Quantitation Report    (LSC Reviewed)

  Data Path : W:\HPCHEM1\MSVOA_U\DATA\VU052618\
  Data File : VU024160.D                                          
  Acq On    : 26 May 2018  21:21
  Operator  : MD/SY
  Sample    : J3091-13 10X
  Misc      : 5.0mL/MSVOA_U/WATER
  ALS Vial  : 19   Sample Multiplier: 1

  Quant Time: May 28 01:59:38 2018
  Quant Method : W:\HPCHEM1\MSVOA_U\METHOD\SOMULM052518WMA.M
  Quant Title  : VOC Analysis
  QLast Update : Mon May 28 00:49:31 2018
  Response via : Initial Calibration

   Internal Standards                R.T. QIon  Response  Conc Units Dev(Min)
   --------------------------------------------------------------------------
     1) 1,4-Difluorobenzene          5.89  114   291984    50.00 ug/L    0.00
    28) Chlorobenzene-d5             9.09  117   274569    50.00 ug/L    0.00
    60) 1,4-Dichlorobenzene-d4      11.49  152    93891    50.00 ug/L    0.00

   System Monitoring Compounds                                        
     4) Vinyl Chloride-d3            1.40   65    83840    37.77 ug/L    0.00  
     Spiked Amount     50.000   Range  60 - 135    Recovery   =   75.54% 
     7) Chloroethane-d5              1.68   69    73714    41.82 ug/L    0.00  
     Spiked Amount     50.000   Range  70 - 130    Recovery   =   83.64% 
    11) 1,1-Dichloroethene-d2        2.27   63   125937    30.50 ug/L    0.00  
     Spiked Amount     50.000   Range  60 - 125    Recovery   =   61.00% 
    21) 2-Butanone-d5                4.18   46   167646    95.00 ug/L    0.00  
     Spiked Amount    100.000   Range  40 - 130    Recovery   =   95.00% 
    24) Chloroform-d                 4.65   84   177827    44.71 ug/L    0.00  
     Spiked Amount     50.000   Range  70 - 125    Recovery   =   89.42% 
    26) 1,2-Dichloroethane-d4        5.31   65   114927    45.61 ug/L    0.00  
     Spiked Amount     50.000   Range  70 - 125    Recovery   =   91.22% 
    32) Benzene-d6                   5.35   84   342857    45.12 ug/L    0.00  
     Spiked Amount     50.000   Range  70 - 125    Recovery   =   90.24% 
    36) 1,2-Dichloropropane-d6       6.34   67   123131    47.28 ug/L    0.00  
     Spiked Amount     50.000   Range  70 - 120    Recovery   =   94.56% 
    41) Toluene-d8                   7.57   98   296483    42.10 ug/L    0.00  
     Spiked Amount     50.000   Range  80 - 120    Recovery   =   84.20% 
    43) trans-1,3-Dichloropropene-   7.85   79    43452    41.96 ug/L    0.00  
     Spiked Amount     50.000   Range  60 - 125    Recovery   =   83.92% 
    47) 2-Hexanone-d5                8.31   63   115279    92.78 ug/L    0.00  
     Spiked Amount    100.000   Range  45 - 130    Recovery   =   92.78% 
    57) 1,1,2,2-Tetrachloroethane-  10.44   84   171342    45.10 ug/L    0.00  
     Spiked Amount     50.000   Range  65 - 120    Recovery   =   90.20% 
    64) 1,2-Dichlorobenzene-d4      11.87  152   107820    52.38 ug/L    0.00  
     Spiked Amount     50.000   Range  80 - 120    Recovery   =  104.76% 

   Target Compounds                                                   Qvalue
     9) Trichlorofluoromethane       1.89  101     7869     2.22 ug/L      96
    34) Trichloroethene              6.19   95   234352    91.27 ug/L      98
    46) Tetrachloroethene            8.23  164     7465     4.16 ug/L      96
   --------------------------------------------------------------------------

   (#) = qualifier out of range (m) = manual integration (+) = signals summed