Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_U\DATA\VU052118\ Data File : VU023972.D Acq On : 21 May 2018 16:23 Operator : MD/SY Sample : J2952-19ME Misc : 5.87g/5.0mL/100uL/5.0mL/MSVOA_U/MEOH ALS Vial : 11 Sample Multiplier: 1 Quant Time: May 22 14:50:15 2018 Quant Method : W:\HPCHEM1\MSVOA_U\METHOD\SOMULM051218WMA.M Quant Title : VOC Analysis QLast Update : Tue May 22 01:05:00 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) 1,4-Difluorobenzene 5.89 114 297497 50.00 ug/L 0.00 28) Chlorobenzene-d5 9.10 117 319963 50.00 ug/L 0.00 60) 1,4-Dichlorobenzene-d4 11.49 152 153942 50.00 ug/L 0.00 System Monitoring Compounds 4) Vinyl Chloride-d3 1.39 65 76068 27.52 ug/L 0.00 Spiked Amount 50.000 Range 60 - 135 Recovery = 55.04%# 7) Chloroethane-d5 1.64 69 49660 22.80 ug/L -0.04 Spiked Amount 50.000 Range 70 - 130 Recovery = 45.60%# 11) 1,1-Dichloroethene-d2 2.23 63 124046m 24.46 ug/L -0.05 Spiked Amount 50.000 Range 60 - 125 Recovery = 48.92%# 21) 2-Butanone-d5 4.20 46 188496 97.98 ug/L 0.02 Spiked Amount 100.000 Range 40 - 130 Recovery = 97.98% 24) Chloroform-d 4.65 84 160215 37.97 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 75.94% 26) 1,2-Dichloroethane-d4 5.31 65 119236 42.95 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 85.90% 32) Benzene-d6 5.34 84 323616 34.65 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 69.30%# 36) 1,2-Dichloropropane-d6 6.33 67 118389 37.53 ug/L 0.00 Spiked Amount 50.000 Range 70 - 120 Recovery = 75.06% 41) Toluene-d8 7.57 98 290267 33.73 ug/L 0.00 Spiked Amount 50.000 Range 80 - 120 Recovery = 67.46%# 43) trans-1,3-Dichloropropene- 7.85 79 46735 35.22 ug/L 0.00 Spiked Amount 50.000 Range 60 - 125 Recovery = 70.44% 47) 2-Hexanone-d5 8.33 63 141515 97.32 ug/L 0.01 Spiked Amount 100.000 Range 45 - 130 Recovery = 97.32% 57) 1,1,2,2-Tetrachloroethane- 10.44 84 195042 43.90 ug/L 0.00 Spiked Amount 50.000 Range 65 - 120 Recovery = 87.80% 64) 1,2-Dichlorobenzene-d4 11.87 152 133451 40.14 ug/L 0.00 Spiked Amount 50.000 Range 80 - 120 Recovery = 80.28% Target Compounds Qvalue 46) Tetrachloroethene 8.23 164 105152 47.90 ug/L 96 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed