LSC Area Percent Report Data Path : W:\HPCHEM1\MSVOA_U\DATA\VU052618\ Data File : VU024177.D Acq On : 27 May 2018 09:00 Operator : MD/SY Sample : J3091-12 Misc : 5.0mL/MSVOA_U/WATER ALS Vial : 36 Sample Multiplier: 1 Integration Parameters: LSCINT.P Integrator: RTE Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 0 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Method : W:\HPCHEM1\MSVOA_U\METHOD\SOMULM052518WMA.M Title : VOC Analysis Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total --- ----- ----- ---- ---- --- ------- ------- ------ ------- 1 0.613 5 7 10 rBV 217 171 0.01% 0.002% 2 0.709 35 37 44 rVB2 232 214 0.02% 0.002% 3 0.812 65 69 72 rBV 220 189 0.02% 0.002% 4 0.838 72 77 83 rVB2 191 214 0.02% 0.002% 5 1.085 137 154 176 rBV 238440 288219 23.57% 2.697% 6 1.179 177 183 199 rVV2 68478 70900 5.80% 0.663% 7 1.291 214 218 226 rVB2 10174 10446 0.85% 0.098% 8 1.394 241 250 263 rBV2 203632 281941 23.05% 2.638% 9 1.452 263 268 281 rVB 31843 38754 3.17% 0.363% 10 1.519 282 289 299 rVV 51670 56930 4.65% 0.533% 11 1.667 328 335 347 rBV 137378 175174 14.32% 1.639% 12 1.815 373 381 391 rBV 34242 49459 4.04% 0.463% 13 2.259 508 519 533 rBV 279169 424607 34.72% 3.973% 14 2.336 535 543 572 rVB2 15373 37457 3.06% 0.350% 15 2.497 577 593 595 rBV5 3864 7921 0.65% 0.074% 16 2.834 684 698 718 rBV 21828 49730 4.07% 0.465% 17 3.079 771 774 779 rBV2 184 198 0.02% 0.002% 18 3.188 803 808 816 rVB3 1176 1854 0.15% 0.017% 19 3.227 817 820 824 rVB 244 207 0.02% 0.002% 20 3.285 836 838 844 rBV2 221 205 0.02% 0.002% 21 3.342 850 856 859 rBV 189 257 0.02% 0.002% 22 3.413 875 878 882 rBV2 324 252 0.02% 0.002% 23 3.432 882 884 889 rVB 342 247 0.02% 0.002% 24 3.461 889 893 895 rBV 180 174 0.01% 0.002% 25 3.526 908 913 918 rBV2 181 204 0.02% 0.002% 26 3.658 951 954 960 rVB 256 248 0.02% 0.002% 27 3.741 974 980 982 rBV3 333 364 0.03% 0.003% 28 4.121 1094 1098 1102 rBV 217 166 0.01% 0.002% 29 4.214 1105 1127 1169 rBV2 68511 342633 28.01% 3.206% 30 4.391 1173 1182 1209 rVB2 16056 46186 3.78% 0.432% 31 4.648 1245 1262 1285 rBV 194637 469114 38.36% 4.389% 32 4.805 1308 1311 1322 rVB3 483 543 0.04% 0.005% 33 4.883 1326 1335 1339 rBV4 837 1333 0.11% 0.012% 34 5.339 1452 1477 1515 rBV2 412764 1223069 100.00% 11.443% 35 5.609 1553 1561 1564 rBV4 1086 1439 0.12% 0.013% 36 5.809 1610 1623 1626 rBV2 334 532 0.04% 0.005% 37 5.889 1633 1648 1683 rBV 368347 772897 63.19% 7.231% 38 6.127 1720 1722 1726 rVB2 327 182 0.01% 0.002% 39 6.188 1726 1741 1772 rBV 414896 849391 69.45% 7.947% 40 6.333 1773 1786 1815 rVB 263563 549161 44.90% 5.138% 41 6.516 1838 1843 1845 rVB2 297 205 0.02% 0.002% 42 6.548 1849 1853 1855 rVB2 249 176 0.01% 0.002% 43 6.583 1862 1864 1869 rVB2 236 192 0.02% 0.002% 44 6.616 1870 1874 1878 rVB2 233 194 0.02% 0.002% 45 6.760 1914 1919 1924 rVB 174 170 0.01% 0.002% 46 6.834 1935 1942 1943 rBV3 758 818 0.07% 0.008% 47 6.886 1956 1958 1961 rVB2 386 183 0.01% 0.002% 48 6.905 1961 1964 1966 rVB2 379 197 0.02% 0.002% 49 7.008 1992 1996 2001 rBV2 550 683 0.06% 0.006% 50 7.175 2045 2048 2050 rBV 249 197 0.02% 0.002% 51 7.233 2053 2066 2094 rVV2 122558 242781 19.85% 2.271% 52 7.403 2108 2119 2130 rVB8 1704 3801 0.31% 0.036% 53 7.477 2138 2142 2143 rBV 326 190 0.02% 0.002% 54 7.509 2149 2152 2156 rBV3 258 196 0.02% 0.002% 55 7.567 2156 2170 2192 rBV 504936 919284 75.16% 8.601% 56 7.812 2243 2246 2248 rBV3 330 271 0.02% 0.003% 57 7.857 2249 2260 2284 rVB2 81380 157068 12.84% 1.470% 58 8.030 2313 2314 2322 rVV2 244 263 0.02% 0.002% 59 8.185 2347 2362 2367 rBV3 4671 8285 0.68% 0.078% 60 8.230 2368 2376 2390 rVB2 22596 39076 3.19% 0.366% 61 8.329 2390 2407 2445 rBV 280067 553612 45.26% 5.180% 62 8.554 2474 2477 2482 rVB3 493 397 0.03% 0.004% 63 8.580 2482 2485 2488 rVB3 311 194 0.02% 0.002% 64 8.789 2547 2550 2555 rVB 223 164 0.01% 0.002% 65 8.963 2599 2604 2606 rBV 319 230 0.02% 0.002% 66 9.095 2631 2645 2685 rBV 529558 916103 74.90% 8.571% 67 9.259 2689 2696 2705 rBV3 1146 1682 0.14% 0.016% 68 9.300 2705 2709 2710 rBV2 333 228 0.02% 0.002% 69 9.384 2729 2735 2745 rVB5 1587 2552 0.21% 0.024% 70 9.596 2798 2801 2806 rBV2 222 166 0.01% 0.002% 71 9.796 2853 2863 2868 rBV4 1226 1939 0.16% 0.018% 72 9.870 2882 2886 2891 rVB2 224 213 0.02% 0.002% 73 10.165 2974 2978 2979 rBV 303 202 0.02% 0.002% 74 10.255 2998 3006 3015 rVB5 2327 4009 0.33% 0.038% 75 10.320 3015 3026 3034 rBV5 1881 2985 0.24% 0.028% 76 10.439 3049 3063 3084 rBV 364632 579989 47.42% 5.426% 77 10.551 3095 3098 3100 rBV 308 163 0.01% 0.002% 78 10.612 3107 3117 3129 rVB 4645 7692 0.63% 0.072% 79 10.783 3164 3170 3174 rBV3 392 471 0.04% 0.004% 80 10.863 3192 3195 3202 rVB2 292 289 0.02% 0.003% 81 11.111 3269 3272 3277 rVB2 274 232 0.02% 0.002% 82 11.165 3286 3289 3292 rBV 184 175 0.01% 0.002% 83 11.262 3314 3319 3320 rBV2 190 192 0.02% 0.002% 84 11.332 3332 3341 3352 rVB 6674 10204 0.83% 0.095% 85 11.377 3353 3355 3360 rVB 354 189 0.02% 0.002% 86 11.426 3363 3370 3378 rBV2 2149 3166 0.26% 0.030% 87 11.490 3378 3390 3415 rBV 450786 710966 58.13% 6.652% 88 11.686 3447 3451 3456 rBV2 319 340 0.03% 0.003% 89 11.757 3462 3473 3489 rBV3 10451 23335 1.91% 0.218% 90 11.866 3494 3507 3525 rVB 450764 724524 59.24% 6.779% 91 12.037 3556 3560 3564 rVB3 787 676 0.06% 0.006% 92 12.088 3574 3576 3579 rVB2 395 185 0.02% 0.002% 93 12.201 3607 3611 3613 rBV2 261 182 0.01% 0.002% 94 12.406 3672 3675 3678 rVB2 260 161 0.01% 0.002% 95 12.448 3683 3688 3691 rVV2 493 603 0.05% 0.006% 96 12.480 3695 3698 3705 rVB4 907 1161 0.09% 0.011% 97 12.895 3822 3827 3836 rVB5 1732 2493 0.20% 0.023% 98 13.512 4017 4019 4029 rVB2 1067 1245 0.10% 0.012% 99 14.467 4313 4316 4322 rBV2 350 480 0.04% 0.004% 100 16.557 4960 4966 4975 rVB 5549 6970 0.57% 0.065% Sum of corrected areas: 10688171