LSC Area Percent Report Data Path : W:\HPCHEM1\MSVOA_U\Data\VU050818\ Data File : VU023751.D Acq On : 08 May 2018 21:48 Operator : MD/SY Sample : J2725-10 Misc : 5.0mL/MSVOA_U/WATER ALS Vial : 28 Sample Multiplier: 1 Integration Parameters: LSCINT.P Integrator: RTE Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 0 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Method : W:\HPCHEM1\MSVOA_U\METHOD\SOMULM050818WMA.M Title : VOC Analysis Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total --- ----- ----- ---- ---- --- ------- ------- ------ ------- 1 1.059 138 146 147 rBV 1473 1420 0.00% 0.000% 2 1.088 147 155 172 rBV 971071 1084864 1.43% 0.321% 3 1.156 173 176 180 rBV 6507 5442 0.01% 0.002% 4 1.182 181 184 188 rBV 6090 5638 0.01% 0.002% 5 1.275 204 213 221 rBV 1560056 2222097 2.93% 0.657% 6 1.680 334 339 358 rVB 149435 201022 0.27% 0.059% 7 2.272 513 523 536 rVB 296257 446308 0.59% 0.132% 8 2.448 570 578 582 rBV3 2320 3445 0.00% 0.001% 9 4.027 1065 1069 1076 rBV 454 608 0.00% 0.000% 10 4.104 1082 1093 1101 rVB3 1507 3082 0.00% 0.001% 11 4.178 1101 1116 1145 rBV 133698 347013 0.46% 0.103% 12 4.651 1244 1263 1289 rBV 218040 514147 0.68% 0.152% 13 4.889 1330 1337 1338 rBV2 456 503 0.00% 0.000% 14 5.001 1360 1372 1384 rVB5 2454 5252 0.01% 0.002% 15 5.345 1454 1479 1486 rBV2 469303 1362528 1.80% 0.403% 16 5.644 1561 1572 1588 rVB2 7524 16561 0.02% 0.005% 17 5.889 1634 1648 1677 rBV 432515 862449 1.14% 0.255% 18 6.194 1735 1743 1751 rVB4 1491 2364 0.00% 0.001% 19 6.336 1772 1787 1808 rBV 311756 622064 0.82% 0.184% 20 7.233 2052 2066 2090 rVV 171682 303732 0.40% 0.090% 21 7.570 2157 2171 2182 rBV 615161 1088025 1.43% 0.322% 22 7.641 2182 2193 2227 rVB 1153684 2086742 2.75% 0.617% 23 7.853 2248 2259 2278 rVV 118264 198616 0.26% 0.059% 24 7.943 2279 2287 2300 rVV2 9614 16231 0.02% 0.005% 25 8.098 2329 2335 2338 rBV4 410 499 0.00% 0.000% 26 8.178 2354 2360 2370 rBV3 630 1144 0.00% 0.000% 27 8.313 2390 2402 2441 rBV 451640 789308 1.04% 0.233% 28 9.094 2631 2645 2680 rVV 604094 1059316 1.40% 0.313% 29 9.255 2680 2695 2719 rVV 6040552 9877414 13.02% 2.921% 30 9.377 2721 2733 2771 rVV 3875885 6536768 8.62% 1.933% 31 9.548 2774 2786 2809 rVB3 66688 131430 0.17% 0.039% 32 9.738 2835 2845 2848 rBV2 36131 50727 0.07% 0.015% 33 9.783 2848 2859 2893 rVB 3349750 5496054 7.25% 1.625% 34 10.014 2920 2931 2950 rVB 24126 39273 0.05% 0.012% 35 10.172 2967 2980 3003 rBV 533128 865244 1.14% 0.256% 36 10.313 3016 3024 3031 rVB4 2349 3726 0.00% 0.001% 37 10.435 3050 3062 3077 rBV 425388 679644 0.90% 0.201% 38 10.512 3077 3086 3097 rVB2 22183 34072 0.04% 0.010% 39 10.593 3099 3111 3125 rBV 196022 302144 0.40% 0.089% 40 10.686 3126 3140 3145 rBV 808835 1336347 1.76% 0.395% 41 10.776 3158 3168 3181 rVB 804951 1209691 1.59% 0.358% 42 10.840 3182 3188 3195 rBV4 6641 10788 0.01% 0.003% 43 10.895 3199 3205 3216 rVB 20865 32679 0.04% 0.010% 44 10.975 3218 3230 3234 rBV 449583 680828 0.90% 0.201% 45 11.152 3262 3285 3297 rBV 4651328 7122828 9.39% 2.106% 46 11.220 3297 3306 3315 rVV 479143 724573 0.96% 0.214% 47 11.271 3315 3322 3331 rVB 162842 236912 0.31% 0.070% 48 11.329 3331 3340 3350 rVB 103543 157784 0.21% 0.047% 49 11.403 3351 3363 3378 rBV 2213428 3542184 4.67% 1.047% 50 11.487 3378 3389 3404 rVB2 870531 1439851 1.90% 0.426% 51 11.577 3404 3417 3427 rBV 2241896 3455848 4.56% 1.022% 52 11.635 3427 3435 3446 rVB 194007 294939 0.39% 0.087% 53 11.696 3446 3454 3463 rVB 32223 48483 0.06% 0.014% 54 11.776 3463 3479 3497 rBV 20080912 31864110 42.01% 9.422% 55 11.866 3497 3507 3524 rVB2 727349 1257766 1.66% 0.372% 56 11.998 3525 3548 3564 rBV2 37579150 64533099 85.08% 19.081% 57 12.152 3587 3596 3600 rBV 63954 96785 0.13% 0.029% 58 12.255 3612 3628 3635 rBV 324578 550110 0.73% 0.163% 59 12.358 3650 3660 3675 rBV 513257 823758 1.09% 0.244% 60 12.483 3691 3699 3709 rVB6 24299 46414 0.06% 0.014% 61 12.599 3710 3735 3745 rBV 4144034 6375251 8.40% 1.885% 62 12.657 3746 3753 3756 rVV 296469 409635 0.54% 0.121% 63 12.702 3756 3767 3786 rVV 6424099 14467652 19.07% 4.278% 64 12.779 3787 3791 3802 rVB 1012784 1362671 1.80% 0.403% 65 12.882 3818 3823 3832 rVB3 32345 44560 0.06% 0.013% 66 12.969 3833 3850 3867 rVV 832277 1259888 1.66% 0.373% 67 13.126 3881 3899 3909 rBV2 1999694 3188747 4.20% 0.943% 68 13.191 3909 3919 3931 rVB 2596747 3915449 5.16% 1.158% 69 13.297 3940 3952 3970 rVB 3324446 5316639 7.01% 1.572% 70 13.393 3972 3982 3995 rBV2 60370 114402 0.15% 0.034% 71 13.464 3996 4004 4009 rBV2 49392 75849 0.10% 0.022% 72 13.615 4043 4051 4067 rVB4 149635 281850 0.37% 0.083% 73 13.760 4078 4096 4113 rBV2 40874267 75853259 100.00% 22.428% 74 13.872 4113 4131 4140 rBV 12140547 20041782 26.42% 5.926% 75 13.953 4151 4156 4166 rVB 301912 443860 0.59% 0.131% 76 14.007 4166 4173 4182 rVB3 131113 186005 0.25% 0.055% 77 14.059 4183 4189 4207 rVB 131060 202466 0.27% 0.060% 78 14.155 4208 4219 4225 rBV2 76899 139531 0.18% 0.041% 79 14.345 4267 4278 4287 rBV3 128694 258877 0.34% 0.077% 80 14.538 4329 4338 4349 rVB2 291735 475003 0.63% 0.140% 81 14.679 4375 4382 4392 rVB2 90061 129917 0.17% 0.038% 82 14.734 4393 4399 4411 rVV2 39971 67220 0.09% 0.020% 83 14.824 4413 4427 4436 rVV 779265 1336957 1.76% 0.395% 84 14.879 4436 4444 4470 rVB2 604558 1200328 1.58% 0.355% 85 14.995 4471 4480 4489 rBV 168256 273746 0.36% 0.081% 86 15.068 4489 4503 4534 rVB 15666941 25397334 33.48% 7.510% 87 15.451 4614 4622 4639 rVB 6573 17302 0.02% 0.005% 88 15.557 4645 4655 4661 rBV 85898 146229 0.19% 0.043% 89 15.612 4662 4672 4684 rVB 1603064 2423937 3.20% 0.717% 90 15.673 4685 4691 4698 rVV4 23987 33423 0.04% 0.010% 91 15.802 4714 4731 4736 rBV5 100919 215119 0.28% 0.064% 92 15.917 4755 4767 4790 rVB 1014773 1758870 2.32% 0.520% 93 16.062 4791 4812 4819 rBV 1192408 1943758 2.56% 0.575% 94 16.294 4865 4884 4903 rVB 327575 785922 1.04% 0.232% 95 16.435 4917 4928 4941 rBV 322520 502952 0.66% 0.149% 96 16.531 4947 4958 4973 rVB3 143867 290664 0.38% 0.086% 97 16.638 4983 4991 5000 rVB3 38731 60349 0.08% 0.018% 98 16.744 5010 5024 5044 rBV 5771478 9205091 12.14% 2.722% 99 16.920 5070 5079 5090 rBV2 80614 129396 0.17% 0.038% 100 17.039 5104 5116 5138 rBV 707435 1136142 1.50% 0.336% Sum of corrected areas: 338200725