Quantitation Report (LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_U\DATA\VU052118\ Data File : VU023965.D Acq On : 21 May 2018 11:45 Operator : MD/SY Sample : VU0521MBL01 Misc : 5.00g/5.0mL/100uL/5.0mL/MSVOA_U/MEOH ALS Vial : 4 Sample Multiplier: 1 Quant Time: May 22 01:15:52 2018 Quant Method : W:\HPCHEM1\MSVOA_U\METHOD\SOMULM051218WMA.M Quant Title : VOC Analysis QLast Update : Tue May 22 01:05:00 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) 1,4-Difluorobenzene 5.89 114 292268 50.00 ug/L 0.00 28) Chlorobenzene-d5 9.09 117 290945 50.00 ug/L 0.00 60) 1,4-Dichlorobenzene-d4 11.49 152 136122 50.00 ug/L 0.00 System Monitoring Compounds 4) Vinyl Chloride-d3 1.40 65 97898 36.05 ug/L 0.00 Spiked Amount 50.000 Range 60 - 135 Recovery = 72.10% 7) Chloroethane-d5 1.68 69 87253 40.77 ug/L 0.00 Spiked Amount 50.000 Range 70 - 130 Recovery = 81.54% 11) 1,1-Dichloroethene-d2 2.27 63 149831 30.07 ug/L 0.00 Spiked Amount 50.000 Range 60 - 125 Recovery = 60.14% 21) 2-Butanone-d5 4.18 46 198753 105.16 ug/L 0.00 Spiked Amount 100.000 Range 40 - 130 Recovery = 105.16% 24) Chloroform-d 4.65 84 195772 47.23 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 94.46% 26) 1,2-Dichloroethane-d4 5.31 65 137621 50.46 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 100.92% 32) Benzene-d6 5.35 84 384029 45.22 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 90.44% 36) 1,2-Dichloropropane-d6 6.34 67 141224 49.23 ug/L 0.00 Spiked Amount 50.000 Range 70 - 120 Recovery = 98.46% 41) Toluene-d8 7.57 98 346413 44.27 ug/L 0.00 Spiked Amount 50.000 Range 80 - 120 Recovery = 88.54% 43) trans-1,3-Dichloropropene- 7.85 79 57480 47.64 ug/L 0.00 Spiked Amount 50.000 Range 60 - 125 Recovery = 95.28% 47) 2-Hexanone-d5 8.31 63 128167 96.93 ug/L 0.00 Spiked Amount 100.000 Range 45 - 130 Recovery = 96.93% 57) 1,1,2,2-Tetrachloroethane- 10.44 84 193243 47.83 ug/L 0.00 Spiked Amount 50.000 Range 65 - 120 Recovery = 95.66% 64) 1,2-Dichlorobenzene-d4 11.87 152 142677 48.53 ug/L 0.00 Spiked Amount 50.000 Range 80 - 120 Recovery = 97.06% Target Compounds Qvalue -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed