LSC Area Percent Report Data Path : W:\HPCHEM1\MSVOA_U\DATA\VU052118\ Data File : VU023974.D Acq On : 21 May 2018 17:14 Operator : MD/SY Sample : J3032-04 Misc : 5.0mL/MSVOA_U/WATER ALS Vial : 13 Sample Multiplier: 1 Integration Parameters: LSCINT.P Integrator: RTE Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 0 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Method : W:\HPCHEM1\MSVOA_U\METHOD\SOMULM051218WMA.M Title : VOC Analysis Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total --- ----- ----- ---- ---- --- ------- ------- ------ ------- 1 0.619 7 9 10 rBV 136 73 0.01% 0.001% 2 0.632 10 13 16 rVV 213 171 0.02% 0.002% 3 0.651 16 19 23 rVV2 209 176 0.02% 0.002% 4 0.863 77 85 88 rBV 148 183 0.02% 0.002% 5 0.944 106 110 116 rVB2 144 154 0.01% 0.002% 6 1.088 136 155 176 rBV 851065 1005533 89.21% 10.180% 7 1.182 180 184 198 rVB3 8193 11009 0.98% 0.111% 8 1.397 244 251 262 rBV 141016 146762 13.02% 1.486% 9 1.680 331 339 356 rVB 117319 150498 13.35% 1.524% 10 2.268 511 522 534 rBV 241144 362836 32.19% 3.674% 11 2.374 549 555 564 rVB3 2785 4681 0.42% 0.047% 12 2.461 569 582 584 rBV3 1436 2488 0.22% 0.025% 13 2.609 625 628 631 rBV 340 308 0.03% 0.003% 14 2.699 652 656 665 rBV4 839 1258 0.11% 0.013% 15 2.783 679 682 685 rBV 142 99 0.01% 0.001% 16 2.844 691 701 708 rVB4 792 1539 0.14% 0.016% 17 3.191 805 809 814 rBV3 280 239 0.02% 0.002% 18 3.288 833 839 842 rBV2 170 193 0.02% 0.002% 19 3.400 868 874 880 rBV3 382 427 0.04% 0.004% 20 3.744 976 981 985 rBV2 133 121 0.01% 0.001% 21 3.780 989 992 1001 rBV2 153 207 0.02% 0.002% 22 3.828 1004 1007 1008 rBV 136 77 0.01% 0.001% 23 3.950 1042 1045 1050 rBV2 146 116 0.01% 0.001% 24 4.001 1054 1061 1067 rVV3 549 778 0.07% 0.008% 25 4.101 1086 1092 1096 rBV2 324 419 0.04% 0.004% 26 4.181 1102 1117 1150 rBV2 121327 319644 28.36% 3.236% 27 4.481 1208 1210 1213 rVB 230 97 0.01% 0.001% 28 4.497 1213 1215 1217 rBV3 179 104 0.01% 0.001% 29 4.651 1245 1263 1293 rBV 190977 443695 39.36% 4.492% 30 4.792 1305 1307 1318 rVB2 557 834 0.07% 0.008% 31 4.841 1319 1322 1324 rBV2 290 207 0.02% 0.002% 32 4.892 1329 1338 1348 rVV2 924 1830 0.16% 0.019% 33 4.960 1357 1359 1361 rBV 146 88 0.01% 0.001% 34 4.985 1361 1367 1369 rBV2 424 448 0.04% 0.005% 35 5.088 1396 1399 1404 rVB2 213 162 0.01% 0.002% 36 5.120 1407 1409 1411 rBV 235 162 0.01% 0.002% 37 5.236 1444 1445 1448 rVB 144 73 0.01% 0.001% 38 5.255 1448 1451 1453 rBV2 234 182 0.02% 0.002% 39 5.345 1453 1479 1511 rBV2 363402 1127177 100.00% 11.412% 40 5.590 1551 1555 1556 rBV 174 142 0.01% 0.001% 41 5.625 1563 1566 1568 rVB3 153 80 0.01% 0.001% 42 5.680 1580 1583 1588 rVB2 368 343 0.03% 0.003% 43 5.712 1588 1593 1596 rBV2 300 347 0.03% 0.004% 44 5.731 1596 1599 1603 rVB2 289 261 0.02% 0.003% 45 5.757 1603 1607 1609 rBV 255 155 0.01% 0.002% 46 5.770 1609 1611 1615 rVB2 203 142 0.01% 0.001% 47 5.792 1615 1618 1620 rBV3 289 235 0.02% 0.002% 48 5.892 1634 1649 1683 rBV 335633 687513 60.99% 6.961% 49 6.146 1726 1728 1731 rVB2 272 147 0.01% 0.001% 50 6.175 1733 1737 1739 rBV2 723 579 0.05% 0.006% 51 6.188 1739 1741 1748 rVB4 1349 1281 0.11% 0.013% 52 6.223 1749 1752 1753 rVB4 178 77 0.01% 0.001% 53 6.233 1753 1755 1757 rVB2 237 107 0.01% 0.001% 54 6.249 1757 1760 1762 rBV 294 131 0.01% 0.001% 55 6.275 1766 1768 1772 rVB2 188 125 0.01% 0.001% 56 6.336 1772 1787 1817 rBV 261307 533194 47.30% 5.398% 57 6.497 1835 1837 1840 rBV2 232 109 0.01% 0.001% 58 6.545 1849 1852 1854 rVV2 312 219 0.02% 0.002% 59 6.603 1867 1870 1872 rVB3 220 116 0.01% 0.001% 60 6.648 1881 1884 1887 rBV 171 116 0.01% 0.001% 61 6.863 1945 1951 1958 rBV4 832 1112 0.10% 0.011% 62 7.233 2053 2066 2090 rBV 126619 231274 20.52% 2.342% 63 7.429 2125 2127 2129 rVV 189 72 0.01% 0.001% 64 7.570 2157 2171 2191 rBV 469463 833814 73.97% 8.442% 65 7.853 2248 2259 2282 rBV 87964 154020 13.66% 1.559% 66 7.998 2302 2304 2310 rVB3 507 375 0.03% 0.004% 67 8.027 2310 2313 2314 rBV3 128 82 0.01% 0.001% 68 8.117 2338 2341 2345 rBV 352 267 0.02% 0.003% 69 8.181 2352 2361 2373 rBV 1418 2417 0.21% 0.024% 70 8.236 2373 2378 2384 rVB4 548 509 0.05% 0.005% 71 8.313 2390 2402 2443 rBV 389421 696719 61.81% 7.054% 72 8.471 2445 2451 2464 rVB3 8759 15466 1.37% 0.157% 73 8.982 2607 2610 2615 rBV2 240 219 0.02% 0.002% 74 9.046 2627 2630 2632 rBV2 254 197 0.02% 0.002% 75 9.094 2632 2645 2684 rVV 507899 865651 76.80% 8.764% 76 9.255 2690 2695 2710 rVB2 2618 3879 0.34% 0.039% 77 9.384 2729 2735 2736 rBV2 1289 1120 0.10% 0.011% 78 9.657 2818 2820 2822 rBV2 129 81 0.01% 0.001% 79 9.750 2845 2849 2852 rBV 241 217 0.02% 0.002% 80 9.786 2852 2860 2877 rVB2 5393 9026 0.80% 0.091% 81 9.866 2883 2885 2889 rBV 243 218 0.02% 0.002% 82 10.175 2973 2981 2987 rBV4 819 1249 0.11% 0.013% 83 10.229 2996 2998 3000 rBV2 167 99 0.01% 0.001% 84 10.271 3008 3011 3013 rBV 332 199 0.02% 0.002% 85 10.320 3021 3026 3032 rVB4 765 971 0.09% 0.010% 86 10.435 3050 3062 3082 rBV 379360 618711 54.89% 6.264% 87 10.612 3110 3117 3133 rVB2 1736 3073 0.27% 0.031% 88 10.712 3144 3148 3151 rBV2 245 230 0.02% 0.002% 89 10.979 3226 3231 3239 rVB3 1602 1967 0.17% 0.020% 90 11.159 3280 3287 3298 rVB4 1412 1940 0.17% 0.020% 91 11.426 3367 3370 3372 rBV2 450 304 0.03% 0.003% 92 11.490 3377 3390 3410 rBV 486616 783050 69.47% 7.928% 93 11.635 3432 3435 3437 rBV2 418 321 0.03% 0.003% 94 11.770 3469 3477 3489 rVB2 8114 12752 1.13% 0.129% 95 11.866 3494 3507 3527 rBV 509540 814127 72.23% 8.243% 96 11.988 3538 3545 3556 rVB2 5280 7756 0.69% 0.079% 97 12.056 3564 3566 3570 rBV2 244 134 0.01% 0.001% 98 12.972 3847 3851 3857 rBV2 790 901 0.08% 0.009% 99 13.191 3918 3919 3920 rBV2 395 142 0.01% 0.001% 100 13.307 3949 3955 3966 rVB4 1231 1945 0.17% 0.020% Sum of corrected areas: 9877073