Quantitation Report (QT Reviewed) Data Path : Z:\VOASRV\HPCHEM1\MSVOA_U\DATA\VU061318\ Data File : VU024502.D Acq On : 13 Jun 2018 12:42 Operator : MD/SY Sample : VSTDICCC050 Misc : 5.0mL/MSVOA_U/WATER ALS Vial : 5 Sample Multiplier: 1 Quant Time: Jun 13 13:14:22 2018 Quant Method : Z:\VOASRV\HPCHEM1\MSVOA_U\METHOD\82U061318W.M Quant Title : SW846 8260 QLast Update : Wed Jun 13 13:03:59 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 4.99 168 195529 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 5.89 114 310178 50.00 ug/l 0.00 63) Chlorobenzene-d5 9.09 117 293080 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 11.49 152 173479 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 5.31 65 161489 41.71 ug/l 0.00 Spiked Amount 50.000 Recovery = 83.42% 35) Dibromofluoromethane 4.89 113 129809 40.75 ug/l 0.00 Spiked Amount 50.000 Recovery = 81.50% 50) Toluene-d8 7.57 98 474811 39.88 ug/l 0.00 Spiked Amount 50.000 Recovery = 79.76% 62) 4-Bromofluorobenzene 10.31 95 186247 42.92 ug/l 0.00 Spiked Amount 50.000 Recovery = 85.84% Target Compounds Qvalue 2) Dichlorodifluoromethane 1.21 85 119205 40.221 ug/l 100 3) Chloromethane 1.33 50 115836 33.542 ug/l 100 4) Vinyl Chloride 1.40 62 125686 32.692 ug/l 99 5) Bromomethane 1.62 94 63196 29.913 ug/l 99 6) Chloroethane 1.70 64 74429 28.620 ug/l 100 7) Trichlorofluoromethane 1.89 101 188535 36.113 ug/l 98 8) Diethyl Ether 2.10 74 71051 34.042 ug/l 86 9) 1,1,2-Trichlorotrifluoroet 2.29 101 118208 40.677 ug/l 98 10) Methyl Iodide 2.41 142 101208 54.928 ug/l 99 11) Tert butyl alcohol 2.82 59 181996 247.463 ug/l 99 12) 1,1-Dichloroethene 2.28 96 111107 40.812 ug/l 94 13) Acrolein 2.19 56 98292 128.392 ug/l 98 14) Allyl chloride 2.60 41 197962 42.860 ug/l 97 15) Acrylonitrile 2.94 53 385728 196.369 ug/l 99 16) Acetone 2.32 43 406171 164.336 ug/l 98 17) Carbon Disulfide 2.48 76 348866 41.652 ug/l 99 18) Methyl Acetate 2.62 43 181427 36.937 ug/l 99 19) Methyl tert-butyl Ether 3.00 73 413159 48.294 ug/l 97 20) Methylene Chloride 2.71 84 126543 37.260 ug/l 99 21) trans-1,2-Dichloroethene 2.99 96 119400 40.875 ug/l 97 22) Diisopropyl ether 3.57 45 402483 43.247 ug/l 96 23) Vinyl Acetate 3.53 43 1844627 269.686 ug/l 99 24) 1,1-Dichloroethane 3.45 63 234653 40.271 ug/l 99 25) 2-Butanone 4.26 43 588419 199.093 ug/l 97 26) 2,2-Dichloropropane 4.23 77 218039 49.081 ug/l 99 27) cis-1,2-Dichloroethene 4.23 96 138036 43.488 ug/l 98 28) Bromochloromethane 4.55 49 110186 51.637 ug/l 89 29) Tetrahydrofuran 4.64 42 350425 207.771 ug/l 97 30) Chloroform 4.68 83 235405 39.873 ug/l 100 31) Cyclohexane 5.00 56 216825 37.523 ug/l 97 32) 1,1,1-Trichloroethane 4.92 97 213406 44.943 ug/l 96 36) 1,1-Dichloropropene 5.14 75 176568 39.889 ug/l 99 37) Ethyl Acetate 4.38 43 210491 42.412 ug/l 98 38) Carbon Tetrachloride 5.14 117 197238 46.794 ug/l 99 39) Methylcyclohexane 6.42 83 219420 45.879 ug/l 96 40) Benzene 5.39 78 514215 38.541 ug/l 100 41) Methacrylonitrile 4.54 41 113791 40.911 ug/l 99 42) 1,2-Dichloroethane 5.41 62 194589 38.082 ug/l 100 43) Isopropyl Acetate 5.55 43 334721 44.283 ug/l 97 44) Trichloroethene 6.19 130 141749 40.775 ug/l 97 45) 1,2-Dichloropropane 6.44 63 137232 38.272 ug/l 99 46) Dibromomethane 6.56 93 98191 41.363 ug/l 99 47) Bromodichloromethane 6.76 83 190225 41.418 ug/l 98 48) Methyl methacrylate 6.63 41 166426 44.913 ug/l 100 49) 1,4-Dioxane 6.61 88 60387 772.457 ug/l 99 51) 4-Methyl-2-Pentanone 7.46 43 1064211 195.149 ug/l 99 52) Toluene 7.64 92 327004 41.299 ug/l 98 53) t-1,3-Dichloropropene 7.88 75 218750 45.800 ug/l 99 54) cis-1,3-Dichloropropene 7.27 75 228784 43.901 ug/l 98 55) 1,1,2-Trichloroethane 8.07 97 128888 37.943 ug/l 99 56) Ethyl methacrylate 8.02 69 221680 50.073 ug/l 99 57) 1,3-Dichloropropane 8.25 76 223970 38.394 ug/l 98 58) 2-Chloroethyl Vinyl ether 7.13 63 442436 194.311 ug/l 96 59) 2-Hexanone 8.36 43 855730 196.135 ug/l 100 60) Dibromochloromethane 8.48 129 162447 47.132 ug/l 100 61) 1,2-Dibromoethane 8.59 107 146257 41.166 ug/l 99 64) Tetrachloroethene 8.23 164 139511 47.884 ug/l 99 65) Chlorobenzene 9.12 112 368774 43.237 ug/l 100 66) 1,1,1,2-Tetrachloroethane 9.21 131 138316 47.247 ug/l 98 67) Ethyl Benzene 9.25 91 644129 46.839 ug/l 97 68) m/p-Xylenes 9.38 106 494852 94.464 ug/l 98 69) o-Xylene 9.78 106 242084 50.135 ug/l 97 70) Styrene 9.80 104 404963 49.257 ug/l 98 71) Bromoform 9.96 173 130235 51.541 ug/l # 99 73) Isopropylbenzene 10.17 105 651781 54.498 ug/l 98 74) N-amyl acetate 10.01 43 310354 57.330 ug/l 97 75) 1,1,2,2-Tetrachloroethane 10.46 83 211831 40.836 ug/l 99 76) 1,2,3-Trichloropropane 10.50 75 188385m 51.774 ug/l 77) Bromobenzene 10.45 156 165582 49.999 ug/l 97 78) n-propylbenzene 10.59 91 772923 52.128 ug/l 97 79) 2-Chlorotoluene 10.66 91 448992 49.888 ug/l 98 80) 1,3,5-Trimethylbenzene 10.78 105 556275 54.846 ug/l 98 81) trans-1,4-Dichloro-2-buten 10.51 75 80572m 46.976 ug/l 82) 4-Chlorotoluene 10.78 91 529463 50.707 ug/l 99 83) tert-Butylbenzene 11.10 119 538380 54.531 ug/l 98 84) 1,2,4-Trimethylbenzene 11.15 105 577535 56.350 ug/l 100 85) sec-Butylbenzene 11.33 105 681754 54.999 ug/l 97 86) p-Isopropyltoluene 11.48 119 606761 55.387 ug/l 98 87) 1,3-Dichlorobenzene 11.42 146 304794 47.885 ug/l 99 88) 1,4-Dichlorobenzene 11.51 146 306820 46.048 ug/l 99 89) n-Butylbenzene 11.89 91 558562 51.818 ug/l 97 90) Hexachloroethane 12.15 117 115428 58.775 ug/l 99 91) 1,2-Dichlorobenzene 11.88 146 302359 47.504 ug/l 100 92) 1,2-Dibromo-3-Chloropropan 12.66 75 62519 59.045 ug/l 96 93) 1,2,4-Trichlorobenzene 13.51 180 211618 56.286 ug/l 99 94) Hexachlorobutadiene 13.70 225 107429 48.104 ug/l 99 95) Naphthalene 13.74 128 654365 63.651 ug/l 100 96) 1,2,3-Trichlorobenzene 13.99 180 213108 56.094 ug/l 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed