 449773 7.73% 1.884% 16 4.471 1204 1207 1212 rVB2 285 234 0.00% 0.001% 17 4.651 1245 1263 1297 rBV 285807 670632 11.52% 2.809% 18 4.886 1330 1336 1341 rBV3 693 1006 0.02% 0.004% 19 4.992 1362 1369 1373 rVB 272 360 0.01% 0.002% 20 5.018 1373 1377 1381 rVB 192 146 0.00% 0.001% 21 5.056 1384 1389 1393 rBV2 689 714 0.01% 0.003% 22 5.217 1435 1439 1443 rBV2 144 150 0.00% 0.001% 23 5.342 1453 1478 1486 rBV2 603473 1751896 30.10% 7.339% 24 5.648 1561 1573 1589 rVB 14669 32147 0.55% 0.135% 25 5.744 1600 1603 1606 rBV3 306 244 0.00% 0.001% 26 5.783 1612 1615 1617 rBV 299 166 0.00% 0.001% 27 5.889 1634 1648 1687 rBV 307783 629317 10.81% 2.636% 28 6.072 1703 1705 1710 rVB2 375 273 0.00% 0.001% 29 6.133 1722 1724 1731 rVB2 273 204 0.00% 0.001% 30 6.181 1731 1739 1741 rBV3 1388 1777 0.03% 0.007% 31 6.226 1750 1753 1760 rVB 173 157 0.00% 0.001% 32 6.268 1762 1766 1769 rBV2 220 156 0.00% 0.001% 33 6.336 1772 1787 1813 rBV 395379 802536 13.79% 3.362% 34 6.850 1943 1947 1948 rBV 228 146 0.00% 0.001% 35 6.866 1950 1952 1956 rVB2 407 262 0.00% 0.001% 36 7.072 2012 2016 2020 rBV2 158 136 0.00% 0.001% 37 7.146 2033 2039 2042 rVB3 194 227 0.00% 0.001% 38 7.230 2052 2065 2095 rBV 213441 385669 6.63% 1.616% 39 7.329 2095 2096 2100 rVV2 953 427 0.01% 0.002% 40 7.345 2100 2101 2106 rVB2 301 162 0.00% 0.001% 41 7.448 2128 2133 2135 rBV2 291 255 0.00% 0.001% 42 7.570 2156 2171 2183 rBV 809078 1419510 24.39% 5.946% 43 7.641 2184 2193 2225 rVB 320057 582866 10.02% 2.442% 44 7.853 2246 2259 2278 rBV 150714 255264 4.39% 1.069% 45 7.943 2284 2287 2299 rVB2 4952 7074 0.12% 0.030% 46 8.175 2356 2359 2362 rBV 292 171 0.00% 0.001% 47 8.226 2373 2375 2377 rVV 269 129 0.00% 0.001% 48 8.313 2390 2402 2440 rBV 585184 992489 17.05% 4.157% 49 8.622 2493 2498 2502 rBV2 529 589 0.01% 0.002% 50 8.953 2598 2601 2604 rVV 204 133 0.00% 0.001% 51 8.982 2607 2610 2614 rVB 163 140 0.00% 0.001% 52 9.014 2617 2620 2624 rBV 164 131 0.00% 0.001% 53 9.095 2631 2645 2676 rBV 449129 764908 13.14% 3.204% 54 9.255 2684 2695 2715 rVB 75439 123327 2.12% 0.517% 55 9.377 2721 2733 2755 rBV 195634 324371 5.57% 1.359% 56 9.545 2778 2785 2787 rBV2 1608 1750 0.03% 0.007% 57 9.638 2810 2814 2817 rBV 169 134 0.00% 0.001% 58 9.738 2839 2845 2848 rVV2 1131 1467 0.03% 0.006% 59 9.783 2848 2859 2888 rVB 111862 186078 3.20% 0.779% 60 9.918 2898 2901 2907 rVB2 175 200 0.00% 0.001% 61 10.014 2926 2931 2937 rBV2 544 639 0.01% 0.003% 62 10.172 2971 2980 2990 rBV2 4555 6302 0.11% 0.026% 63 10.435 3049 3062 3084 rBV 542811 868128 14.92% 3.637% 64 10.529 3088 3091 3097 rVB2 327 255 0.00% 0.001% 65 10.561 3097 3101 3105 rBV2 133 149 0.00% 0.001% 66 10.590 3105 3110 3112 rBV2 806 701 0.01% 0.003% 67 10.686 3131 3140 3145 rBV2 12569 19374 0.33% 0.081% 68 10.776 3158 3168 3177 rBV 14635 20875 0.36% 0.087% 69 10.975 3222 3230 3245 rBV2 2862 4942 0.08% 0.021% 70 11.091 3263 3266 3269 rVB 408 255 0.00% 0.001% 71 11.152 3275 3285 3303 rVB 47696 71535 1.23% 0.300% 72 11.223 3303 3307 3310 rBV3 484 423 0.01% 0.002% 73 11.278 3321 3324 3329 rBV2 269 172 0.00% 0.001% 74 11.403 3351 3363 3377 rVV 248279 393724 6.77% 1.649% 75 11.487 3377 3389 3406 rVV 525331 830719 14.27% 3.480% 76 11.574 3407 3416 3427 rVV 26916 40856 0.70% 0.171% 77 11.631 3429 3434 3443 rVB2 1472 1881 0.03% 0.008% 78 11.770 3465 3477 3493 rBV 317243 487256 8.37% 2.041% 79 11.863 3493 3506 3526 rVB 883492 1408611 24.21% 5.901% 80 11.985 3531 3544 3567 rBV 429965 675849 11.61% 2.831% 81 12.255 3622 3628 3634 rBV2 1529 1842 0.03% 0.008% 82 12.358 3651 3660 3673 rBV 8796 13112 0.23% 0.055% 83 12.483 3691 3699 3707 rBV7 1728 2747 0.05% 0.012% 84 12.599 3722 3735 3748 rVB3 23085 38674 0.66% 0.162% 85 12.702 3752 3767 3777 rBV2 56456 112861 1.94% 0.473% 86 12.969 3842 3850 3862 rBV2 7785 10770 0.19% 0.045% 87 13.098 3881 3890 3892 rBV4 4284 5517 0.09% 0.023% 88 13.127 3893 3899 3910 rVV2 13530 20791 0.36% 0.087% 89 13.191 3911 3919 3928 rVB4 8862 13666 0.23% 0.057% 90 13.297 3942 3952 3963 rBV4 10761 16695 0.29% 0.070% 91 13.509 4013 4018 4025 rVB5 1015 1370 0.02% 0.006% 92 13.615 4048 4051 4052 rBV 508 283 0.00% 0.001% 93 13.747 4078 4092 4116 rBV 3710762 5819500 100.00% 24.378% 94 13.866 4118 4129 4140 rBV 171381 266785 4.58% 1.118% 95 14.059 4185 4189 4197 rBV6 847 820 0.01% 0.003% 96 14.824 4421 4427 4435 rBV2 2261 3296 0.06% 0.014% 97 14.882 4435 4445 4465 rVB 85501 137779 2.37% 0.577% 98 15.065 4492 4502 4521 rVB 91166 149556 2.57% 0.626% 99 15.618 4669 4674 4690 rVB4 2827 4856 0.08% 0.020% 100 16.747 5017 5025 5036 rBV 15056 23007 0.40% 0.096% Sum of corrected areas: 23872423