Quantitation Report (LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_U\DATA\VU052318\ Data File : VU024030.D Acq On : 23 May 2018 10:51 Operator : MD/SY Sample : VU0523MBL01 Misc : 5.00g/5.0mL/100uL/5.0mL/MSVOA_U/MEOH ALS Vial : 3 Sample Multiplier: 1 Quant Time: May 24 04:20:12 2018 Quant Method : W:\HPCHEM1\MSVOA_U\METHOD\SOMULM051218WMA.M Quant Title : VOC Analysis QLast Update : Thu May 24 04:14:38 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) 1,4-Difluorobenzene 5.89 114 285726 50.00 ug/L 0.00 28) Chlorobenzene-d5 9.09 117 289848 50.00 ug/L 0.00 60) 1,4-Dichlorobenzene-d4 11.49 152 130693 50.00 ug/L 0.00 System Monitoring Compounds 4) Vinyl Chloride-d3 1.40 65 87973 33.13 ug/L 0.00 Spiked Amount 50.000 Range 60 - 135 Recovery = 66.26% 7) Chloroethane-d5 1.68 69 75982 36.32 ug/L 0.00 Spiked Amount 50.000 Range 70 - 130 Recovery = 72.64% 11) 1,1-Dichloroethene-d2 2.27 63 134822 27.68 ug/L 0.00 Spiked Amount 50.000 Range 60 - 125 Recovery = 55.36%# 21) 2-Butanone-d5 4.18 46 181202 98.07 ug/L 0.00 Spiked Amount 100.000 Range 40 - 130 Recovery = 98.07% 24) Chloroform-d 4.65 84 180895 44.64 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 89.28% 26) 1,2-Dichloroethane-d4 5.31 65 125295 46.99 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 93.98% 32) Benzene-d6 5.35 84 353375 41.77 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 83.54% 36) 1,2-Dichloropropane-d6 6.33 67 127041 44.45 ug/L 0.00 Spiked Amount 50.000 Range 70 - 120 Recovery = 88.90% 41) Toluene-d8 7.57 98 314994 40.41 ug/L 0.00 Spiked Amount 50.000 Range 80 - 120 Recovery = 80.82% 43) trans-1,3-Dichloropropene- 7.85 79 52423 43.61 ug/L 0.00 Spiked Amount 50.000 Range 60 - 125 Recovery = 87.22% 47) 2-Hexanone-d5 8.31 63 127794 97.01 ug/L 0.00 Spiked Amount 100.000 Range 45 - 130 Recovery = 97.01% 57) 1,1,2,2-Tetrachloroethane- 10.44 84 183992 45.72 ug/L 0.00 Spiked Amount 50.000 Range 65 - 120 Recovery = 91.44% 64) 1,2-Dichlorobenzene-d4 11.87 152 135426 47.98 ug/L 0.00 Spiked Amount 50.000 Range 80 - 120 Recovery = 95.96% Target Compounds Qvalue -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed