Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_U\DATA\VU052318\ Data File : VU024037.D Acq On : 23 May 2018 15:01 Operator : MD/SY Sample : J3081-02 50X Misc : 5.0mL/MSVOA_U/WATER ALS Vial : 10 Sample Multiplier: 1 Quant Time: May 24 04:36:59 2018 Quant Method : W:\HPCHEM1\MSVOA_U\METHOD\SOMULM051218WMA.M Quant Title : VOC Analysis QLast Update : Thu May 24 04:14:38 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) 1,4-Difluorobenzene 5.89 114 278394 50.00 ug/L 0.00 28) Chlorobenzene-d5 9.09 117 289992 50.00 ug/L 0.00 60) 1,4-Dichlorobenzene-d4 11.49 152 123080 50.00 ug/L 0.00 System Monitoring Compounds 4) Vinyl Chloride-d3 1.40 65 21904 8.47 ug/L 0.00 Spiked Amount 50.000 Range 60 - 135 Recovery = 16.94%# 7) Chloroethane-d5 1.68 69 28235 13.85 ug/L 0.00 Spiked Amount 50.000 Range 70 - 130 Recovery = 27.70%# 11) 1,1-Dichloroethene-d2 2.27 63 27387 5.77 ug/L 0.00 Spiked Amount 50.000 Range 60 - 125 Recovery = 11.54%# 21) 2-Butanone-d5 4.18 46 193595 107.54 ug/L 0.00 Spiked Amount 100.000 Range 40 - 130 Recovery = 107.54% 24) Chloroform-d 4.65 84 102660 26.00 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 52.00%# 26) 1,2-Dichloroethane-d4 5.32 65 74763 28.78 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 57.56%# 32) Benzene-d6 5.35 84 121196 14.32 ug/L 0.00 Spiked Amount 50.000 Range 70 - 125 Recovery = 28.64%# 36) 1,2-Dichloropropane-d6 6.34 67 68484 23.95 ug/L 0.00 Spiked Amount 50.000 Range 70 - 120 Recovery = 47.90%# 41) Toluene-d8 7.57 98 75086 9.63 ug/L 0.00 Spiked Amount 50.000 Range 80 - 120 Recovery = 19.26%# 43) trans-1,3-Dichloropropene- 7.86 79 24599 20.45 ug/L 0.00 Spiked Amount 50.000 Range 60 - 125 Recovery = 40.90%# 47) 2-Hexanone-d5 8.32 63 120406 91.36 ug/L 0.00 Spiked Amount 100.000 Range 45 - 130 Recovery = 91.36% 57) 1,1,2,2-Tetrachloroethane- 10.44 84 167015 41.48 ug/L 0.00 Spiked Amount 50.000 Range 65 - 120 Recovery = 82.96% 64) 1,2-Dichlorobenzene-d4 11.87 152 85261 32.07 ug/L 0.00 Spiked Amount 50.000 Range 80 - 120 Recovery = 64.14%# Target Compounds Qvalue 20) cis-1,2-Dichloroethene 4.23 96 16307 6.81 ug/L 98 34) Trichloroethene 6.19 95 42987 17.67 ug/L 97 46) Tetrachloroethene 8.23 164 2550 1.28 ug/L 91 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed