Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_U\DATA\VU051418\ Data File : VU023849.D Acq On : 14 May 2018 12:12 Operator : MD/SY Sample : VU0514WBS01 Misc : 25.0mL/MSVOA_U/WATER ALS Vial : 4 Sample Multiplier: 1 Quant Time: May 15 04:22:10 2018 Quant Method : W:\HPCHEM1\MSVOA_U\METHOD\524U043018DW.M Quant Title : METHOD 524.2 VOLATILES DRINKING WATER QLast Update : Thu May 03 10:23:54 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Fluorobenzene 5.75 96 40332 1.00 ug/l 0.00 System Monitoring Compounds 57) 4-Bromofluorobenzene 10.31 95 14266 1.08 ug/l 0.00 Spiked Amount 1.000 Recovery = 108.00% 68) 1,2-Dichlorobenzene-d4 11.86 152 15208 1.19 ug/l 0.00 Spiked Amount 1.000 Recovery = 119.00% Target Compounds Qvalue 2) Dichlorodifluoromethane 1.21 85 29058 2.219 ug/l 98 3) Chloromethane 1.33 50 33761 2.225 ug/l 98 4) Vinyl Chloride 1.40 62 32946 2.263 ug/l 99 5) Bromomethane 1.63 94 16256 2.089 ug/l 99 6) Chloroethane 1.70 64 19813 2.445 ug/l 98 7) Trichlorofluoromethane 1.89 101 40314 2.413 ug/l 99 8) 1,1,2-Trichloro-1,2,2-trif 2.29 101 23949 2.333 ug/l 96 9) 1,1-Dichloroethene 2.29 96 21438 2.249 ug/l 94 10) Iodomethane 2.41 142 12546 1.107 ug/l 98 11) Allyl Chloride 2.60 41 42533 2.428 ug/l 96 12) Acrylonitrile 2.94 53 10284 5.229 ug/l 95 13) Acetone 2.33 43 49556 29.689 ug/l 95 14) Carbon Disulfide 2.48 76 73832 2.355 ug/l 97 15) Methylene Chloride 2.70 84 25385 2.339 ug/l 95 16) trans-1,2-Dichloroethene 2.99 96 23294 2.281 ug/l 98 17) 1,1-Dichloroethane 3.45 63 47158 2.345 ug/l 99 18) 2-Butanone 4.28 43 43909 16.279 ug/l 99 19) Cyclohexane 5.00 56 30344 1.746 ug/l 95 20) Methylcyclohexane 6.42 83 32833 1.852 ug/l 96 21) 2,2-Dichloropropane 4.23 77 33172 2.080 ug/l # 76 22) cis-1,2-Dichloroethene 4.23 96 23816 2.155 ug/l 97 23) Diethyl Ether 2.10 59 18016 2.312 ug/l 97 24) tert-Butyl Alcohol 2.84 59 17163 29.213 ug/l # 82 25) Methyl tert-Butyl Ether 3.00 73 53604 2.238 ug/l 93 26) Bromochloromethane 4.55 128 10414 2.385 ug/l 94 27) Chloroform 4.68 83 42855 2.263 ug/l 100 28) 1,1,1-Trichloroethane 4.92 97 33629 2.164 ug/l 98 29) 1,1-Dichloropropene 5.14 75 31449 2.063 ug/l 99 30) Carbon Tetrachloride 5.14 117 28361 2.170 ug/l 98 31) Isopropyl Ether 3.58 45 68230 2.010 ug/l 94 32) Ethyl-t-butyl ether 4.08 59 54267 1.871 ug/l 99 33) Tert-Amyl methyl ether 5.59 73 42709 1.739 ug/l 98 34) Propionitrile 4.34 54 9072 11.813 ug/l # 85 35) Benzene 5.39 78 90589 1.999 ug/l 99 36) 1,2-Dichloroethane 5.41 62 25065 1.956 ug/l 98 37) Trichloroethene 6.19 130 23650 1.944 ug/l 100 38) 1,2-Dichloropropane 6.44 63 24635 1.982 ug/l 100 39) Methacrylonitrile 4.55 41 7453 1.898 ug/l 97 40) Methyl acrylate 4.44 55 10769 1.977 ug/l # 95 41) Tetrahydrofuran 4.65 42 7854 3.882 ug/l 99 42) 1-Chlorobutane 5.07 56 42132 1.907 ug/l 99 43) Dibromomethane 6.56 93 11019 2.062 ug/l 98 44) Bromodichloromethane 6.76 83 27593 2.054 ug/l 97 45) 4-Methyl-2-Pentanone 7.47 43 64841 10.264 ug/l 98 46) t-1,4-Dichloro-2-butene 10.52 75 7887m 4.223 ug/l 47) Methyl methacrylate 6.63 69 18779 3.878 ug/l 97 48) Ethyl methacrylate 8.02 69 15590 1.841 ug/l 100 49) Toluene 7.64 92 51228 1.957 ug/l 97 50) t-1,3-Dichloropropene 7.89 75 22267 1.942 ug/l 96 51) cis-1,3-Dichloropropene 7.27 75 28021 1.878 ug/l 97 52) 1,1,2-Trichloroethane 8.07 97 15402 2.025 ug/l 98 53) 1,3-Dichloropropane 8.25 76 26941 1.993 ug/l 98 54) 2-Hexanone 8.37 43 58312 13.551 ug/l 97 55) Dibromochloromethane 8.48 129 17287 2.074 ug/l 99 56) 1,2-Dibromoethane 8.59 107 13678 2.087 ug/l 99 58) Tetrachloroethene 8.23 164 22832 2.059 ug/l 97 59) Chlorobenzene 9.12 112 56215 2.007 ug/l 99 60) 1,1,1,2-Tetrachloroethane 9.21 131 19929 2.094 ug/l 97 61) Pentachloroethane 11.10 117 16406 2.429 ug/l 93 62) Hexachloroethane 12.15 117 15108 2.331 ug/l 97 63) Ethyl Benzene 9.25 91 90101 1.935 ug/l 98 64) m/p-Xylenes 9.38 106 72035 4.011 ug/l 98 65) o-Xylene 9.78 106 35349 2.044 ug/l 100 66) Styrene 9.80 104 57675 2.022 ug/l 99 67) Bromoform 9.96 173 9299 2.137 ug/l 96 69) Isopropylbenzene 10.17 105 89258 2.004 ug/l 99 70) 1,1,2,2-Tetrachloroethane 10.46 83 19655 2.293 ug/l 100 71) 1,2,3-Trichloropropane 10.50 75 23218 3.785 ug/l # 75 72) Bromobenzene 10.46 156 24691 2.226 ug/l 100 73) n-propylbenzene 10.59 120 26575 2.158 ug/l 97 74) 2-Chlorotoluene 10.66 126 23475 2.156 ug/l 95 75) 1,3,5-Trimethylbenzene 10.78 105 81218 2.164 ug/l 100 76) 4-Chlorotoluene 10.78 126 25907 2.297 ug/l 94 77) tert-Butylbenzene 11.10 119 77744 2.211 ug/l 98 78) 1,2,4-Trimethylbenzene 11.15 105 83228 2.197 ug/l 100 79) sec-Butylbenzene 11.33 105 108461 2.203 ug/l 100 80) Nitrobenzene 12.88 77 2280 8.506 ug/l # 91 81) p-Isopropyltoluene 11.48 119 90687 2.241 ug/l 99 82) 1,3-Dichlorobenzene 11.42 146 51742 2.338 ug/l 100 83) 1,4-Dichlorobenzene 11.51 146 52851 2.391 ug/l 100 84) n-Butylbenzene 11.90 91 87502 2.215 ug/l 97 85) 1,2-Dichlorobenzene 11.88 146 46487 2.326 ug/l 99 86) 1,2-Dibromo-3-Chloropropan 12.66 75 2660 2.199 ug/l 90 87) 1,2,4-Trichlorobenzene 13.51 180 29773 2.060 ug/l 99 88) Hexachlorobutadiene 13.70 225 22534 2.571 ug/l 99 89) Naphthalene 13.75 128 36757 1.689 ug/l 100 90) 1,2,3-Trichlorobenzene 13.99 180 27408 2.020 ug/l 100 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed