LSC Area Percent Report Data Path : W:\HPCHEM1\MSVOA_U\DATA\VU052118\ Data File : VU023965.D Acq On : 21 May 2018 11:45 Operator : MD/SY Sample : VU0521MBL01 Misc : 5.00g/5.0mL/100uL/5.0mL/MSVOA_U/MEOH ALS Vial : 4 Sample Multiplier: 1 Integration Parameters: LSCINT.P Integrator: RTE Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 0 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Method : W:\HPCHEM1\MSVOA_U\METHOD\SOMULM051218WMA.M Title : VOC Analysis Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total --- ----- ----- ---- ---- --- ------- ------- ------ ------- 1 0.609 3 6 11 rBV 188 183 0.01% 0.002% 2 0.667 19 24 29 rVB 179 202 0.01% 0.002% 3 0.693 29 32 35 rBV2 175 107 0.01% 0.001% 4 0.748 46 49 52 rVV2 166 133 0.01% 0.001% 5 0.799 57 65 70 rBV2 193 323 0.02% 0.003% 6 0.870 83 87 89 rBV 266 186 0.01% 0.002% 7 0.892 89 94 98 rBV2 211 259 0.02% 0.002% 8 0.915 98 101 103 rBV 168 98 0.01% 0.001% 9 0.982 119 122 125 rBV2 150 106 0.01% 0.001% 10 1.088 136 155 180 rBV 1364475 1549490 100.00% 14.336% 11 1.182 181 184 192 rVB 5531 5450 0.35% 0.050% 12 1.400 245 252 265 rBV 151329 159161 10.27% 1.473% 13 1.680 331 339 355 rVB 127438 159286 10.28% 1.474% 14 2.272 512 523 536 rBV 258945 390485 25.20% 3.613% 15 2.397 558 562 565 rBV2 275 249 0.02% 0.002% 16 2.474 581 586 590 rBV3 454 479 0.03% 0.004% 17 2.532 602 604 607 rBV 158 81 0.01% 0.001% 18 2.580 617 619 621 rBV 125 84 0.01% 0.001% 19 2.609 625 628 629 rBV 199 115 0.01% 0.001% 20 2.674 645 648 649 rBV 131 79 0.01% 0.001% 21 2.703 649 657 665 rVB3 1530 2287 0.15% 0.021% 22 2.841 690 700 711 rBV2 1667 3473 0.22% 0.032% 23 2.979 741 743 749 rVB3 372 256 0.02% 0.002% 24 3.072 770 772 777 rVB2 194 180 0.01% 0.002% 25 3.098 778 780 782 rBV2 189 115 0.01% 0.001% 26 3.130 789 790 795 rBV2 109 106 0.01% 0.001% 27 3.185 800 807 811 rVV2 305 341 0.02% 0.003% 28 3.227 818 820 823 rBV 139 90 0.01% 0.001% 29 3.275 830 835 838 rBV 178 230 0.01% 0.002% 30 3.349 854 858 860 rBV 110 116 0.01% 0.001% 31 3.368 862 864 866 rBV 167 122 0.01% 0.001% 32 3.445 886 888 892 rVB 203 91 0.01% 0.001% 33 3.474 892 897 900 rBV2 236 202 0.01% 0.002% 34 3.503 904 906 911 rVB 228 144 0.01% 0.001% 35 3.539 911 917 919 rBV2 212 238 0.02% 0.002% 36 3.641 947 949 954 rVV2 165 170 0.01% 0.002% 37 3.706 965 969 970 rBV 236 148 0.01% 0.001% 38 3.741 976 980 984 rBV 154 152 0.01% 0.001% 39 3.821 999 1005 1008 rVB2 191 249 0.02% 0.002% 40 3.850 1008 1014 1018 rBV2 240 215 0.01% 0.002% 41 3.873 1018 1021 1023 rBV2 201 157 0.01% 0.001% 42 3.928 1036 1038 1041 rVB 159 91 0.01% 0.001% 43 3.947 1041 1044 1048 rBV2 202 180 0.01% 0.002% 44 3.966 1048 1050 1054 rBV 171 118 0.01% 0.001% 45 4.053 1068 1077 1079 rBV 259 400 0.03% 0.004% 46 4.072 1079 1083 1089 rBV2 625 731 0.05% 0.007% 47 4.178 1102 1116 1150 rBV 121404 324350 20.93% 3.001% 48 4.651 1246 1263 1286 rBV 198636 470611 30.37% 4.354% 49 4.860 1325 1328 1329 rBV 254 148 0.01% 0.001% 50 4.886 1331 1336 1338 rBV3 449 500 0.03% 0.005% 51 4.928 1346 1349 1352 rBV 149 104 0.01% 0.001% 52 4.976 1361 1364 1367 rBV 310 162 0.01% 0.001% 53 4.995 1367 1370 1373 rBV2 315 256 0.02% 0.002% 54 5.098 1397 1402 1404 rBV 208 177 0.01% 0.002% 55 5.130 1408 1412 1414 rBV2 137 96 0.01% 0.001% 56 5.149 1414 1418 1419 rBV2 133 89 0.01% 0.001% 57 5.243 1441 1447 1449 rBV2 222 269 0.02% 0.002% 58 5.342 1454 1478 1524 rBV2 389567 1196097 77.19% 11.066% 59 5.667 1576 1579 1580 rBV 310 174 0.01% 0.002% 60 5.889 1633 1648 1692 rBV 339806 707663 45.67% 6.547% 61 6.188 1733 1741 1749 rVB6 1947 3704 0.24% 0.034% 62 6.217 1749 1750 1754 rVV2 226 121 0.01% 0.001% 63 6.236 1754 1756 1758 rVB2 335 148 0.01% 0.001% 64 6.336 1771 1787 1817 rBV 283086 573197 36.99% 5.303% 65 6.603 1867 1870 1873 rBV 150 92 0.01% 0.001% 66 6.616 1873 1874 1881 rBV2 143 128 0.01% 0.001% 67 6.670 1888 1891 1894 rVB2 241 138 0.01% 0.001% 68 6.690 1894 1897 1899 rBV 206 133 0.01% 0.001% 69 6.725 1905 1908 1910 rBV2 202 116 0.01% 0.001% 70 6.741 1910 1913 1915 rBV2 148 92 0.01% 0.001% 71 6.776 1921 1924 1927 rBV2 110 82 0.01% 0.001% 72 6.863 1947 1951 1963 rVB3 970 1599 0.10% 0.015% 73 6.921 1963 1969 1970 rBV 214 200 0.01% 0.002% 74 6.931 1970 1972 1975 rVB2 198 107 0.01% 0.001% 75 6.963 1975 1982 1983 rBV 249 292 0.02% 0.003% 76 6.985 1988 1989 1994 rVB 126 107 0.01% 0.001% 77 7.066 2010 2014 2018 rBV2 211 221 0.01% 0.002% 78 7.120 2028 2031 2035 rBV 150 145 0.01% 0.001% 79 7.233 2053 2066 2087 rBV 141381 258381 16.68% 2.391% 80 7.345 2099 2101 2104 rVB2 269 88 0.01% 0.001% 81 7.468 2133 2139 2140 rBV2 339 272 0.02% 0.003% 82 7.571 2157 2171 2204 rBV 498154 922799 59.56% 8.538% 83 7.853 2247 2259 2276 rBV 101331 173163 11.18% 1.602% 84 8.040 2314 2317 2319 rBV 194 105 0.01% 0.001% 85 8.130 2343 2345 2349 rBV2 132 85 0.01% 0.001% 86 8.175 2354 2359 2361 rBV2 254 226 0.01% 0.002% 87 8.313 2390 2402 2432 rBV 382541 668734 43.16% 6.187% 88 8.635 2495 2502 2506 rBV4 530 709 0.05% 0.007% 89 8.844 2563 2567 2570 rBV2 223 186 0.01% 0.002% 90 9.095 2631 2645 2680 rBV 511245 882478 56.95% 8.165% 91 9.779 2855 2858 2861 rBV2 280 229 0.01% 0.002% 92 10.320 3021 3026 3031 rVB4 998 1176 0.08% 0.011% 93 10.435 3049 3062 3085 rBV 389803 625194 40.35% 5.784% 94 10.541 3092 3095 3099 rBV 214 197 0.01% 0.002% 95 10.783 3166 3170 3173 rBV2 275 244 0.02% 0.002% 96 11.422 3366 3369 3371 rBV2 317 224 0.01% 0.002% 97 11.487 3377 3389 3414 rBV 522244 836815 54.01% 7.742% 98 11.866 3493 3507 3529 rBV 534701 877669 56.64% 8.120% 99 12.483 3695 3699 3706 rVB2 577 725 0.05% 0.007% 100 13.516 4017 4020 4021 rBV3 477 314 0.02% 0.003% Sum of corrected areas: 10808489