LSC Area Percent Report Data Path : W:\HPCHEM1\MSVOA_U\DATA\VU052318\ Data File : VU024030.D Acq On : 23 May 2018 10:51 Operator : MD/SY Sample : VU0523MBL01 Misc : 5.00g/5.0mL/100uL/5.0mL/MSVOA_U/MEOH ALS Vial : 3 Sample Multiplier: 1 Integration Parameters: LSCINT.P Integrator: RTE Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 0 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Method : W:\HPCHEM1\MSVOA_U\METHOD\SOMULM051218WMA.M Title : VOC Analysis Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total --- ----- ----- ---- ---- --- ------- ------- ------ ------- 1 0.773 54 57 59 rBV2 220 156 0.01% 0.002% 2 0.873 85 88 92 rVB 201 145 0.01% 0.001% 3 0.896 92 95 98 rBV 144 135 0.01% 0.001% 4 0.912 98 100 104 rVB 203 156 0.01% 0.002% 5 0.934 104 107 109 rBV2 169 124 0.01% 0.001% 6 0.998 122 127 131 rVB2 254 293 0.02% 0.003% 7 1.024 131 135 137 rBV 174 174 0.01% 0.002% 8 1.089 137 155 177 rBV 1413924 1639181 100.00% 15.798% 9 1.397 245 251 263 rBV 135923 139194 8.49% 1.342% 10 1.680 331 339 352 rBV 108321 137937 8.41% 1.329% 11 2.272 512 523 536 rBV 233422 348855 21.28% 3.362% 12 2.436 571 574 579 rBV2 463 432 0.03% 0.004% 13 2.478 580 587 598 rVB2 1623 2601 0.16% 0.025% 14 2.616 627 630 636 rVV2 333 386 0.02% 0.004% 15 2.696 650 655 667 rVB3 1083 2005 0.12% 0.019% 16 2.777 677 680 684 rBV2 173 139 0.01% 0.001% 17 2.822 691 694 695 rBV 475 224 0.01% 0.002% 18 2.889 713 715 718 rVB 198 111 0.01% 0.001% 19 2.989 739 746 752 rVB4 837 1213 0.07% 0.012% 20 3.066 767 770 774 rVB2 239 169 0.01% 0.002% 21 3.146 792 795 800 rBV 203 191 0.01% 0.002% 22 3.378 861 867 873 rBV3 256 352 0.02% 0.003% 23 3.432 879 884 888 rBV2 273 261 0.02% 0.003% 24 3.452 888 890 894 rVV2 214 163 0.01% 0.002% 25 3.548 916 920 924 rBV2 317 367 0.02% 0.004% 26 3.603 933 937 939 rBV2 190 147 0.01% 0.001% 27 3.690 961 964 967 rVB2 166 123 0.01% 0.001% 28 3.786 987 994 998 rVV2 144 158 0.01% 0.002% 29 3.850 1007 1014 1017 rBV2 319 386 0.02% 0.004% 30 3.944 1040 1043 1046 rBV2 152 110 0.01% 0.001% 31 4.031 1066 1070 1071 rBV 132 110 0.01% 0.001% 32 4.076 1079 1084 1088 rBV2 267 315 0.02% 0.003% 33 4.178 1101 1116 1148 rBV 111708 296561 18.09% 2.858% 34 4.375 1175 1177 1180 rVB 610 346 0.02% 0.003% 35 4.397 1182 1184 1186 rBV2 324 212 0.01% 0.002% 36 4.516 1219 1221 1225 rVB 257 179 0.01% 0.002% 37 4.555 1230 1233 1238 rVB3 374 305 0.02% 0.003% 38 4.651 1243 1263 1296 rBV 184565 443513 27.06% 4.275% 39 4.821 1313 1316 1317 rBV2 177 124 0.01% 0.001% 40 4.892 1330 1338 1346 rVB4 902 1655 0.10% 0.016% 41 4.931 1347 1350 1358 rVB 242 262 0.02% 0.003% 42 4.989 1360 1368 1372 rBV3 485 655 0.04% 0.006% 43 5.011 1372 1375 1379 rVB3 223 168 0.01% 0.002% 44 5.059 1387 1390 1394 rBV 164 169 0.01% 0.002% 45 5.220 1438 1440 1444 rVB 197 143 0.01% 0.001% 46 5.243 1444 1447 1454 rVB2 302 393 0.02% 0.004% 47 5.342 1454 1478 1500 rBV2 357779 1080268 65.90% 10.412% 48 5.648 1568 1573 1577 rVV3 249 219 0.01% 0.002% 49 5.674 1577 1581 1584 rVB2 220 147 0.01% 0.001% 50 5.809 1619 1623 1625 rBV2 148 118 0.01% 0.001% 51 5.825 1625 1628 1632 rVB2 149 123 0.01% 0.001% 52 5.889 1632 1648 1691 rBV 343563 703861 42.94% 6.784% 53 6.185 1732 1740 1751 rVB6 1999 3840 0.23% 0.037% 54 6.284 1766 1771 1772 rBV2 166 176 0.01% 0.002% 55 6.336 1772 1787 1807 rBV 254714 517438 31.57% 4.987% 56 6.866 1950 1952 1954 rBV 162 114 0.01% 0.001% 57 7.005 1992 1995 1999 rVB 245 155 0.01% 0.001% 58 7.230 2052 2065 2088 rBV 130036 237210 14.47% 2.286% 59 7.416 2121 2123 2126 rVB2 245 136 0.01% 0.001% 60 7.432 2126 2128 2132 rVB 330 223 0.01% 0.002% 61 7.567 2157 2170 2212 rBV 474459 841165 51.32% 8.107% 62 7.854 2247 2259 2280 rBV 93227 161438 9.85% 1.556% 63 7.976 2295 2297 2302 rBV2 243 165 0.01% 0.002% 64 8.175 2355 2359 2369 rVB3 543 951 0.06% 0.009% 65 8.233 2375 2377 2380 rBV 271 183 0.01% 0.002% 66 8.313 2389 2402 2439 rBV 375032 666887 40.68% 6.427% 67 8.796 2550 2552 2556 rVB 258 138 0.01% 0.001% 68 9.095 2628 2645 2685 rBV 520803 883112 53.88% 8.511% 69 9.259 2690 2696 2700 rBV4 599 857 0.05% 0.008% 70 9.313 2709 2713 2714 rBV 237 171 0.01% 0.002% 71 9.381 2729 2734 2742 rVB3 890 1254 0.08% 0.012% 72 9.432 2747 2750 2752 rBV2 222 181 0.01% 0.002% 73 9.503 2770 2772 2775 rBV2 220 152 0.01% 0.001% 74 9.525 2775 2779 2783 rVV2 187 202 0.01% 0.002% 75 9.770 2853 2855 2857 rBV2 187 112 0.01% 0.001% 76 9.796 2857 2863 2867 rVV4 737 818 0.05% 0.008% 77 10.075 2943 2950 2953 rBV 310 404 0.02% 0.004% 78 10.149 2970 2973 2975 rBV 240 194 0.01% 0.002% 79 10.172 2975 2980 2987 rVV2 564 795 0.05% 0.008% 80 10.352 3031 3036 3040 rBV2 277 316 0.02% 0.003% 81 10.435 3049 3062 3082 rBV 370122 594239 36.25% 5.727% 82 10.535 3090 3093 3094 rBV 303 171 0.01% 0.002% 83 10.619 3108 3119 3126 rBV2 1405 2632 0.16% 0.025% 84 10.664 3130 3133 3135 rBV 197 134 0.01% 0.001% 85 10.863 3191 3195 3198 rVB2 236 202 0.01% 0.002% 86 10.889 3198 3203 3206 rBV2 260 317 0.02% 0.003% 87 10.937 3215 3218 3221 rBV 248 182 0.01% 0.002% 88 10.976 3225 3230 3232 rBV2 239 250 0.02% 0.002% 89 11.017 3240 3243 3247 rBV2 254 225 0.01% 0.002% 90 11.361 3347 3350 3355 rBV2 295 248 0.02% 0.002% 91 11.422 3365 3369 3377 rVB5 1371 1774 0.11% 0.017% 92 11.490 3377 3390 3415 rBV 494518 809392 49.38% 7.801% 93 11.660 3440 3443 3446 rVB 347 234 0.01% 0.002% 94 11.677 3446 3448 3452 rVV 203 113 0.01% 0.001% 95 11.699 3452 3455 3458 rVB2 399 222 0.01% 0.002% 96 11.863 3494 3506 3524 rBV 509715 833973 50.88% 8.038% 97 12.487 3695 3700 3708 rVB2 1033 1533 0.09% 0.015% 98 12.895 3823 3827 3839 rVB4 1549 2203 0.13% 0.021% 99 13.654 4060 4063 4067 rBV 717 490 0.03% 0.005% 100 14.001 4166 4171 4183 rVB5 1661 2599 0.16% 0.025% Sum of corrected areas: 10375654