LSC Area Percent Report Data Path : W:\HPCHEM1\MSVOA_U\Data\VU050818\ Data File : VU023745.D Acq On : 08 May 2018 19:10 Operator : MD/SY Sample : J2725-10DL 5X Misc : 5.0mL/MSVOA_U/WATER ALS Vial : 22 Sample Multiplier: 1 Integration Parameters: LSCINT.P Integrator: RTE Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 0 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Method : W:\HPCHEM1\MSVOA_U\METHOD\SOMULM050818WMA.M Title : VOC Analysis Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total --- ----- ----- ---- ---- --- ------- ------- ------ ------- 1 1.088 134 155 173 rBV 598514 681020 4.49% 0.999% 2 1.182 180 184 196 rVB4 6792 9290 0.06% 0.014% 3 1.297 208 220 227 rBV 38387 91040 0.60% 0.133% 4 1.397 246 251 270 rVB 182540 199910 1.32% 0.293% 5 1.680 332 339 358 rVB 135980 176500 1.16% 0.259% 6 2.272 512 523 537 rBV 293945 441508 2.91% 0.647% 7 2.455 572 580 581 rBV3 1571 1886 0.01% 0.003% 8 2.834 695 698 704 rBV4 1036 1375 0.01% 0.002% 9 3.381 865 868 878 rVB3 816 1195 0.01% 0.002% 10 4.178 1102 1116 1149 rBV 127300 338614 2.23% 0.496% 11 4.651 1245 1263 1286 rBV 207901 484902 3.20% 0.711% 12 4.879 1329 1334 1335 rBV2 401 377 0.00% 0.001% 13 4.892 1336 1338 1345 rVB4 641 632 0.00% 0.001% 14 4.992 1363 1369 1371 rBV4 977 1040 0.01% 0.002% 15 5.342 1450 1478 1489 rBV2 429753 1289445 8.51% 1.891% 16 5.645 1565 1572 1578 rBV3 889 1429 0.01% 0.002% 17 5.889 1633 1648 1693 rBV 399134 815308 5.38% 1.195% 18 6.185 1736 1740 1744 rBV5 746 827 0.01% 0.001% 19 6.204 1744 1746 1751 rVB3 877 582 0.00% 0.001% 20 6.336 1772 1787 1807 rBV 286748 577670 3.81% 0.847% 21 6.866 1948 1952 1956 rVB2 438 340 0.00% 0.000% 22 6.905 1959 1964 1969 rBV2 631 777 0.01% 0.001% 23 7.230 2053 2065 2086 rBV 155101 278969 1.84% 0.409% 24 7.571 2156 2171 2183 rBV 568191 1009256 6.66% 1.480% 25 7.641 2184 2193 2227 rVB 207215 395526 2.61% 0.580% 26 7.853 2247 2259 2278 rBV 105205 182264 1.20% 0.267% 27 8.233 2370 2377 2387 rVB5 1104 1574 0.01% 0.002% 28 8.313 2387 2402 2442 rBV 411279 728939 4.81% 1.069% 29 8.712 2516 2526 2529 rBV2 259 436 0.00% 0.001% 30 9.095 2632 2645 2680 rBV 577636 995490 6.57% 1.460% 31 9.252 2681 2694 2719 rVV 1033463 1696990 11.20% 2.488% 32 9.378 2721 2733 2766 rVB 669263 1124933 7.42% 1.649% 33 9.551 2778 2787 2802 rVB3 10448 18910 0.12% 0.028% 34 9.651 2812 2818 2819 rBV3 560 441 0.00% 0.001% 35 9.738 2837 2845 2848 rBV3 5268 6979 0.05% 0.010% 36 9.783 2848 2859 2893 rVB 568410 922655 6.09% 1.353% 37 10.014 2923 2931 2941 rBV4 3266 4960 0.03% 0.007% 38 10.172 2968 2980 3001 rBV 87281 140703 0.93% 0.206% 39 10.384 3043 3046 3049 rBV 338 292 0.00% 0.000% 40 10.435 3049 3062 3080 rBV 402849 639691 4.22% 0.938% 41 10.516 3080 3087 3095 rVB4 3124 4123 0.03% 0.006% 42 10.593 3099 3111 3127 rBV 29437 45617 0.30% 0.067% 43 10.686 3128 3140 3145 rBV 120650 202003 1.33% 0.296% 44 10.776 3158 3168 3183 rVB 122842 186137 1.23% 0.273% 45 10.895 3199 3205 3217 rVB4 2078 3212 0.02% 0.005% 46 10.976 3218 3230 3235 rBV 69831 115804 0.76% 0.170% 47 11.152 3263 3285 3297 rBV 759192 1155002 7.62% 1.694% 48 11.220 3297 3306 3315 rVV 69143 106813 0.70% 0.157% 49 11.271 3315 3322 3332 rVV2 21052 33060 0.22% 0.048% 50 11.329 3332 3340 3352 rVB 16826 24498 0.16% 0.036% 51 11.403 3352 3363 3377 rBV 388099 617846 4.08% 0.906% 52 11.487 3377 3389 3404 rVV 725605 1139802 7.52% 1.671% 53 11.574 3404 3416 3427 rVV 378584 580526 3.83% 0.851% 54 11.631 3427 3434 3445 rVB 26997 41065 0.27% 0.060% 55 11.693 3445 3453 3462 rVB4 4649 7229 0.05% 0.011% 56 11.770 3462 3477 3495 rBV 3757756 5798007 38.25% 8.501% 57 11.863 3495 3506 3523 rVB 658740 1058072 6.98% 1.551% 58 11.985 3530 3544 3564 rBV 7864943 12013665 79.26% 17.615% 59 12.152 3588 3596 3600 rBV2 9343 13947 0.09% 0.020% 60 12.255 3613 3628 3635 rBV 49661 82207 0.54% 0.121% 61 12.358 3650 3660 3675 rBV 86545 135291 0.89% 0.198% 62 12.429 3676 3682 3691 rVB5 6103 8468 0.06% 0.012% 63 12.487 3692 3700 3708 rVB9 3741 6477 0.04% 0.009% 64 12.596 3712 3734 3745 rBV 690692 1051122 6.93% 1.541% 65 12.654 3745 3752 3755 rBV 39969 48549 0.32% 0.071% 66 12.699 3755 3766 3778 rBV 1065932 2126039 14.03% 3.117% 67 12.779 3786 3791 3802 rVB 170949 243123 1.60% 0.356% 68 12.889 3817 3825 3834 rVB5 8284 13721 0.09% 0.020% 69 12.969 3839 3850 3869 rVB 126409 193979 1.28% 0.284% 70 13.127 3884 3899 3909 rBV2 322492 515878 3.40% 0.756% 71 13.188 3909 3918 3931 rVB 379020 574394 3.79% 0.842% 72 13.297 3939 3952 3970 rVB 519425 844498 5.57% 1.238% 73 13.393 3974 3982 3990 rBV4 8821 14233 0.09% 0.021% 74 13.461 3997 4003 4009 rBV3 6323 10183 0.07% 0.015% 75 13.557 4027 4033 4039 rBV3 4270 6286 0.04% 0.009% 76 13.676 4064 4070 4076 rVB5 2126 2700 0.02% 0.004% 77 13.747 4077 4092 4113 rBV 9493874 15158042 100.00% 22.226% 78 13.863 4114 4128 4138 rBV 2225243 3517877 23.21% 5.158% 79 13.953 4152 4156 4165 rVB 42773 54531 0.36% 0.080% 80 14.059 4183 4189 4202 rVB2 19218 29326 0.19% 0.043% 81 14.152 4209 4218 4225 rBV3 10473 18169 0.12% 0.027% 82 14.345 4267 4278 4287 rBV5 17534 34752 0.23% 0.051% 83 14.538 4329 4338 4349 rVB2 44789 70993 0.47% 0.104% 84 14.680 4374 4382 4392 rBV2 15121 21223 0.14% 0.031% 85 14.734 4394 4399 4411 rVB4 5514 8351 0.06% 0.012% 86 14.824 4413 4427 4436 rBV 118246 202448 1.34% 0.297% 87 14.882 4436 4445 4470 rVB2 88466 173076 1.14% 0.254% 88 14.995 4471 4480 4489 rBV 24280 37602 0.25% 0.055% 89 15.065 4489 4502 4518 rBV 2801452 4376830 28.87% 6.418% 90 15.561 4649 4656 4661 rBV3 5543 8592 0.06% 0.013% 91 15.612 4662 4672 4685 rVB 198325 302499 2.00% 0.444% 92 15.802 4717 4731 4736 rBV5 11150 21986 0.15% 0.032% 93 15.921 4756 4768 4791 rVB 103762 187038 1.23% 0.274% 94 16.065 4802 4813 4820 rBV 144435 235440 1.55% 0.345% 95 16.268 4867 4876 4877 rBV3 17749 20614 0.14% 0.030% 96 16.438 4919 4929 4940 rVB 34615 53359 0.35% 0.078% 97 16.532 4949 4958 4972 rVB3 14349 26348 0.17% 0.039% 98 16.744 5011 5024 5045 rBV 783432 1255300 8.28% 1.841% 99 16.921 5075 5079 5092 rVB3 8719 11336 0.07% 0.017% 100 17.043 5108 5117 5140 rVB 48263 86649 0.57% 0.127% Sum of corrected areas: 68200632