LSC Area Percent Report Data Path : W:\HPCHEM1\MSVOA_U\DATA\VU052118\ Data File : VU023972.D Acq On : 21 May 2018 16:23 Operator : MD/SY Sample : J2952-19ME Misc : 5.87g/5.0mL/100uL/5.0mL/MSVOA_U/MEOH ALS Vial : 11 Sample Multiplier: 1 Integration Parameters: LSCINT.P Integrator: RTE Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 0 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Method : W:\HPCHEM1\MSVOA_U\METHOD\SOMULM051218WMA.M Title : VOC Analysis Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total --- ----- ----- ---- ---- --- ------- ------- ------ ------- 1 0.629 8 12 17 rVB2 169 195 0.02% 0.002% 2 0.677 23 27 32 rBV2 115 134 0.01% 0.001% 3 0.706 32 36 39 rVB2 196 119 0.01% 0.001% 4 0.863 81 85 86 rBV 162 118 0.01% 0.001% 5 0.989 117 124 127 rBV2 183 227 0.02% 0.002% 6 1.082 132 153 173 rBV 1018374 1173868 100.00% 10.897% 7 1.175 179 182 192 rVB2 5454 5246 0.45% 0.049% 8 1.268 207 211 222 rVB3 5891 9025 0.77% 0.084% 9 1.394 243 250 271 rVB 93761 125875 10.72% 1.169% 10 1.641 322 327 341 rVB 69589 80214 6.83% 0.745% 11 2.227 498 509 526 rBV 204723 316046 26.92% 2.934% 12 2.432 569 573 581 rVB2 880 1027 0.09% 0.010% 13 2.497 591 593 597 rVB3 236 164 0.01% 0.002% 14 2.542 605 607 610 rBV 272 178 0.02% 0.002% 15 2.574 615 617 625 rVB2 466 453 0.04% 0.004% 16 2.683 641 651 667 rVB2 5625 10510 0.90% 0.098% 17 2.831 684 697 708 rBV3 4313 9289 0.79% 0.086% 18 2.931 725 728 734 rVB 375 325 0.03% 0.003% 19 3.185 804 807 810 rBV2 162 124 0.01% 0.001% 20 3.265 824 832 840 rVB6 913 1609 0.14% 0.015% 21 3.474 894 897 901 rBV2 144 110 0.01% 0.001% 22 3.548 916 920 921 rBV 215 143 0.01% 0.001% 23 3.580 926 930 933 rBV 204 168 0.01% 0.002% 24 3.625 942 944 948 rBV 176 164 0.01% 0.002% 25 3.657 948 954 960 rVV2 146 271 0.02% 0.003% 26 3.735 975 978 983 rBV 231 246 0.02% 0.002% 27 3.905 1028 1031 1035 rVV2 156 153 0.01% 0.001% 28 3.927 1035 1038 1042 rVB2 141 117 0.01% 0.001% 29 3.966 1047 1050 1052 rBV 182 117 0.01% 0.001% 30 4.005 1059 1062 1065 rVV2 136 117 0.01% 0.001% 31 4.024 1065 1068 1072 rVV 221 188 0.02% 0.002% 32 4.120 1094 1098 1101 rVB2 269 213 0.02% 0.002% 33 4.140 1101 1104 1106 rBV2 248 205 0.02% 0.002% 34 4.204 1106 1124 1169 rVV 91005 306179 26.08% 2.842% 35 4.519 1218 1222 1225 rBV 264 217 0.02% 0.002% 36 4.648 1243 1262 1289 rBV 158176 406006 34.59% 3.769% 37 4.770 1296 1300 1306 rBV3 327 382 0.03% 0.004% 38 4.863 1325 1329 1330 rBV2 312 220 0.02% 0.002% 39 4.889 1330 1337 1346 rVB5 718 1368 0.12% 0.013% 40 4.972 1360 1363 1364 rBV2 715 325 0.03% 0.003% 41 5.024 1376 1379 1385 rVB2 302 278 0.02% 0.003% 42 5.062 1385 1391 1394 rBV2 172 241 0.02% 0.002% 43 5.185 1424 1429 1432 rBV2 181 156 0.01% 0.001% 44 5.333 1451 1475 1499 rBV2 349414 1001350 85.30% 9.296% 45 5.619 1555 1564 1572 rBV7 2495 4878 0.42% 0.045% 46 5.670 1578 1580 1584 rVV2 218 109 0.01% 0.001% 47 5.744 1600 1603 1604 rBV 250 119 0.01% 0.001% 48 5.799 1616 1620 1623 rBV 177 146 0.01% 0.001% 49 5.821 1623 1627 1632 rVB2 156 140 0.01% 0.001% 50 5.886 1632 1647 1681 rBV 339534 727177 61.95% 6.750% 51 6.178 1729 1738 1751 rBV8 2623 5198 0.44% 0.048% 52 6.252 1752 1761 1772 rBV6 2722 5252 0.45% 0.049% 53 6.332 1772 1786 1806 rBV 226990 479402 40.84% 4.450% 54 6.532 1846 1848 1852 rVB 253 196 0.02% 0.002% 55 6.561 1852 1857 1861 rBV2 240 290 0.02% 0.003% 56 6.586 1861 1865 1869 rVB2 120 115 0.01% 0.001% 57 6.641 1880 1882 1885 rBV 222 149 0.01% 0.001% 58 6.731 1907 1910 1912 rBV2 144 106 0.01% 0.001% 59 6.866 1946 1952 1957 rBV4 977 1279 0.11% 0.012% 60 6.895 1957 1961 1962 rBV4 607 468 0.04% 0.004% 61 6.921 1967 1969 1974 rVB2 387 220 0.02% 0.002% 62 6.947 1974 1977 1982 rVB 140 114 0.01% 0.001% 63 7.008 1994 1996 2000 rBV2 189 151 0.01% 0.001% 64 7.111 2025 2028 2031 rBV 174 127 0.01% 0.001% 65 7.230 2053 2065 2092 rBV 112696 219306 18.68% 2.036% 66 7.387 2110 2114 2115 rBV 421 290 0.02% 0.003% 67 7.480 2139 2143 2145 rBV2 311 252 0.02% 0.002% 68 7.567 2157 2170 2198 rBV 414582 771216 65.70% 7.159% 69 7.857 2248 2260 2282 rBV 76089 147178 12.54% 1.366% 70 8.184 2353 2362 2363 rBV2 1103 1343 0.11% 0.012% 71 8.230 2363 2376 2393 rVV 453210 796587 67.86% 7.395% 72 8.326 2395 2406 2434 rVB 389768 734205 62.55% 6.816% 73 8.631 2498 2501 2502 rBV2 300 183 0.02% 0.002% 74 8.760 2537 2541 2543 rBV2 191 146 0.01% 0.001% 75 8.969 2603 2606 2611 rBV 155 124 0.01% 0.001% 76 9.020 2618 2622 2624 rBV 304 223 0.02% 0.002% 77 9.098 2632 2646 2675 rBV 541197 976301 83.17% 9.063% 78 9.252 2692 2694 2695 rBV 254 108 0.01% 0.001% 79 9.384 2729 2735 2741 rBV2 551 806 0.07% 0.007% 80 9.606 2802 2804 2806 rBV2 166 106 0.01% 0.001% 81 9.673 2823 2825 2829 rBV2 180 150 0.01% 0.001% 82 9.831 2869 2874 2877 rBV2 340 388 0.03% 0.004% 83 9.869 2883 2886 2887 rBV 190 126 0.01% 0.001% 84 9.982 2918 2921 2925 rBV2 267 290 0.02% 0.003% 85 10.056 2942 2944 2947 rBV2 161 130 0.01% 0.001% 86 10.319 3022 3026 3034 rVB3 1102 1577 0.13% 0.015% 87 10.438 3050 3063 3083 rBV 393650 638224 54.37% 5.925% 88 10.609 3109 3116 3127 rVB4 2408 3653 0.31% 0.034% 89 10.660 3127 3132 3138 rBV2 312 373 0.03% 0.003% 90 10.696 3138 3143 3145 rBV 322 314 0.03% 0.003% 91 10.821 3178 3182 3185 rVB2 444 354 0.03% 0.003% 92 11.098 3262 3268 3270 rBV2 263 254 0.02% 0.002% 93 11.426 3367 3370 3371 rBV 299 158 0.01% 0.001% 94 11.490 3377 3390 3411 rBV 607254 958617 81.66% 8.899% 95 11.782 3478 3481 3486 rVB2 347 217 0.02% 0.002% 96 11.866 3494 3507 3526 rBV 519989 830608 70.76% 7.711% 97 12.053 3560 3565 3566 rBV3 392 342 0.03% 0.003% 98 12.191 3605 3608 3613 rBV2 487 561 0.05% 0.005% 99 12.483 3692 3699 3709 rVB 2824 4519 0.38% 0.042% 100 14.284 4252 4259 4268 rVB2 2600 3719 0.32% 0.035% Sum of corrected areas: 10772264